Synthesis of Insensitive N-2,4-dinitrophenyl-N1-nitroguanidine

A new, insensitive nitroguanidyl functionalized nitrogen-rich material derived from 2,4-dinitrophenyl derivative was synthesized. N-2,4-dinitrophenyl-N 1 -nitroguanidine (DNP-NQ) has a crystal density of 1.74 g/cm 3 . The synthesis and properties of DNP-NQ are described. DNP-NQ was characterized by...

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Bibliographic Details
Published inJournal of energetic materials Vol. 34; no. 4; pp. 395 - 398
Main Authors Warner, Kirstin F., Bellitto, Victor J., Sorensen, Daniel N., Remmers, Daniel L.
Format Journal Article
LanguageEnglish
Published Philadelphia Taylor & Francis 01.10.2016
Taylor & Francis Ltd
Subjects
4-dinitrophenyl
insensitive
nitroguanidyl functionality
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ISSN0737-0652
1545-8822
DOI10.1080/07370652.2015.1107661

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Summary:A new, insensitive nitroguanidyl functionalized nitrogen-rich material derived from 2,4-dinitrophenyl derivative was synthesized. N-2,4-dinitrophenyl-N 1 -nitroguanidine (DNP-NQ) has a crystal density of 1.74 g/cm 3 . The synthesis and properties of DNP-NQ are described. DNP-NQ was characterized by nuclear magnetic resonance (NMR), infrared spectroscopy, and gas pycnometry. Thermal properties were studied by differential scanning calorimetry (DSC). Results from small-scale sensitivity tests indicate that DNP-NQ is less sensitive than Cyclotrimethylenetrinitramine (RDX). DNP-NQ can be prepared in high yield.
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ISSN:0737-0652
1545-8822
DOI:10.1080/07370652.2015.1107661