碱熔-电感耦合等离子体质谱法测定铌钽矿中铌钽锂铍
TD985%P575; 这是一篇矿物分析测试领域的论文.建立了碱熔-电感耦合等离子体质谱法同时测定铌钽矿中铌钽锂铍的快速测定方法.采用过氧化钠∶氢氧化钠=1∶1的混合熔剂分解样品,水提取使铌钽等元素完全形成沉淀,与液体分离,采用10％硫酸+10％过氧化氢溶液25 mL转化沉淀和溶液后用电感耦合等离子体质谱仪测定样品中铌、钽、锂、铍元素的含量.采用该方法测定国家一级标准物质GBW 07153、GBW 07155、GBW 07185,各元素的测定值与认定值基本一致,相对误差为0.50％～4.77％,相对标准偏差(n=6)为-0.009％～0.008％,适用于铌钽精矿、难分解或复杂样品中铌钽等元素的...
Saved in:
| Published in | 矿产综合利用 Vol. 45; no. 3; pp. 200 - 205 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | Chinese |
| Published |
河南省岩石矿物测试中心自然资源部贵金属分析与勘查技术重点实验室,河南 郑州 450012%华北水利水电大学,河南 郑州 450012
2024
河南省地质局地质灾害防治中心,河南 郑州 450012 |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1000-6532 |
| DOI | 10.3969/j.issn.1000-6532.2024.03.031 |
Cover
| Abstract | TD985%P575; 这是一篇矿物分析测试领域的论文.建立了碱熔-电感耦合等离子体质谱法同时测定铌钽矿中铌钽锂铍的快速测定方法.采用过氧化钠∶氢氧化钠=1∶1的混合熔剂分解样品,水提取使铌钽等元素完全形成沉淀,与液体分离,采用10％硫酸+10％过氧化氢溶液25 mL转化沉淀和溶液后用电感耦合等离子体质谱仪测定样品中铌、钽、锂、铍元素的含量.采用该方法测定国家一级标准物质GBW 07153、GBW 07155、GBW 07185,各元素的测定值与认定值基本一致,相对误差为0.50％～4.77％,相对标准偏差(n=6)为-0.009％～0.008％,适用于铌钽精矿、难分解或复杂样品中铌钽等元素的测定,并在生产实践中进行了应用. |
|---|---|
| AbstractList | TD985%P575; 这是一篇矿物分析测试领域的论文.建立了碱熔-电感耦合等离子体质谱法同时测定铌钽矿中铌钽锂铍的快速测定方法.采用过氧化钠∶氢氧化钠=1∶1的混合熔剂分解样品,水提取使铌钽等元素完全形成沉淀,与液体分离,采用10％硫酸+10％过氧化氢溶液25 mL转化沉淀和溶液后用电感耦合等离子体质谱仪测定样品中铌、钽、锂、铍元素的含量.采用该方法测定国家一级标准物质GBW 07153、GBW 07155、GBW 07185,各元素的测定值与认定值基本一致,相对误差为0.50％～4.77％,相对标准偏差(n=6)为-0.009％～0.008％,适用于铌钽精矿、难分解或复杂样品中铌钽等元素的测定,并在生产实践中进行了应用. |
| Abstract_FL | This is an article in the field of mineral analysis and testing.A rapid method for the simultaneous determination of Nb,Ta,Li and Be in Nb Ta ore by alkali fusion inductively coupled plasma mass spectrometry was established.The mixed alkali of sodium peroxide and sodium hydroxide=1∶1 is used to decompose the sample.During extraction,niobium,tantalum and other elements are completely precipitated and separated from the liquid.The content of niobium,tantalum,lithium and beryllium in the sample is determined by inductively coupled plasma mass spectrometer after conversion and precipitation with 25 mL of 10％sulfuric acid+10％hydrogen peroxide solution.This method is used to determine the national first-class reference materials GBW 07153,GBW 07155 and GBW 07185.The measured values of each element are basically consistent with the certified values,with a relative error of 0.50％～4.77％and a relative standard deviation(n=6)of-0.009％～0.008％.It is applicable to the determination of niobium and tantalum in niobium tantalum concentrates,refractory or complex samples,and has been applied in production practice. |
| Author | 崔承洋 李志伟 钟莅湘 李振 |
| AuthorAffiliation | 河南省地质局地质灾害防治中心,河南 郑州 450012;河南省岩石矿物测试中心自然资源部贵金属分析与勘查技术重点实验室,河南 郑州 450012%华北水利水电大学,河南 郑州 450012 |
| AuthorAffiliation_xml | – name: 河南省地质局地质灾害防治中心,河南 郑州 450012;河南省岩石矿物测试中心自然资源部贵金属分析与勘查技术重点实验室,河南 郑州 450012%华北水利水电大学,河南 郑州 450012 |
| Author_FL | LI Zhen ZHONG Lixiang CUI Chengyang LI Zhiwei |
| Author_FL_xml | – sequence: 1 fullname: LI Zhen – sequence: 2 fullname: ZHONG Lixiang – sequence: 3 fullname: CUI Chengyang – sequence: 4 fullname: LI Zhiwei |
| Author_xml | – sequence: 1 fullname: 李振 – sequence: 2 fullname: 钟莅湘 – sequence: 3 fullname: 崔承洋 – sequence: 4 fullname: 李志伟 |
| BookMark | eNo9T8tKw0AA3EMFa-1fCJ4S95HNZo9SrAoFL3oum01WW0sKLiJ6EhFRVCgmXrwUPBQvEYsWBCn-TPP6CyMVYWCGGZhhlkAl6Ac-ACsImoTbfK1rdrQOTAQhNGxKsIkhtkxISqAKqP77i6CudceFxLaIxSiqgmb2PM6uIiOLJunlMD8fJYPrLL7JRl9JPJhNw_zjJX8bp--P6eQ2eX0qwrviYZoNv2ef8VwX0UUR3i-DBSV62q__cQ3sNTd2G1tGa2dzu7HeMjSCGBlCccu2KFOCMgc50uYegx7lDhO-JBALyJWShEipHIbLDAvKhed7rssYYpzUwOq890QESgT77W7_-CgoF9uH8uygd_r7G5LyNfkBBKxqYg |
| ClassificationCodes | TD985%P575 |
| ContentType | Journal Article |
| Copyright | Copyright © Wanfang Data Co. Ltd. All Rights Reserved. |
| Copyright_xml | – notice: Copyright © Wanfang Data Co. Ltd. All Rights Reserved. |
| DBID | 2B. 4A8 92I 93N PSX TCJ |
| DOI | 10.3969/j.issn.1000-6532.2024.03.031 |
| DatabaseName | Wanfang Data Journals - Hong Kong WANFANG Data Centre Wanfang Data Journals 万方数据期刊 - 香港版 China Online Journals (COJ) China Online Journals (COJ) |
| DatabaseTitleList | |
| DeliveryMethod | fulltext_linktorsrc |
| DocumentTitle_FL | Determination of Niobium,Tantalum,Lithium and Beryllium in Niobium Tantalum Ore by Alkali Fusion Inductively Coupled Plasma Mass Spectrometry |
| EndPage | 205 |
| ExternalDocumentID | kczhly202403031 |
| GrantInformation_xml | – fundername: 国土资源部公益性行业科研专项-自然资源行业标准修订计划 funderid: (201919035) |
| GroupedDBID | -02 2B. 4A8 92I 93N ALMA_UNASSIGNED_HOLDINGS CCEZO CDRFL GROUPED_DOAJ PSX TCJ |
| ID | FETCH-LOGICAL-s1021-af946457fa57818c69d70d5987aec302a09ffc33ccf872d702a59adedbb771793 |
| ISSN | 1000-6532 |
| IngestDate | Thu May 29 03:58:33 EDT 2025 |
| IsPeerReviewed | true |
| IsScholarly | true |
| Issue | 3 |
| Keywords | 电感耦合等离子体质谱法 锂 Lithium 碱熔 铌 铍 矿物分析测试 Niobium Alkali fusion Tantalum Beryllium Inductively coupled plasma mass spectrometry 钽 Mineral analysis and testing |
| Language | Chinese |
| LinkModel | OpenURL |
| MergedId | FETCHMERGED-LOGICAL-s1021-af946457fa57818c69d70d5987aec302a09ffc33ccf872d702a59adedbb771793 |
| PageCount | 6 |
| ParticipantIDs | wanfang_journals_kczhly202403031 |
| PublicationCentury | 2000 |
| PublicationDate | 2024 |
| PublicationDateYYYYMMDD | 2024-01-01 |
| PublicationDate_xml | – year: 2024 text: 2024 |
| PublicationDecade | 2020 |
| PublicationTitle | 矿产综合利用 |
| PublicationTitle_FL | Multipurpose Utilization of Mineral Resources |
| PublicationYear | 2024 |
| Publisher | 河南省岩石矿物测试中心自然资源部贵金属分析与勘查技术重点实验室,河南 郑州 450012%华北水利水电大学,河南 郑州 450012 河南省地质局地质灾害防治中心,河南 郑州 450012 |
| Publisher_xml | – name: 河南省岩石矿物测试中心自然资源部贵金属分析与勘查技术重点实验室,河南 郑州 450012%华北水利水电大学,河南 郑州 450012 – name: 河南省地质局地质灾害防治中心,河南 郑州 450012 |
| SSID | ssib036434751 ssib051374773 ssj0002912118 ssib000270156 ssib001105368 ssib012291026 |
| Score | 2.3697784 |
| Snippet | TD985%P575; 这是一篇矿物分析测试领域的论文.建立了碱熔-电感耦合等离子体质谱法同时测定铌钽矿中铌钽锂铍的快速测定方法.采用过氧化钠∶氢氧化钠=1∶1的混合熔剂分解样品,... |
| SourceID | wanfang |
| SourceType | Aggregation Database |
| StartPage | 200 |
| Title | 碱熔-电感耦合等离子体质谱法测定铌钽矿中铌钽锂铍 |
| URI | https://d.wanfangdata.com.cn/periodical/kczhly202403031 |
| Volume | 45 |
| hasFullText | 1 |
| inHoldings | 1 |
| isFullTextHit | |
| isPrint | |
| journalDatabaseRights | – providerCode: PRVAON databaseName: DOAJ Directory of Open Access Journals issn: 1000-6532 databaseCode: DOA dateStart: 20180101 customDbUrl: isFulltext: true dateEnd: 99991231 titleUrlDefault: https://www.doaj.org/ omitProxy: true ssIdentifier: ssj0002912118 providerName: Directory of Open Access Journals |
| link | http://utb.summon.serialssolutions.com/2.0.0/link/0/eLvHCXMwnR1Na9VAMJQK4kUUFb_poXsqryb7kewekzShCHpqobeS5L1YUJ5g24M9iYgoKhRbL14KHoqXikULghR_ibe2r-9fODPZ5qW2qPUShpmd2fl62dnN7j7HGc0gT2AgKltuh-ctmcMDhuG8JVQZFBJreLpn-85df3Ja3p5RM0PDPxu7lhYX8vFi6dhzJf8TVcBBXPGU7AkiWwsFBMAQX3hChOH5TzFmScBCziIPAe0zI1sIGckixRKfaclMyhKN2xlCnyWKGZdpTWwTTBsCfBZFSAIMUBPgBUAgVyRZqAlwqQ9oKZghySBfV1wJMyFLDLLomACOElCNlEUpCdQo_Jg2BlXV_IA00ayUD0sIWRggBlSN4oYhCp-hsVaH9b5c1NGAiQm5IWZhOqBQ99YvCdOVPYBsMCu0HQQisyEdfMTo6Bj5CukmIDVjkNtcR-GDFVQSwdGDqPQEcYDSMZTyJIMfmJFSm9r4ADVAUu10MDilMNSeJRU0xUxDREPiAqpPwVMII3tIATbY0sa1ShSDXKZSw2MmsW6FhEIrk4O00NZc0MFoIqUsrPIsxAxDDHraCtSUBBBd8K1NlARJoJ6OLSaU8BM_6pkxq6XVCZRLxqTCmplxZVtZXWJypE8pKhv5UGPqn4PC3jCLKNUh7U_Wc2P0xmsSfCUODe_VbaX2NSaaY7XrNso-Tqf_j1QUwviGKgrsYLzuYBwziG5HtjXM4Tvb7xdLcw8eYxsYQ_GWh1MclwsbKz72oz9eZDCYvcBcRwxm_x7nUMsPZkcCJg8yGHzEV54IZGBnH1h4QnPuedXhX6vnaWfUGnHrTybQicVumXXvNYrrqXPOWTsrHgmrV9x5Z2hp7oKT9j5s9p6vtnqrW3vP1vafrO8uv-htvOytf9_dWN7ZXtn_-nH_8-bel3d7W692P73vr7zuv93urf3Y-bZRwf3Vp_2VNxed6TSZiidb9m9fWvMebhjLSoPbLYIyg2rC04Vv2oHbVkYHWacQLs9cU5aFEEVR6oADjWfKZO1OO8-DAOuNS85w92G3c9kZCUop8lJmAhJFFh5IUu1OKQrN8aZD17_ijFi7Z-1rfX72t9hd_XuTa84ZhKuF2evO8MKjxc4NmKos5Dcp4L8AB3bgCQ |
| linkProvider | Directory of Open Access Journals |
| openUrl | ctx_ver=Z39.88-2004&ctx_enc=info%3Aofi%2Fenc%3AUTF-8&rfr_id=info%3Asid%2Fsummon.serialssolutions.com&rft_val_fmt=info%3Aofi%2Ffmt%3Akev%3Amtx%3Ajournal&rft.genre=article&rft.atitle=%E7%A2%B1%E7%86%94-%E7%94%B5%E6%84%9F%E8%80%A6%E5%90%88%E7%AD%89%E7%A6%BB%E5%AD%90%E4%BD%93%E8%B4%A8%E8%B0%B1%E6%B3%95%E6%B5%8B%E5%AE%9A%E9%93%8C%E9%92%BD%E7%9F%BF%E4%B8%AD%E9%93%8C%E9%92%BD%E9%94%82%E9%93%8D&rft.jtitle=%E7%9F%BF%E4%BA%A7%E7%BB%BC%E5%90%88%E5%88%A9%E7%94%A8&rft.au=%E6%9D%8E%E6%8C%AF&rft.au=%E9%92%9F%E8%8E%85%E6%B9%98&rft.au=%E5%B4%94%E6%89%BF%E6%B4%8B&rft.au=%E6%9D%8E%E5%BF%97%E4%BC%9F&rft.date=2024&rft.pub=%E6%B2%B3%E5%8D%97%E7%9C%81%E5%B2%A9%E7%9F%B3%E7%9F%BF%E7%89%A9%E6%B5%8B%E8%AF%95%E4%B8%AD%E5%BF%83%E8%87%AA%E7%84%B6%E8%B5%84%E6%BA%90%E9%83%A8%E8%B4%B5%E9%87%91%E5%B1%9E%E5%88%86%E6%9E%90%E4%B8%8E%E5%8B%98%E6%9F%A5%E6%8A%80%E6%9C%AF%E9%87%8D%E7%82%B9%E5%AE%9E%E9%AA%8C%E5%AE%A4%2C%E6%B2%B3%E5%8D%97+%E9%83%91%E5%B7%9E+450012%25%E5%8D%8E%E5%8C%97%E6%B0%B4%E5%88%A9%E6%B0%B4%E7%94%B5%E5%A4%A7%E5%AD%A6%2C%E6%B2%B3%E5%8D%97+%E9%83%91%E5%B7%9E+450012&rft.issn=1000-6532&rft.volume=45&rft.issue=3&rft.spage=200&rft.epage=205&rft_id=info:doi/10.3969%2Fj.issn.1000-6532.2024.03.031&rft.externalDocID=kczhly202403031 |
| thumbnail_s | http://utb.summon.serialssolutions.com/2.0.0/image/custom?url=http%3A%2F%2Fwww.wanfangdata.com.cn%2Fimages%2FPeriodicalImages%2Fkczhly%2Fkczhly.jpg |