顶空气相色谱法测定土壤或底泥中的八种苯系物
O65%X83; 为快速、准确监测环境土壤或底泥中苯系物的含量,建立了一种顶空气相色谱法同时测定土壤或底泥中8种苯系物的方法.采用Nukol毛细管气相色谱柱实现了各组分的良好分离,优化了色谱条件,顶空进样条件.在优化条件下,8种苯系物在13 min内能实现完全分离,在10～500 μg·kg-1浓度范围内组分含量与峰面积呈线性相关,相关系数为0.990 6～0.995 7,检出限为2μg·kg-1,回收率为94％～114％,相对标准偏差为2.4％～5.2％(n=3).结果表明,建立的顶空气相色谱法简单快速,无需有机溶剂,重现性好,回收率高,适合于土壤或底泥中苯系物的测定....
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| Published in | 浙江大学学报（理学版） Vol. 40; no. 3; pp. 319 - 323 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | Chinese |
| Published |
浙江省海洋水产研究所浙江省海水增养殖重点实验室,浙江舟山,316100
2013
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| Subjects | |
| Online Access | Get full text |
| ISSN | 1008-9497 |
| DOI | 10.3785/j.issn.1008-9497.2013.03.016 |
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| Abstract | O65%X83; 为快速、准确监测环境土壤或底泥中苯系物的含量,建立了一种顶空气相色谱法同时测定土壤或底泥中8种苯系物的方法.采用Nukol毛细管气相色谱柱实现了各组分的良好分离,优化了色谱条件,顶空进样条件.在优化条件下,8种苯系物在13 min内能实现完全分离,在10～500 μg·kg-1浓度范围内组分含量与峰面积呈线性相关,相关系数为0.990 6～0.995 7,检出限为2μg·kg-1,回收率为94％～114％,相对标准偏差为2.4％～5.2％(n=3).结果表明,建立的顶空气相色谱法简单快速,无需有机溶剂,重现性好,回收率高,适合于土壤或底泥中苯系物的测定. |
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| AbstractList | O65%X83; 为快速、准确监测环境土壤或底泥中苯系物的含量,建立了一种顶空气相色谱法同时测定土壤或底泥中8种苯系物的方法.采用Nukol毛细管气相色谱柱实现了各组分的良好分离,优化了色谱条件,顶空进样条件.在优化条件下,8种苯系物在13 min内能实现完全分离,在10～500 μg·kg-1浓度范围内组分含量与峰面积呈线性相关,相关系数为0.990 6～0.995 7,检出限为2μg·kg-1,回收率为94％～114％,相对标准偏差为2.4％～5.2％(n=3).结果表明,建立的顶空气相色谱法简单快速,无需有机溶剂,重现性好,回收率高,适合于土壤或底泥中苯系物的测定. |
| Author | 孙秀梅 钟志 金衍健 胡红美 郭远明 |
| AuthorAffiliation | 浙江省海洋水产研究所浙江省海水增养殖重点实验室,浙江舟山,316100 |
| AuthorAffiliation_xml | – name: 浙江省海洋水产研究所浙江省海水增养殖重点实验室,浙江舟山,316100 |
| Author_FL | JIN Yan-jian SUN Xiu-mei GUO Yuan-ming HU Hong-mei ZHONG Zhi |
| Author_FL_xml | – sequence: 1 fullname: HU Hong-mei – sequence: 2 fullname: SUN Xiu-mei – sequence: 3 fullname: GUO Yuan-ming – sequence: 4 fullname: ZHONG Zhi – sequence: 5 fullname: JIN Yan-jian |
| Author_xml | – sequence: 1 fullname: 胡红美 – sequence: 2 fullname: 孙秀梅 – sequence: 3 fullname: 郭远明 – sequence: 4 fullname: 钟志 – sequence: 5 fullname: 金衍健 |
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| Keywords | 顶空气相色谱法 底泥 Nukol毛细管气相色谱柱 苯系物 土壤 |
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| Snippet | O65%X83; 为快速、准确监测环境土壤或底泥中苯系物的含量,建立了一种顶空气相色谱法同时测定土壤或底泥中8种苯系物的方法.采用Nukol毛细管气相色谱柱实现了各组分的良好分... |
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| Title | 顶空气相色谱法测定土壤或底泥中的八种苯系物 |
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