Synthesis and crystal structure of bis{2-bromo-6-(((4-(1-(methoxyimino)ethyl)phenyl)imino)methyl)phenolato-κ2N,O}cobalt(II)–dichloromethane(1/1), C34H32Br2Cl4CoN4O4
Br Cl CoN , monoclinic, 2/ (no. 15), = 30.281(3) Å, = 8.9971(8) Å, = 13.9050(13) Å, = 107.053(5)°, = 4, = 3621.7(6) Å , ) = 0.0648, ) = 0.1629, = 173(2) K.
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| Published in | Zeitschrift für Kristallographie. New crystal structures Vol. 235; no. 1; pp. 59 - 60 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
De Gruyter
01.01.2020
|
| Subjects | |
| Online Access | Get full text |
| ISSN | 1433-7266 2197-4578 |
| DOI | 10.1515/ncrs-2019-0474 |
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| Abstract | Br
Cl
CoN
, monoclinic,
2/
(no. 15),
= 30.281(3) Å,
= 8.9971(8) Å,
= 13.9050(13) Å,
= 107.053(5)°,
= 4,
= 3621.7(6) Å
,
) = 0.0648,
) = 0.1629,
= 173(2) K. |
|---|---|
| AbstractList | C34H32Br2Cl4CoN4O4, monoclinic, C2/c (no. 15), a = 30.281(3) Å, b = 8.9971(8) Å, c = 13.9050(13) Å, β = 107.053(5)°, Z = 4, V = 3621.7(6) Å3, Rgt(F) = 0.0648, wRref(F2) = 0.1629, T = 173(2) K. Br Cl CoN , monoclinic, 2/ (no. 15), = 30.281(3) Å, = 8.9971(8) Å, = 13.9050(13) Å, = 107.053(5)°, = 4, = 3621.7(6) Å , ) = 0.0648, ) = 0.1629, = 173(2) K. |
| Author | Fu, Tao Zhao, Ji-Xing Wei, Ping Zhao, Li Li, Qing-Lin Ma, Jin-Xia |
| Author_xml | – sequence: 1 givenname: Tao surname: Fu fullname: Fu, Tao organization: Lanzhou Jiaotong University, School of Chemical and Biological Engineering, Lanzhou 730070, P.R. China – sequence: 2 givenname: Jin-Xia surname: Ma fullname: Ma, Jin-Xia organization: Lanzhou Jiaotong University, School of Chemical and Biological Engineering, Lanzhou 730070, P.R. China – sequence: 3 givenname: Ping surname: Wei fullname: Wei, Ping organization: Lanzhou Jiaotong University, School of Chemical and Biological Engineering, Lanzhou 730070, P.R. China – sequence: 4 givenname: Qing-Lin surname: Li fullname: Li, Qing-Lin organization: Lanzhou Jiaotong University, School of Chemical and Biological Engineering, Lanzhou 730070, P.R. China – sequence: 5 givenname: Ji-Xing surname: Zhao fullname: Zhao, Ji-Xing organization: Shihezi University, Analysis and Testing Center, Xinjiang 832003, P.R. China – sequence: 6 givenname: Li orcidid: 0000-0002-9898-9552 surname: Zhao fullname: Zhao, Li email: zhaoli_72@163.com organization: School of Chemical and Biological Engineering, Lanzhou Jiaotong University, Lanzhou 730070, P.R. China |
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| References | Zhao, L.; An, Q. Q.; Zhao, J. X.; Li, P. P.; Wang, F. (j_ncrs-2019-0474_ref_004) 2017; 232 Sun, Y. X.; Lu, R. E.; Li, X. R.; Zhao, Y. Y.; Li, C. Y. (j_ncrs-2019-0474_ref_006) 2015; 31 Ma, J. X.; Li, Q. L.; Li, P. P.; Zhao, J. X.; Zhao, L. (j_ncrs-2019-0474_ref_007) 2018; 233 Sun, Y. X.; Zhao, Y. Y.; Li, C. Y.; Yu, B.; Guo, J. Q.; Li, J. (j_ncrs-2019-0474_ref_005) 2016; 32 Sheldrick, G. M. (j_ncrs-2019-0474_ref_002) 2008; A64 Zhao, J. X.; Zhao, L.; Li, P. P.; Wang, F.; An, Q. Q. (j_ncrs-2019-0474_ref_003) 2017; 232 Li, P. P.; Zhao, L.; Zhao, J. X.; Zhu, Z. B.; Wang, F.; An, Q. Q. (j_ncrs-2019-0474_ref_009) 2017; 232 Ma, J. X.; Li, Q. L.; Li, P. P.; Zhao, J. X.; Zhao, L. (j_ncrs-2019-0474_ref_008) 2018; 233 |
| References_xml | – volume: 32 start-page: 913 year: 2016 end-page: 920 ident: j_ncrs-2019-0474_ref_005 article-title: Supramolecular cobalt(II) and copper(II) complexes with Schiff base ligand: Syntheses, characterizations and crystal structures publication-title: Chin. J. Inorg. Chem – volume: 233 start-page: 789 year: 2018 end-page: 791 ident: j_ncrs-2019-0474_ref_007 article-title: Synthesis and crystal structure of bis{((E)-((4-((E)-1-(methoxyimino) ethyl)phenyl)imino)methyl)-2-naphtholato-κ2N,O}nickel(II), C40H34N4NiO4 publication-title: Z. Kristallogr. NCS – volume: A64 start-page: 112 year: 2008 end-page: 122 ident: j_ncrs-2019-0474_ref_002 article-title: A short history of SHELX publication-title: Acta Crystallogr – volume: 31 start-page: 1055 year: 2015 end-page: 1062 ident: j_ncrs-2019-0474_ref_006 article-title: A Schiff base ligand containing oxime group and its Cu(II) complex: syntheses and supramolecular structures publication-title: Chin. J. Inorg. Chem – volume: 232 start-page: 595 year: 2017 end-page: 597 ident: j_ncrs-2019-0474_ref_004 article-title: Crystal structure of bis(2-((E)-((4-((E)-1-(ethoxyimino)ethyl) phenyl)imino)methyl)-5-methoxyphenolato-κ2O,N)copper(II), C36H38CuN4O6 publication-title: Z. Kristallogr. NCS – volume: 233 start-page: 767 year: 2018 end-page: 769 ident: j_ncrs-2019-0474_ref_008 article-title: Crystal structure of bis{5-methoxy-2-((E)-((4-((E)-1-(methoxyimino) ethyl)phenyl)imino)methyl)phenolato-κ2N,O}nickel(II), C34H34N4NiO6 publication-title: Z. Kristallogr. NCS – volume: 232 start-page: 731 year: 2017 end-page: 732 ident: j_ncrs-2019-0474_ref_003 article-title: Crystal structure of (E)-1-(4-(((E)-5-bromo-2-hydroxybenzylidene)amino) phenyl)ethan-1-one O-methyl oxime, C16H15BrN2O2 publication-title: Z. Kristallogr. NCS – volume: 232 start-page: 889 year: 2017 end-page: 890 ident: j_ncrs-2019-0474_ref_009 article-title: Synthesis and crystal structure of bis{1-(((4-(1-(hydroxyimino)ethyl)phenyl) imino)methyl)naphthalen-2-olato-κ2O,N}copper(II), C38H30CuN4O4 publication-title: Z. Kristallogr. NCS |
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| Snippet | Br
Cl
CoN
, monoclinic,
2/
(no. 15),
= 30.281(3) Å,
= 8.9971(8) Å,
= 13.9050(13) Å,
= 107.053(5)°,
= 4,
= 3621.7(6) Å
,
) = 0.0648,
) = 0.1629,
= 173(2) K. C34H32Br2Cl4CoN4O4, monoclinic, C2/c (no. 15), a = 30.281(3) Å, b = 8.9971(8) Å, c = 13.9050(13) Å, β = 107.053(5)°, Z = 4, V = 3621.7(6) Å3, Rgt(F) = 0.0648,... |
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| Title | Synthesis and crystal structure of bis{2-bromo-6-(((4-(1-(methoxyimino)ethyl)phenyl)imino)methyl)phenolato-κ2N,O}cobalt(II)–dichloromethane(1/1), C34H32Br2Cl4CoN4O4 |
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