Simultaneous determination of trichothecene mycotoxins in cereals by LC-MS/MS
This study was designed to determine the residual trichothecene mycotoxins in cereal samples. The optimal solvent for extraction was 84% (v/v) aqueous acetonitrile with 1% (v/v) formic acid. The best performing clean-up method was dispersive-solid phase with a mixture octadecyl silica and primary-se...
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| Published in | Food science and biotechnology Vol. 31; no. 2; pp. 165 - 174 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Singapore
Springer Singapore
01.02.2022
Springer Nature B.V 한국식품과학회 |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1226-7708 2092-6456 2092-6456 |
| DOI | 10.1007/s10068-021-01024-5 |
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| Abstract | This study was designed to determine the residual trichothecene mycotoxins in cereal samples. The optimal solvent for extraction was 84% (v/v) aqueous acetonitrile with 1% (v/v) formic acid. The best performing clean-up method was dispersive-solid phase with a mixture octadecyl silica and primary-secondary amine. The recoveries for the studied mycotoxins ranged from 83.3 to 92.8%. The methodology was successfully applied for monitoring 100 cereal samples obtained from a Korean market. The bean sample were found to be co-contamination with deoxynivalenol and HT-2 toxin. Deoxynivalenol possessed the highest detection freauency (4/100) and amount (727.38 µg/kg) among the trichothecene mycotoxins. The hazard index was less than 1.0 for all the observed mycotoxins in all cereal samples except one white rice sample (1.2681). This results indicated that periodic risk assessments of trichothecene mycotoxin through cereal intake are necessary for the health and safety. |
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| AbstractList | This study was designed to determine the residual trichothecene mycotoxins in cereal samples. The optimal solvent for extraction was 84% (v/v) aqueous acetonitrile with 1% (v/v) formic acid. The best performing clean-up method was dispersive-solid phase with a mixture octadecyl silica and primary-secondary amine. The recoveries for the studied mycotoxins ranged from 83.3 to 92.8%. The methodology was successfully applied for monitoring 100 cereal samples obtained from a Korean market. The bean sample were found to be co-contamination with deoxynivalenol and HT-2 toxin. Deoxynivalenol possessed the highest detection freauency (4/100) and amount (727.38 µg/kg) among the trichothecene mycotoxins. The hazard index was less than 1.0 for all the observed mycotoxins in all cereal samples except one white rice sample (1.2681). This results indicated that periodic risk assessments of trichothecene mycotoxin through cereal intake are necessary for the health and safety.This study was designed to determine the residual trichothecene mycotoxins in cereal samples. The optimal solvent for extraction was 84% (v/v) aqueous acetonitrile with 1% (v/v) formic acid. The best performing clean-up method was dispersive-solid phase with a mixture octadecyl silica and primary-secondary amine. The recoveries for the studied mycotoxins ranged from 83.3 to 92.8%. The methodology was successfully applied for monitoring 100 cereal samples obtained from a Korean market. The bean sample were found to be co-contamination with deoxynivalenol and HT-2 toxin. Deoxynivalenol possessed the highest detection freauency (4/100) and amount (727.38 µg/kg) among the trichothecene mycotoxins. The hazard index was less than 1.0 for all the observed mycotoxins in all cereal samples except one white rice sample (1.2681). This results indicated that periodic risk assessments of trichothecene mycotoxin through cereal intake are necessary for the health and safety. This study was designed to determine theresidual trichothecene mycotoxins in cereal samples. Theoptimal solvent for extraction was 84% (v/v) aqueousacetonitrile with 1% (v/v) formic acid. The best performingclean-up method was dispersive-solid phase with a mixtureoctadecyl silica and primary-secondary amine. The recoveriesfor the studied mycotoxins ranged from 83.3 to92.8%. The methodology was successfully applied formonitoring 100 cereal samples obtained from a Koreanmarket. The bean sample were found to be co-contaminationwith deoxynivalenol and HT-2 toxin. Deoxynivalenolpossessed the highest detection freauency (4/100) andamount (727.38 lg/kg) among the trichothecene mycotoxins. The hazard index was less than 1.0 for all theobserved mycotoxins in all cereal samples except onewhite rice sample (1.2681). This results indicated thatperiodic risk assessments of trichothecene mycotoxinthrough cereal intake are necessary for the health andsafety. KCI Citation Count: 2 This study was designed to determine the residual trichothecene mycotoxins in cereal samples. The optimal solvent for extraction was 84% (v/v) aqueous acetonitrile with 1% (v/v) formic acid. The best performing clean-up method was dispersive-solid phase with a mixture octadecyl silica and primary-secondary amine. The recoveries for the studied mycotoxins ranged from 83.3 to 92.8%. The methodology was successfully applied for monitoring 100 cereal samples obtained from a Korean market. The bean sample were found to be co-contamination with deoxynivalenol and HT-2 toxin. Deoxynivalenol possessed the highest detection freauency (4/100) and amount (727.38 µg/kg) among the trichothecene mycotoxins. The hazard index was less than 1.0 for all the observed mycotoxins in all cereal samples except one white rice sample (1.2681). This results indicated that periodic risk assessments of trichothecene mycotoxin through cereal intake are necessary for the health and safety. This study was designed to determine the residual trichothecene mycotoxins in cereal samples. The optimal solvent for extraction was 84% (v/v) aqueous acetonitrile with 1% (v/v) formic acid. The best performing clean-up method was dispersive-solid phase with a mixture octadecyl silica and primary-secondary amine. The recoveries for the studied mycotoxins ranged from 83.3 to 92.8%. The methodology was successfully applied for monitoring 100 cereal samples obtained from a Korean market. The bean sample were found to be co-contamination with deoxynivalenol and HT-2 toxin. Deoxynivalenol possessed the highest detection freauency (4/100) and amount (727.38 µg/kg) among the trichothecene mycotoxins. The hazard index was less than 1.0 for all the observed mycotoxins in all cereal samples except one white rice sample (1.2681). This results indicated that periodic risk assessments of trichothecene mycotoxin through cereal intake are necessary for the health and safety. |
| Author | Yoo, Miyoung Lee, Sanghee Nam, Tae Gyu Jung, Young Sung Kim, Dan-Bi |
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| Cites_doi | 10.5740/jaoacint.17-0340 10.4141/cjas92-082 10.1016/j.chroma.2016.12.040 10.2903/j.efsa.2011.2481 10.1007/s10068-018-0537-4 10.1016/j.fct.2020.111280 10.4155/bio-2017-0214 10.1038/srep24328 10.1007/s12550-016-0257-7 10.2298/JSC0507005A 10.1016/j.foodcont.2012.07.041 10.1016/j.foodchem.2009.05.082 10.1016/j.foodchem.2015.01.040 10.1007/s12161-013-9785-3 10.3390/foods9020137 10.1016/j.chroma.2017.11.050 10.1111/j.1541-4337.2009.00079.x 10.4315/0362-028X.JFP-17-006 10.1002/fsn3.959 10.1016/j.yrtph.2009.09.013 10.1111/ijfs.14734 10.1016/j.foodcont.2005.06.001 10.1016/j.foodcont.2020.107171 10.1039/c5tx00293a 10.2174/1389200211314060002 10.1016/j.etap.2003.11.009 10.1007/s10068-021-00943-7 |
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| SubjectTerms | Acetonitrile beans biotechnology Cereals Chemistry Chemistry and Materials Science Contamination Deoxynivalenol Food Science Formic acid HT-2 toxin markets Mycotoxins Nutrition Research Article rice risk Risk assessment Silica Silicon dioxide Solid phases solvents Toxins 식품과학 |
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