Depth-sensing cyclic nanoindentation of tantalum

• Published in: International journal of refractory metals & hard materials Vol. 66; pp. 144 - 149
• Main Authors: Haghshenas, M., Klassen, R.J., Liu, S.F.
• Format: Journal Article
• Language: English
• Published: Shrewsbury Elsevier BV 01.08.2017
• Subjects: Data acquisition; Dislocation density; Hardness testing; Indentation; Nanoindentation; Plastic deformation; Sensitivity; Size effects; Strain rate; Strain rate sensitivity; Tantalum; Yield strength
• ISSN: 0263-4368
• DOI: 10.1016/j.ijrmhm.2017.03.015

In the present paper, depth-sensing multi-cycling instrumented indentation testing of tantalum is studied to assess depth-dependent plastic deformation of the metal at room temperature. Loading/unloading/reloading scheme in cyclic indentation testing is a reliable indentation-based approach in which data collection is not necessarily adversely affected by lateral in-homogeneities of the sample leading to more accurate measurements. The experimental results show indentation size effect (ISE) and depth-dependent strain rate sensitivity in Ta. To interpret these phenomena, the density of geometrically necessary dislocations (GNDs) and statistically stored dislocations (SSDs) constructed by the Nix-Gao model were used. The observed dependence of hardness and activation volume upon indentation depth indicated that the average flow stress, and hence the average plastic strain, is higher around the small indentations than around the deep indentations.