壳聚糖澄清芦柑果汁工艺条件的优化

为了制备稳定的澄清芦柑果汁,该文基于Box-Behnken试验设计,探讨了壳聚糖浓度、澄清温度、澄清时间对果汁澄清度的影响;建立了二次多项式回归模型,分析模型的有效性与因子间的交互作用,并对壳聚糖澄清芦柑果汁的工艺参数进行了优化。结果表明：壳聚糖澄清芦柑果汁的最佳工艺参数为：壳聚糖浓度0.80 g/L、温度59℃和时间71 min。在此最佳工艺条件下果汁透光率达到97.8%,且试验结果与模型预测值（98.3%）相吻合,所得回归模型拟合情况良好（R2=0.9886）,达到设计要求。进一步对经壳聚糖澄清后的芦柑果汁的相关指标进行测定,发现果汁中可溶性固形物、维生素C及总酸含量依次从11.30±0....

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Bibliographic Details
Published in农业工程学报 Vol. 29; no. 23; pp. 268 - 275
Main Author 许键 蔡慧农 倪辉 杜希萍 黄高凌
Format Journal Article
LanguageChinese
Published 集美大学生物工程学院,厦门,361021%集美大学生物工程学院，厦门 361021 2013
福建省高校食品微生物与酶工程技术研究中心，厦门 361021
厦门市食品与生物工程技术研究中心，厦门 361021
Subjects
优化
加工
品质调控
响应面
壳聚糖
澄清
芦柑汁
品质调控
芦柑汁
chitosan
quality control
clarification
response surface methodology
澄清
加工
响应面
壳聚糖
optimization
优化
ponkan juice
processing
Online AccessGet full text
ISSN1002-6819
DOI10.3969/j.issn.1002-6819.2013.23.037

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Summary:为了制备稳定的澄清芦柑果汁,该文基于Box-Behnken试验设计,探讨了壳聚糖浓度、澄清温度、澄清时间对果汁澄清度的影响;建立了二次多项式回归模型,分析模型的有效性与因子间的交互作用,并对壳聚糖澄清芦柑果汁的工艺参数进行了优化。结果表明：壳聚糖澄清芦柑果汁的最佳工艺参数为：壳聚糖浓度0.80 g/L、温度59℃和时间71 min。在此最佳工艺条件下果汁透光率达到97.8%,且试验结果与模型预测值（98.3%）相吻合,所得回归模型拟合情况良好（R2=0.9886）,达到设计要求。进一步对经壳聚糖澄清后的芦柑果汁的相关指标进行测定,发现果汁中可溶性固形物、维生素C及总酸含量依次从11.30±0.15%、31.33±3.25 mg/100mL、0.71±0.00 g/100mL略降为9.50±0.25%、21.8±5.28 mg/100mL、0.51±0 g/100mL,而总酚、果胶、蛋白质质量浓度依次从990.3±8.02 mg/L、366±4.70μg/mL、595.53±20.62μg/mL减少为557.87±4.67 mg/L、186.24±44.32μg/mL、26.42±0.30μg/mL有较明显下降,但澄清后的果汁非生物稳定性很好。该试验用响应面法优选出的澄清工艺合理可行,为芦柑果汁深加工及果汁产品开发提供了理论依据。
Bibliography:11-2047/S
Clarity of juice is an important factor regarding the quality of the juice as it fetches consumer attention for the product in the market. Clarification is a key step in the processing of fruit juice and is most often achieved through micro filtration, enzymatic treatment, or by using common clarifying aids like chitosan, gelatin, bentonite, silica sol, polyvinyl pyrrolidine, or a combination of these compounds. Chitosan（poly-b（1–4）N-acetyl-glucosamine） being poly-cationic in nature, nontoxic, and biodegradable, has been found to be an effective coagulating agent in aiding the removing pectin and other carbohydrates which are present in the juice. The clarification of ponkan juice by means of chitosan was studied in this paper. In order to obtain the optimal reaction conditions of clarification of ponkan juice by commercially inexpensive chitosan, the process conditions of clarification with chitosan on ponkan juice were optimized by a Box-Behnken center-united experiment design. Taking juice clarifi
ISSN:1002-6819
DOI:10.3969/j.issn.1002-6819.2013.23.037