GC-TCD法同时检测加热不燃烧卷烟烟草材料中的水分、1,2-丙二醇、烟碱和丙三醇

TS411.1; 为准确检测加热不燃烧卷烟烟草材料中的主要成分,以正丁醇和1,3-丁二醇为内标,以甲醇为溶剂振荡萃取,建立了同时检测加热不燃烧卷烟烟草材料中水分、1,2-丙二醇、烟碱和丙三醇含量(质量分数)的气相色谱-热导检测器(GC-TCD)方法,并采用该方法测定了6个加热不燃烧卷烟烟草材料样品.结果表明:①方法的回收率为95.18％～100.80％,相对标准偏差(RSD)为0.56％～1.27％,4种目标物的检出限为0.10～1.02 mg/g.②所测样品中水分、1,2-丙二醇、烟碱和丙三醇的含量分别为90.27～119.63、0.33～2.41、14.54～15.14和130.93～14...

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Published in烟草科技 Vol. 53; no. 5; pp. 41 - 46
Main Authors 肯生叶, 温光和, 杨雪燕, 田飞宇, 杨屹, 李峰, 饶国华, 段勤
Format Journal Article
LanguageChinese
Published 云南养瑞科技集团有限公司,昆明市经开区春漫大道80号,650500%广东中烟工业有限责任公司技术中心,广州市荔湾区东沙环翠南路88号,510385 01.05.2020
Subjects
丙三醇
1,2-丙二醇
烟碱
气相色谱-热导检测器(GC-TCD)
加热不燃烧卷烟
水分
Online AccessGet full text
ISSN1002-0861
DOI10.16135/j.issn1002-0861.2019.0267

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Abstract TS411.1; 为准确检测加热不燃烧卷烟烟草材料中的主要成分,以正丁醇和1,3-丁二醇为内标,以甲醇为溶剂振荡萃取,建立了同时检测加热不燃烧卷烟烟草材料中水分、1,2-丙二醇、烟碱和丙三醇含量(质量分数)的气相色谱-热导检测器(GC-TCD)方法,并采用该方法测定了6个加热不燃烧卷烟烟草材料样品.结果表明:①方法的回收率为95.18％～100.80％,相对标准偏差(RSD)为0.56％～1.27％,4种目标物的检出限为0.10～1.02 mg/g.②所测样品中水分、1,2-丙二醇、烟碱和丙三醇的含量分别为90.27～119.63、0.33～2.41、14.54～15.14和130.93～143.83 mg/g.该方法简单、灵敏、准确,适用于加热不燃烧卷烟烟草材料中4种主要成分的同时测定.
AbstractList TS411.1; 为准确检测加热不燃烧卷烟烟草材料中的主要成分,以正丁醇和1,3-丁二醇为内标,以甲醇为溶剂振荡萃取,建立了同时检测加热不燃烧卷烟烟草材料中水分、1,2-丙二醇、烟碱和丙三醇含量(质量分数)的气相色谱-热导检测器(GC-TCD)方法,并采用该方法测定了6个加热不燃烧卷烟烟草材料样品.结果表明:①方法的回收率为95.18％～100.80％,相对标准偏差(RSD)为0.56％～1.27％,4种目标物的检出限为0.10～1.02 mg/g.②所测样品中水分、1,2-丙二醇、烟碱和丙三醇的含量分别为90.27～119.63、0.33～2.41、14.54～15.14和130.93～143.83 mg/g.该方法简单、灵敏、准确,适用于加热不燃烧卷烟烟草材料中4种主要成分的同时测定.
Author 段勤
田飞宇
杨雪燕
肯生叶
温光和
杨屹
饶国华
李峰
AuthorAffiliation 云南养瑞科技集团有限公司,昆明市经开区春漫大道80号,650500%广东中烟工业有限责任公司技术中心,广州市荔湾区东沙环翠南路88号,510385
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Author_FL KEN Shengye
DUAN Qin
LI Feng
RAO Guohua
WEN Guanghe
YANG Xueyan
TIAN Feiyu
YANG Yi
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Keywords 丙三醇
1,2-丙二醇
烟碱
气相色谱-热导检测器(GC-TCD)
加热不燃烧卷烟
水分
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Title GC-TCD法同时检测加热不燃烧卷烟烟草材料中的水分、1,2-丙二醇、烟碱和丙三醇
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