Quantitative detection using two‐dimension shell‐isolated nanoparticle film

Surface‐enhanced Raman spectroscopy (SERS) can provide a fingerprint of molecules with ultrahigh sensitivity, down to the single‐molecule level. However, accurate quantitative detection in practical samples using SERS is still a great challenge. Herein, a highly uniform shell‐isolated Ag@SiO2 nanopa...

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Published in	Journal of Raman spectroscopy Vol. 48; no. 7; pp. 919 - 924
Main Authors	Yang, Jing‐Liang, Yang, Zhen‐Wei, Zhang, Yue‐Jiao, Ren, He, Zhang, Hua, Xu, Qing‐Chi, Panneerselvam, Rajapandiyan, Sivashanmugan, Kundan, Li, Jian‐Feng, Tian, Zhong‐Qun
Format	Journal Article
Language	English
Published	Bognor Regis Wiley Subscription Services, Inc 01.07.2017
Subjects	Ag@SiO2 nanoparticle Melamine Milk Nanoparticles quantitative analysis Raman spectroscopy Reproducibility Sensitivity shell‐isolated nanoparticle‐enhanced Raman spectroscopy Silicon dioxide Silver Spectroscopy Spectrum analysis surface‐enhanced Raman spectroscopy
Online Access	Get full text
ISSN	0377-0486 1097-4555
DOI	10.1002/jrs.5151

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Abstract	Surface‐enhanced Raman spectroscopy (SERS) can provide a fingerprint of molecules with ultrahigh sensitivity, down to the single‐molecule level. However, accurate quantitative detection in practical samples using SERS is still a great challenge. Herein, a highly uniform shell‐isolated Ag@SiO2 nanoparticle (Ag SHIN) monolayer film was prepared and employed as a substrate for the quantitative determination of melamine in milk samples through shell‐isolated nanoparticle‐enhanced Raman spectroscopy. The Ag SHIN film exhibits excellent reproducibility, high stability, as well as ultrahigh sensitivity with a limit of detection of 0.03 ppm. A linear relationship between the Raman intensity and the melamine concentration in a wide range (1 ppb to 5 ppm) was obtained. These results demonstrate that the Ag SHIN monolayer film is a promising and reliable substrate for the quantitative SERS analysis of practical samples. Copyright © 2017 John Wiley & Sons, Ltd. A highly uniform, reproducible, and stable shell‐isolated Ag@SiO2 nanoparticle monolayer film was prepared. It was employed as a substrate for the quantitative determination of melamine in milk samples through shell‐isolated nanoparticle‐enhanced Raman spectroscopy, and showed ultrahigh sensitivity with a limit of detection down to 0.03 ppm.
AbstractList	Surface‐enhanced Raman spectroscopy (SERS) can provide a fingerprint of molecules with ultrahigh sensitivity, down to the single‐molecule level. However, accurate quantitative detection in practical samples using SERS is still a great challenge. Herein, a highly uniform shell‐isolated Ag@SiO2 nanoparticle (Ag SHIN) monolayer film was prepared and employed as a substrate for the quantitative determination of melamine in milk samples through shell‐isolated nanoparticle‐enhanced Raman spectroscopy. The Ag SHIN film exhibits excellent reproducibility, high stability, as well as ultrahigh sensitivity with a limit of detection of 0.03 ppm. A linear relationship between the Raman intensity and the melamine concentration in a wide range (1 ppb to 5 ppm) was obtained. These results demonstrate that the Ag SHIN monolayer film is a promising and reliable substrate for the quantitative SERS analysis of practical samples. Copyright © 2017 John Wiley & Sons, Ltd. A highly uniform, reproducible, and stable shell‐isolated Ag@SiO2 nanoparticle monolayer film was prepared. It was employed as a substrate for the quantitative determination of melamine in milk samples through shell‐isolated nanoparticle‐enhanced Raman spectroscopy, and showed ultrahigh sensitivity with a limit of detection down to 0.03 ppm. Surface‐enhanced Raman spectroscopy (SERS) can provide a fingerprint of molecules with ultrahigh sensitivity, down to the single‐molecule level. However, accurate quantitative detection in practical samples using SERS is still a great challenge. Herein, a highly uniform shell‐isolated Ag@SiO 2 nanoparticle (Ag SHIN) monolayer film was prepared and employed as a substrate for the quantitative determination of melamine in milk samples through shell‐isolated nanoparticle‐enhanced Raman spectroscopy. The Ag SHIN film exhibits excellent reproducibility, high stability, as well as ultrahigh sensitivity with a limit of detection of 0.03 ppm. A linear relationship between the Raman intensity and the melamine concentration in a wide range (1 ppb to 5 ppm) was obtained. These results demonstrate that the Ag SHIN monolayer film is a promising and reliable substrate for the quantitative SERS analysis of practical samples. Copyright © 2017 John Wiley & Sons, Ltd. Surface-enhanced Raman spectroscopy (SERS) can provide a fingerprint of molecules with ultrahigh sensitivity, down to the single-molecule level. However, accurate quantitative detection in practical samples using SERS is still a great challenge. Herein, a highly uniform shell-isolated Ag@SiO2 nanoparticle (Ag SHIN) monolayer film was prepared and employed as a substrate for the quantitative determination of melamine in milk samples through shell-isolated nanoparticle-enhanced Raman spectroscopy. The Ag SHIN film exhibits excellent reproducibility, high stability, as well as ultrahigh sensitivity with a limit of detection of 0.03 ppm. A linear relationship between the Raman intensity and the melamine concentration in a wide range (1 ppb to 5 ppm) was obtained. These results demonstrate that the Ag SHIN monolayer film is a promising and reliable substrate for the quantitative SERS analysis of practical samples. Copyright © 2017 John Wiley & Sons, Ltd.
Author	Xu, Qing‐Chi Tian, Zhong‐Qun Yang, Zhen‐Wei Yang, Jing‐Liang Ren, He Sivashanmugan, Kundan Zhang, Hua Panneerselvam, Rajapandiyan Zhang, Yue‐Jiao Li, Jian‐Feng
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Snippet	Surface‐enhanced Raman spectroscopy (SERS) can provide a fingerprint of molecules with ultrahigh sensitivity, down to the single‐molecule level. However,... Surface-enhanced Raman spectroscopy (SERS) can provide a fingerprint of molecules with ultrahigh sensitivity, down to the single-molecule level. However,...
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SubjectTerms	Ag@SiO2 nanoparticle Melamine Milk Nanoparticles quantitative analysis Raman spectroscopy Reproducibility Sensitivity shell‐isolated nanoparticle‐enhanced Raman spectroscopy Silicon dioxide Silver Spectroscopy Spectrum analysis surface‐enhanced Raman spectroscopy
Title	Quantitative detection using two‐dimension shell‐isolated nanoparticle film
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