Nonisothermal crystallization kinetics of poly(lactide)-effect of plasticizers and nucleating agent

Poly(lactide), a bio‐based aliphatic polyester, is a subject to large research effort. One point of optimization is the acceleration of its crystallization kinetics to promote crystallinity under nonisothermal polymer processing conditions by means of compounding with nucleating agents and plasticiz...

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Published inPolymer engineering and science Vol. 53; no. 5; pp. 1085 - 1098
Main Authors Courgneau, Cécile, Ducruet, Violette, Avérous, Luc, Grenet, Jean, Domenek, Sandra
Format Journal Article
LanguageEnglish
Published Hoboken Wiley Subscription Services, Inc., A Wiley Company 01.05.2013
Wiley
Society of Plastics Engineers, Inc
Blackwell Publishing Ltd
Wiley-Blackwell
Subjects
Acceleration
Agricultural sciences
Aliphatic compounds
Applied sciences
Blends
Chemical properties
Chemical reaction, Rate of
Citrates
Crystallization
Effects
Exact sciences and technology
Forms of application and semi-finished materials
Identification and classification
Kinetics
Lactic acid
Life Sciences
Molecular weight
Nucleation
Optimization
Plasticizers
Polyester resins
Polyethylene glycol
Polymer industry, paints, wood
Polymer processing
Properties
Talcs
Technology of polymers
Thermal properties
France
Heat treatment
Talc
Optically active polymer
Ester polymer
Citrate
Crystallinity
Experimental study
Modeling
Optimization
Property formulation relationship
Ethylene oxide polymer
Kinetic model
Additive
Lactic acid polymer
Cyclic ether polymer
Plasticizer
Aliphatic polymer
Non isothermal condition
Kinetics
Activation energy
Nucleating agent
ISOTHERMAL CRYSTALLIZATION
STEREOCOMPLEX CRYSTALLITES
BEHAVIOR
POLY(L-LACTIC ACID)
TRIPHENYL PHOSPHATE
POLYMER CRYSTALLIZATION
POLY(PROPYLENE GLYCOL)
MECHANICAL-PROPERTIES
PHASE-CHANGE
THERMAL-ANALYSIS
Online AccessGet full text
ISSN0032-3888
1548-2634
DOI10.1002/pen.23357

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Abstract Poly(lactide), a bio‐based aliphatic polyester, is a subject to large research effort. One point of optimization is the acceleration of its crystallization kinetics to promote crystallinity under nonisothermal polymer processing conditions by means of compounding with nucleating agents and plasticizers. The nonisothermal crystallization kinetics of neat and formulated poly(L,D‐lactide) (PDLLA) from the melt with talc and polyethylene glycol (PEG) or acetyl tributyl citrate (ATBC) were studied with the help of the Avrami–Jeziorny and Liu–Mo analysis. Talc showed to be a moderately efficient nucleating agent, as it causes only small increase of crystallization kinetics and shows no effect on the crystallization activation energy. A synergistic effect with plasticizers was observed, expanding the crystallization window significantly. PEG was found to be a more efficient plasticizer than ATBC but causes large decrease in the molecular weight average of PDLLA upon thermal treatment. The talc/ATBC system is efficient starting with an ATBC concentration of 9 wt%. The acceleration observed was a crystallization half‐time decrease of 30% compared to neat PLA and reaching maximum crystallization enthalpies even at cooling rate of 25°C min−1. The ATBC/talc system can be recommended as an efficient system for acceleration of nonisothermal crystallization kinetics of PDLLA. POLYM. ENG. SCI., 2013. © 2012 Society of Plastics Engineers
AbstractList Poly(lactide), a bio-based aliphatic polyester, is a subject to large research effort. One point of optimization is the acceleration of its crystallization kinetics to promote crystallinity under nonisothermal polymer processing conditions by means of compounding with nucleating agents and plasticizers. The nonisothermal crystallization kinetics of neat and formulated poly(^sub l,d^-lactide) (PDLLA) from the melt with talc and polyethylene glycol (PEG) or acetyl tributyl citrate (ATBC) were studied with the help of the Avrami-Jeziorny and Liu-Mo analysis. Talc showed to be a moderately efficient nucleating agent, as it causes only small increase of crystallization kinetics and shows no effect on the crystallization activation energy. A synergistic effect with plasticizers was observed, expanding the crystallization window significantly. PEG was found to be a more efficient plasticizer than ATBC but causes large decrease in the molecular weight average of PDLLA upon thermal treatment. The talc/ATBC system is efficient starting with an ATBC concentration of 9 wt%. The acceleration observed was a crystallization half-time decrease of 30% compared to neat PLA and reaching maximum crystallization enthalpies even at cooling rate of 25°C min^sup -1^. The ATBC/talc system can be recommended as an efficient system for acceleration of nonisothermal crystallization kinetics of PDLLA. [PUBLICATION ABSTRACT]
Poly(lactide), a bio-based aliphatic polyester, is a subject to large research effort. One point of optimization is the acceleration of its crystallization kinetics to promote crystallinity under nonisothermal polymer processing conditions by means of compounding with nucleating agents and plasticizers. The nonisothermal crystallization kinetics of neat and formulated poly( sigma ub l,d approximately lactide) (PDLLA) from the melt with talc and polyethylene glycol (PEG) or acetyl tributyl citrate (ATBC) were studied with the help of the Avrami-Jeziorny and Liu-Mo analysis. Talc showed to be a moderately efficient nucleating agent, as it causes only small increase of crystallization kinetics and shows no effect on the crystallization activation energy. A synergistic effect with plasticizers was observed, expanding the crystallization window significantly. PEG was found to be a more efficient plasticizer than ATBC but causes large decrease in the molecular weight average of PDLLA upon thermal treatment. The talc/ATBC system is efficient starting with an ATBC concentration of 9 wt%. The acceleration observed was a crystallization half-time decrease of 30% compared to neat PLA and reaching maximum crystallization enthalpies even at cooling rate of 25 degree C min sigma up -1 greater than or equal to The ATBC/talc system can be recommended as an efficient system for acceleration of nonisothermal crystallization kinetics of PDLLA. [PUBLICATIONABSTRACT]
Poly(lactide), a bio‐based aliphatic polyester, is a subject to large research effort. One point of optimization is the acceleration of its crystallization kinetics to promote crystallinity under nonisothermal polymer processing conditions by means of compounding with nucleating agents and plasticizers. The nonisothermal crystallization kinetics of neat and formulated poly(L,D‐lactide) (PDLLA) from the melt with talc and polyethylene glycol (PEG) or acetyl tributyl citrate (ATBC) were studied with the help of the Avrami–Jeziorny and Liu–Mo analysis. Talc showed to be a moderately efficient nucleating agent, as it causes only small increase of crystallization kinetics and shows no effect on the crystallization activation energy. A synergistic effect with plasticizers was observed, expanding the crystallization window significantly. PEG was found to be a more efficient plasticizer than ATBC but causes large decrease in the molecular weight average of PDLLA upon thermal treatment. The talc/ATBC system is efficient starting with an ATBC concentration of 9 wt%. The acceleration observed was a crystallization half‐time decrease of 30% compared to neat PLA and reaching maximum crystallization enthalpies even at cooling rate of 25°C min−1. The ATBC/talc system can be recommended as an efficient system for acceleration of nonisothermal crystallization kinetics of PDLLA. POLYM. ENG. SCI., 2013. © 2012 Society of Plastics Engineers
Poly(lactide), a bio-based aliphatic polyester, is a subject to large research effort. One point of optimization is the acceleration of its crystallization kinetics to promote crystallinity under nonisothermal polymer processing conditions by means of compounding with nucleating agents and plasticizers. The nonisothermal crystallization kinetics of neat and formulated poly(L,D-lactide) (PDLLA) from the melt with talc and polyethylene glycol (PEG) or acetyl tributyl citrate (ATBC) were studied with the help of the Avrami--Jeziorny and Liu-Mo analysis. Talc showed to be a moderately efficient nucleating agent, as it causes only small increase of crystallization kinetics and shows no effect on the crystallization activation energy. A synergistic effect with plasticizers was observed, expanding the crystallization window significantly. PEG was found to be a more efficient plasticizer than ATBC but causes large decrease in the molecular weight average of PDLLA upon thermal treatment. The talc/ATBC system is efficient starting with an ATBC concentration of 9 wt%. The acceleration observed was a crystallization halftime decrease of 30% compared to neat PLA and reaching maximum crystallization enthalpies even at cooling rate of 25°C [min.sup.-1]. The ATBC/talc system can be recommended as an efficient system for acceleration of nonisothermal crystallization kinetics of PDLLA. POLYM. ENG. SCI., 53: 1085-1098, 2013. © 2012 Society of Plastics Engineers
Poly(lactide), a bio-based aliphatic polyester, is a subject to large research effort. One point of optimization is the acceleration of its crystallization kinetics to promote crystallinity under nonisothermal polymer processing conditions by means of compounding with nucleating agents and plasticizers. The nonisothermal crystallization kinetics of neat and formulated poly(L,D-lactide) (PDLLA) from the melt with talc and polyethylene glycol (PEG) or acetyl tributyl citrate (ATBC) were studied with the help of the AvramiJeziorny and LiuMo analysis. Talc showed to be a moderately efficient nucleating agent, as it causes only small increase of crystallization kinetics and shows no effect on the crystallization activation energy. A synergistic effect with plasticizers was observed, expanding the crystallization window significantly. PEG was found to be a more efficient plasticizer than ATBC but causes large decrease in the molecular weight average of PDLLA upon thermal treatment. The talc/ATBC system is efficient starting with an ATBC concentration of 9 wt%. The acceleration observed was a crystallization half-time decrease of 30% compared to neat PLA and reaching maximum crystallization enthalpies even at cooling rate of 25 degrees C min1. The ATBC/talc system can be recommended as an efficient system for acceleration of nonisothermal crystallization kinetics of PDLLA. POLYM. ENG. SCI., 2013. (c) 2012 Society of Plastics Engineers
Poly(lactide), a bio‐based aliphatic polyester, is a subject to large research effort. One point of optimization is the acceleration of its crystallization kinetics to promote crystallinity under nonisothermal polymer processing conditions by means of compounding with nucleating agents and plasticizers. The nonisothermal crystallization kinetics of neat and formulated poly( L,D ‐lactide) (PDLLA) from the melt with talc and polyethylene glycol (PEG) or acetyl tributyl citrate (ATBC) were studied with the help of the Avrami–Jeziorny and Liu–Mo analysis. Talc showed to be a moderately efficient nucleating agent, as it causes only small increase of crystallization kinetics and shows no effect on the crystallization activation energy. A synergistic effect with plasticizers was observed, expanding the crystallization window significantly. PEG was found to be a more efficient plasticizer than ATBC but causes large decrease in the molecular weight average of PDLLA upon thermal treatment. The talc/ATBC system is efficient starting with an ATBC concentration of 9 wt%. The acceleration observed was a crystallization half‐time decrease of 30% compared to neat PLA and reaching maximum crystallization enthalpies even at cooling rate of 25°C min −1 . The ATBC/talc system can be recommended as an efficient system for acceleration of nonisothermal crystallization kinetics of PDLLA. POLYM. ENG. SCI., 2013. © 2012 Society of Plastics Engineers
Audience Academic
Author Courgneau, Cécile
Domenek, Sandra
Ducruet, Violette
Avérous, Luc
Grenet, Jean
Author_xml – sequence: 1
  givenname: Cécile
  surname: Courgneau
  fullname: Courgneau, Cécile
  organization: INRA, UMR 1145 Ingénierie procédés Aliments, 1 avenue des Olympiades, F 91300 Massy, France
– sequence: 2
  givenname: Violette
  surname: Ducruet
  fullname: Ducruet, Violette
  organization: INRA, UMR 1145 Ingénierie procédés Aliments, 1 avenue des Olympiades, F 91300 Massy, France
– sequence: 3
  givenname: Luc
  surname: Avérous
  fullname: Avérous, Luc
  organization: ECPM-LIPHT, EAc (CNRS) 4379, Université de Strasbourg, 25 rue Becquerel, 67087 Strasbourg Cedex 2, France
– sequence: 4
  givenname: Jean
  surname: Grenet
  fullname: Grenet, Jean
  organization: AMME-LECAP International Laboratory, LECAP, EA4528, Institute for Material Research, Université de Rouen, 76801 Saint Etienne du Rouvray, France
– sequence: 5
  givenname: Sandra
  surname: Domenek
  fullname: Domenek, Sandra
  email: sandra.domenek@agroparistech.fr
  organization: AgroParisTech, UMR 1145 Ingénierie procédés Aliments, 1 avenue des Olympiades, F 91300 Massy, France
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ContentType Journal Article
Copyright Copyright © 2012 Society of Plastics Engineers
2014 INIST-CNRS
COPYRIGHT 2013 Society of Plastics Engineers, Inc.
Copyright Blackwell Publishing Ltd. May 2013
Distributed under a Creative Commons Attribution 4.0 International License
Copyright_xml – notice: Copyright © 2012 Society of Plastics Engineers
– notice: 2014 INIST-CNRS
– notice: COPYRIGHT 2013 Society of Plastics Engineers, Inc.
– notice: Copyright Blackwell Publishing Ltd. May 2013
– notice: Distributed under a Creative Commons Attribution 4.0 International License
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IEDL.DBID DR2
ISSN 0032-3888
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IsDoiOpenAccess true
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Issue 5
Keywords Heat treatment
Talc
Optically active polymer
Ester polymer
Citrate
Crystallinity
Experimental study
Modeling
Optimization
Property formulation relationship
Ethylene oxide polymer
Kinetic model
Additive
Lactic acid polymer
Cyclic ether polymer
Plasticizer
Aliphatic polymer
Non isothermal condition
Kinetics
Activation energy
Nucleating agent
ISOTHERMAL CRYSTALLIZATION
STEREOCOMPLEX CRYSTALLITES
BEHAVIOR
POLY(L-LACTIC ACID)
TRIPHENYL PHOSPHATE
POLYMER CRYSTALLIZATION
POLY(PROPYLENE GLYCOL)
MECHANICAL-PROPERTIES
PHASE-CHANGE
THERMAL-ANALYSIS
Language English
License http://onlinelibrary.wiley.com/termsAndConditions#vor
CC BY 4.0
Distributed under a Creative Commons Attribution 4.0 International License: http://creativecommons.org/licenses/by/4.0
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PublicationDate May 2013
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  year: 2013
  text: May 2013
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PublicationTitle Polymer engineering and science
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2007; 466
2010; 59
1941; 9
1995; 36
2008; 108
1956; 57
2008; 107
2009; 112
2009; 113
2008; 33
2011; 19
2001; 42
1995; 20
2011; 522
2003; 90
1940; 8
2010; 118
2002; 86
2010; 117
1971; 12
1969; 7
2009; 364
1997; 18
1996; 62
2008; 110
2003; 44
2010; 31
1997; 66
2000; 21
2004; 45
2009
2006; 7
2005; 41
2003; 36
1978; 19
2000; 153
2005; 46
2006; 234
2006; 86
2006; 44
1999; 39
1997; 37
2002; 23
2006; 47
1998; 70
2001; 39
2007; 43
1996; 46
1998; 31
1939; 7
2007; 45
2007; 48
2010; 50
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Snippet Poly(lactide), a bio‐based aliphatic polyester, is a subject to large research effort. One point of optimization is the acceleration of its crystallization...
Poly(lactide), a bio-based aliphatic polyester, is a subject to large research effort. One point of optimization is the acceleration of its crystallization...
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SourceType Open Access Repository
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Publisher
StartPage 1085
SubjectTerms Acceleration
Agricultural sciences
Aliphatic compounds
Applied sciences
Blends
Chemical properties
Chemical reaction, Rate of
Citrates
Crystallization
Effects
Exact sciences and technology
Forms of application and semi-finished materials
Identification and classification
Kinetics
Lactic acid
Life Sciences
Molecular weight
Nucleation
Optimization
Plasticizers
Polyester resins
Polyethylene glycol
Polymer industry, paints, wood
Polymer processing
Properties
Talcs
Technology of polymers
Thermal properties
Title Nonisothermal crystallization kinetics of poly(lactide)-effect of plasticizers and nucleating agent
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