无溶剂合成SAPO-5沸石中表面活性剂对其片状形貌的控制
在表面活性剂如十六烷基三甲基溴化铵（CTAB）的存在下，采用无溶剂法合成出具有片状形貌的SAPO-5沸石晶体。 X射线衍射和扫描电镜结果表明，所合成的样品具有很好的结晶度和可控的片状形貌，在合成过程中， CTAB的添加量对其片状形貌特别是片状的厚度的影响很大。考虑到一维的微孔AFI结构独特，具有特殊片状形貌的SAPO-5晶体有望应用于催化方面。...
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| Published in | 催化学报 Vol. 36; no. 6; pp. 797 - 800 |
|---|---|
| Main Author | |
| Format | Journal Article |
| Language | Chinese |
| Published |
浙江大学化学系浙江省应用化学重点实验室,浙江杭州,310028
2015
|
| Subjects | |
| Online Access | Get full text |
| ISSN | 0253-9837 1872-2067 |
| DOI | 10.1016/S1872-2067(14)60285-0| |
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| Abstract | 在表面活性剂如十六烷基三甲基溴化铵（CTAB）的存在下，采用无溶剂法合成出具有片状形貌的SAPO-5沸石晶体。 X射线衍射和扫描电镜结果表明，所合成的样品具有很好的结晶度和可控的片状形貌，在合成过程中， CTAB的添加量对其片状形貌特别是片状的厚度的影响很大。考虑到一维的微孔AFI结构独特，具有特殊片状形貌的SAPO-5晶体有望应用于催化方面。 |
|---|---|
| AbstractList | 在表面活性剂如十六烷基三甲基溴化铵(CTAB)的存在下，采用无溶剂法合成出具有片状形貌的SAPO-5沸石晶体。 X射线衍射和扫描电镜结果表明，所合成的样品具有很好的结晶度和可控的片状形貌，在合成过程中， CTAB的添加量对其片状形貌特别是片状的厚度的影响很大。考虑到一维的微孔AFI结构独特，具有特殊片状形貌的SAPO-5晶体有望应用于催化方面。 在表面活性剂如十六烷基三甲基溴化铵（CTAB）的存在下，采用无溶剂法合成出具有片状形貌的SAPO-5沸石晶体。 X射线衍射和扫描电镜结果表明，所合成的样品具有很好的结晶度和可控的片状形貌，在合成过程中， CTAB的添加量对其片状形貌特别是片状的厚度的影响很大。考虑到一维的微孔AFI结构独特，具有特殊片状形貌的SAPO-5晶体有望应用于催化方面。 |
| Abstract_FL | SAPO-5 crystals with plate-like morphology were synthesized in the presence of surfactants such as cetyltrimethyl ammonium bromide under solvent-free conditions. X-ray diffraction patterns and scanning electron microscopy images revealed that the samples had high crystallinity and control-lable plate-like morphology. The amount of surfactant added played an important role in controlling the thickness of the zeolite crystals. Considering the unique one-dimensional microporous archi-tecture of AFI, SAPO-5 crystals with unique plate-like morphology are expected to be of great im-portance in catalytic applications. |
| Author | 陈鲜 孟祥举 肖丰收 |
| AuthorAffiliation | 浙江大学化学系浙江省应用化学重点实验室,浙江杭州310028 |
| AuthorAffiliation_xml | – name: 浙江大学化学系浙江省应用化学重点实验室,浙江杭州,310028 |
| Author_FL | Xiangju Meng Feng-shou Xiao Xian Chen |
| Author_FL_xml | – sequence: 1 fullname: Xian Chen – sequence: 2 fullname: Xiangju Meng – sequence: 3 fullname: Feng-shou Xiao |
| Author_xml | – sequence: 1 fullname: 陈鲜 孟祥举 肖丰收 |
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| DOI | 10.1016/S1872-2067(14)60285-0| |
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| DocumentTitleAlternate | Solvent-free synthesis of SAPO-5 zeolite with plate-like morphology in the presence of surfactants |
| DocumentTitle_FL | Solvent-free synthesis of SAPO-5 zeolite with plate-like morphology in the presence of surfactants |
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| Keywords | 表面活性剂 AFI结构 片状形貌 Solvent-free synthesis Plate-like morphology 无溶剂合成 Surfactant AFI structure |
| Language | Chinese |
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| Notes | Xian Chen, Xiangju Meng, Feng-shou Xiao（ Key Lab of Applied Chemistry of Zhejian9 Province, Department of Chemistry, Zhejiang University, Hangzhou 310007, Zhejiang, China） Solvent-free synthesis;AFI structure;Plate-like morphology;Surfactant 21-1195/O6 SAPO-5 crystals with plate-like morphology were synthesized in the presence of surfactants such as cetyltrimethyl ammonium bromide under solvent-free conditions. X-ray diffraction patterns and scanning electron microscopy images revealed that the samples had high crystallinity and control-lable plate-like morphology. The amount of surfactant added played an important role in controlling the thickness of the zeolite crystals. Considering the unique one-dimensional microporous archi-tecture of AFI, SAPO-5 crystals with unique plate-like morphology are expected to be of great im-portance in catalytic applications. |
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| PublicationTitle | 催化学报 |
| PublicationTitleAlternate | Chinese Journal of Catalysis |
| PublicationTitle_FL | Chinese Journal of Catalysis |
| PublicationYear | 2015 |
| Publisher | 浙江大学化学系浙江省应用化学重点实验室,浙江杭州,310028 |
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| Snippet | 在表面活性剂如十六烷基三甲基溴化铵（CTAB）的存在下，采用无溶剂法合成出具有片状形貌的SAPO-5沸石晶体。 X射线衍射和扫描电镜结果表明，所合成的样品具有很好的结晶度和... 在表面活性剂如十六烷基三甲基溴化铵(CTAB)的存在下，采用无溶剂法合成出具有片状形貌的SAPO-5沸石晶体。 X射线衍射和扫描电镜结果表明，所合成的样品具有很好的结晶度和可... |
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| SubjectTerms | AFI结构 无溶剂合成 片状形貌 表面活性剂 |
| Title | 无溶剂合成SAPO-5沸石中表面活性剂对其片状形貌的控制 |
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