微切助互作技术提取橘皮香精油研究
目的建立应用微切助互作技术从橘皮中高效提取香精油的方法。方法以邵阳当地蜜橘为研究对象,硫酸钾和β-环糊精作为助剂,通过微切助互作技术处理,并采用单因素试验和正交试验作为实验方法,以柑橘皮中香精油的提取率为主要考察指标,对研磨时间、球磨机转速、球磨珠粒数和助剂添加量等4个因素进行研究。结果在助剂添加量为0.2 g,研磨时间为10 min,球磨珠粒数为5粒,球磨机转速为9 r/s条件下所得的香精油提取率最高,可达1.72%。各因素对提取率的影响次序为：助剂添加量〉研磨时间〉球磨机转速〉球磨珠粒数,比传统水蒸汽蒸馏组提取率高0.53%,比不含有β-环糊精助剂的超微粉碎组高0.16%,比未添加硫酸钾和...
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| Published in | 食品安全质量检测学报 Vol. 7; no. 10; pp. 4045 - 4049 |
|---|---|
| Main Author | |
| Format | Journal Article |
| Language | Chinese |
| Published |
邵阳学院生物与化学工程系，邵阳 422000
2016
湖南省果蔬清洁加工工程技术研究中心，邵阳 422000 大连赛姆生物工程技术有限公司博士后工作站，大连 116620 湖南省果蔬清洁加工工程技术研究中心，邵阳 422000%邵阳学院生物与化学工程系，邵阳 422000 教育部动物性食品安全保障技术工程研究中心，大连理工大学生命科学与技术学院，大连 116024 教育部动物性食品安全保障技术工程研究中心，大连理工大学生命科学与技术学院，大连 116024%大连赛姆生物工程技术有限公司博士后工作站，大连 116620 |
| Subjects | |
| Online Access | Get full text |
| ISSN | 2095-0381 |
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| Abstract | 目的建立应用微切助互作技术从橘皮中高效提取香精油的方法。方法以邵阳当地蜜橘为研究对象,硫酸钾和β-环糊精作为助剂,通过微切助互作技术处理,并采用单因素试验和正交试验作为实验方法,以柑橘皮中香精油的提取率为主要考察指标,对研磨时间、球磨机转速、球磨珠粒数和助剂添加量等4个因素进行研究。结果在助剂添加量为0.2 g,研磨时间为10 min,球磨珠粒数为5粒,球磨机转速为9 r/s条件下所得的香精油提取率最高,可达1.72%。各因素对提取率的影响次序为：助剂添加量〉研磨时间〉球磨机转速〉球磨珠粒数,比传统水蒸汽蒸馏组提取率高0.53%,比不含有β-环糊精助剂的超微粉碎组高0.16%,比未添加硫酸钾和β-环糊精助剂超微粉碎组高0.29%,比未进行超微粉碎的粗粉组高0.4%。结论与传统热回流方法比较,该方法高效安全,适合提取橘皮中的香精油。 |
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| AbstractList | 目的建立应用微切助互作技术从橘皮中高效提取香精油的方法。方法以邵阳当地蜜橘为研究对象,硫酸钾和β-环糊精作为助剂,通过微切助互作技术处理,并采用单因素试验和正交试验作为实验方法,以柑橘皮中香精油的提取率为主要考察指标,对研磨时间、球磨机转速、球磨珠粒数和助剂添加量等4个因素进行研究。结果在助剂添加量为0.2 g,研磨时间为10 min,球磨珠粒数为5粒,球磨机转速为9 r/s条件下所得的香精油提取率最高,可达1.72%。各因素对提取率的影响次序为：助剂添加量〉研磨时间〉球磨机转速〉球磨珠粒数,比传统水蒸汽蒸馏组提取率高0.53%,比不含有β-环糊精助剂的超微粉碎组高0.16%,比未添加硫酸钾和β-环糊精助剂超微粉碎组高0.29%,比未进行超微粉碎的粗粉组高0.4%。结论与传统热回流方法比较,该方法高效安全,适合提取橘皮中的香精油。 目的：建立应用微切助互作技术从橘皮中高效提取香精油的方法。方法以邵阳当地蜜橘为研究对象,硫酸钾和β-环糊精作为助剂,通过微切助互作技术处理,并采用单因素试验和正交试验作为实验方法,以柑橘皮中香精油的提取率为主要考察指标,对研磨时间、球磨机转速、球磨珠粒数和助剂添加量等4个因素进行研究。结果在助剂添加量为0.2 g,研磨时间为10 min,球磨珠粒数为5粒,球磨机转速为9 r/s条件下所得的香精油提取率最高,可达1.72%。各因素对提取率的影响次序为：助剂添加量>研磨时间>球磨机转速>球磨珠粒数,比传统水蒸汽蒸馏组提取率高0.53%,比不含有β-环糊精助剂的超微粉碎组高0.16%,比未添加硫酸钾和β-环糊精助剂超微粉碎组高0.29%,比未进行超微粉碎的粗粉组高0.4%。结论与传统热回流方法比较,该方法高效安全,适合提取橘皮中的香精油。 |
| Abstract_FL | ObjectiveTo establish a method for the extraction of essential oil from citrus peel by press-shear assisted interaction technology. MethodsWith Shaoyang local tangerine as materials, K2SO4 andβ-cyclodextrin as additives, citrus peel essential oil was extracted by pressure-shear induced chemical transitions. With citrus peel essential oil extraction rate as the main examine index, the milling time, rotating speed of mill, milling beads number and amount of additives added were optimized by the single factor and orthogonal experiment.ResultsThe results showed the best extraction condition was as the following: the reagent was 0.2 g, the grinding time was 10 min, the number of milling beads was 5, and the rotating speed of mill was at 9r/s. From the orthogonal experiment, the influence of various factors on the extraction yield order was: additive> polishing time>rotating speed of mill>grinding beads numbers. In optimal conditions, the extraction rate of essential oils was up to 1.72%, 0.53% higher than traditional steam distillation extraction rate, 0.16% higher than theβ-cyclodextrin ultrafine grinding aid group, 0.29% higher than no addition of K2SO4 andβ-cyclodextrin ultrafine grinding aid group and 0.4% than meal group. ConclusionCompared with heat reflux method, press-shear assisted interaction technology can significantly increase the rate of essential oil extraction from citrus peel. |
| Author | 龙艳珍 吴菲菲 赵良忠 尹锦辉 巢玲 徐永平 李化强 |
| AuthorAffiliation | 邵阳学院生物与化学工程系,邵阳422000 湖南省果蔬清洁加工工程技术研究中心,邵阳422000 大连赛姆生物工程技术有限公司博士后工作站,大连116620 教育部动物性食品安全保障技术工程研究中心,大连理工大学生命科学与技术学院,大连116024 |
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| Author_FL | ZHAO Liang-Zhong XU Yong-Ping LONG Yan-Zhen WU Fei-Fei CHAO Ling YIN Jin-Hui LI Hua-Qiang |
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| DocumentTitleAlternate | Extraction method of essential oil by press-shear assisted interaction technology from citrus peel |
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| Keywords | β-环糊精 柑橘皮 香精油 硫酸钾 press-shear assisted interaction technology 微切助互作技术 K2SO4 essential oil citrus peel β-cyclodextrin |
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| Notes | Objective To establish a method for the extraction of essential oil from citrus peel by press-shear assisted interaction technology.Methods With Shaoyang local tangerine as materials,K2SO4 and β-cyclodextrin as additives,citrus peel essential oil was extracted by pressure-shear induced chemical transitions.With citrus peel essential oil extraction rate as the main examine index,the milling time,rotating speed of mill,milling beads number and amount of additives added were optimized by the single factor and orthogonal experiment.Results The results showed the best extraction condition was as the following：the reagent was 0.2 g,the grinding time was 10 min,the number of milling beads was 5,and the rotating speed of mill was at 9r/s.From the orthogonal experiment,the influence of various factors on the extraction yield order was：additive〉 polishing timerotating speed of mil〉lgrinding beads numbers.In optimal conditions,the extraction rate of essential oils was up to 1.72%,0.53%higher than traditional steam disti |
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| PublicationTitle | 食品安全质量检测学报 |
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| PublicationYear | 2016 |
| Publisher | 邵阳学院生物与化学工程系，邵阳 422000 湖南省果蔬清洁加工工程技术研究中心，邵阳 422000 大连赛姆生物工程技术有限公司博士后工作站，大连 116620 湖南省果蔬清洁加工工程技术研究中心，邵阳 422000%邵阳学院生物与化学工程系，邵阳 422000 教育部动物性食品安全保障技术工程研究中心，大连理工大学生命科学与技术学院，大连 116024 教育部动物性食品安全保障技术工程研究中心，大连理工大学生命科学与技术学院，大连 116024%大连赛姆生物工程技术有限公司博士后工作站，大连 116620 |
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| Snippet | 目的建立应用微切助互作技术从橘皮中高效提取香精油的方法。方法以邵阳当地蜜橘为研究对象,硫酸钾和β-环糊精作为助剂,通过微切助互作技术处理,并采用单因素试验和正交试验... 目的：建立应用微切助互作技术从橘皮中高效提取香精油的方法。方法以邵阳当地蜜橘为研究对象,硫酸钾和β-环糊精作为助剂,通过微切助互作技术处理,并采用单因素试验和正交试... |
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| Title | 微切助互作技术提取橘皮香精油研究 |
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