Analysis of Electroless Copper Plating Baths by Isotachophoresis
Simultaneous analysis of EDTA (complexing agent), Cu-EDTA (copper complex of EDTA) and formate (oxidation product of formaldehyde) contained in copper plating baths used in the full-additive process was carried out within 20 minutes, by isotachophoresis using hydrochloric acid and histidine (pH 6.0)...
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| Published in | Journal of the Metal Finishing Society of Japan Vol. 37; no. 4; pp. 195 - 199 |
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| Main Authors | , , |
| Format | Journal Article |
| Language | Japanese |
| Published |
The Surface Finishing Society of Japan
01.01.1986
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| Online Access | Get full text |
| ISSN | 0026-0614 1884-3395 1884-3395 |
| DOI | 10.4139/sfj1950.37.195 |
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| Summary: | Simultaneous analysis of EDTA (complexing agent), Cu-EDTA (copper complex of EDTA) and formate (oxidation product of formaldehyde) contained in copper plating baths used in the full-additive process was carried out within 20 minutes, by isotachophoresis using hydrochloric acid and histidine (pH 6.0) as the leading electrolyte and sodium caproate as the terminal electrolyte. Free copper ions were not detected. Gas chromatography showed that the formaldehyde decreased in proportion to the increase of formate. This shows that isotachophoresis can be used to monitor the concentration of the reducing agent (formaldehyde) in a copper plating bath. Several amines and amino acids added to the copper plating bath were also determined. |
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| Bibliography: | ObjectType-Article-2 SourceType-Scholarly Journals-1 ObjectType-Feature-1 content type line 23 |
| ISSN: | 0026-0614 1884-3395 1884-3395 |
| DOI: | 10.4139/sfj1950.37.195 |