羟基磷灰石纳米棒的水热制备及其晶体生长机理研究

O611; 以无水CaCl2和(NH4)2 HPO4为原料,尿素为均相沉淀剂,十六烷基三甲基溴化铵(CTAB)为模板剂,利用水热法制备了羟基磷灰石(HA)纳米棒.采用X射线衍射仪(XRD)、扫描电镜(SEM)和透射电镜(TEM)对产物的物相组成、微观形貌进行了表征.结果 表明:通过改变反应温度和时间,可实现HA纳米形貌的可控微调.在120℃水热反应12h可以制备出单晶密排六方结构HA纳米棒,其长约为0.5～1.0 μm,直径约为15～30 nm.并从晶体结构的角度详细研究了CTAB在合成纳米棒结构中所起的作用,并通过实验进行了验证....

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Published in材料工程 Vol. 48; no. 1; pp. 136 - 143
Main Authors 焦华, 赵康, 石蕊, 马利宁, 卞铁荣, 汤玉斐
Format Journal Article
LanguageChinese
Published 西安理工大学,西安,710048 20.01.2020
Subjects
水热法
纳米棒
羟基磷灰石
生长机理
Online AccessGet full text
ISSN1001-4381
DOI10.11868/j.issn.1001-4381.2018.001206

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Abstract O611; 以无水CaCl2和(NH4)2 HPO4为原料,尿素为均相沉淀剂,十六烷基三甲基溴化铵(CTAB)为模板剂,利用水热法制备了羟基磷灰石(HA)纳米棒.采用X射线衍射仪(XRD)、扫描电镜(SEM)和透射电镜(TEM)对产物的物相组成、微观形貌进行了表征.结果 表明:通过改变反应温度和时间,可实现HA纳米形貌的可控微调.在120℃水热反应12h可以制备出单晶密排六方结构HA纳米棒,其长约为0.5～1.0 μm,直径约为15～30 nm.并从晶体结构的角度详细研究了CTAB在合成纳米棒结构中所起的作用,并通过实验进行了验证.
AbstractList O611; 以无水CaCl2和(NH4)2 HPO4为原料,尿素为均相沉淀剂,十六烷基三甲基溴化铵(CTAB)为模板剂,利用水热法制备了羟基磷灰石(HA)纳米棒.采用X射线衍射仪(XRD)、扫描电镜(SEM)和透射电镜(TEM)对产物的物相组成、微观形貌进行了表征.结果 表明:通过改变反应温度和时间,可实现HA纳米形貌的可控微调.在120℃水热反应12h可以制备出单晶密排六方结构HA纳米棒,其长约为0.5～1.0 μm,直径约为15～30 nm.并从晶体结构的角度详细研究了CTAB在合成纳米棒结构中所起的作用,并通过实验进行了验证.
Author 石蕊
马利宁
赵康
卞铁荣
焦华
汤玉斐
AuthorAffiliation 西安理工大学,西安,710048
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MA Li-ning
TANG Yu-fei
SHI Rui
ZHAO Kang
BIAN Tie-rong
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Keywords 水热法
纳米棒
羟基磷灰石
生长机理
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Snippet O611; 以无水CaCl2和(NH4)2 HPO4为原料,尿素为均相沉淀剂,十六烷基三甲基溴化铵(CTAB)为模板剂,利用水热法制备了羟基磷灰石(HA)纳米棒.采用X射线衍射仪(XRD)、扫描电...
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StartPage 136
Title 羟基磷灰石纳米棒的水热制备及其晶体生长机理研究
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