橙汁加工过程对农药炔螨特残留的影响

为弄清橙汁加工过程中农药炔螨特残留的动态,通过田间喷施浓度为5倍于最高推荐剂量的农药溶液以强化炔螨特在甜橙上的残留,然后按照橙汁商业化加工过程进行加工,采用QuEChERS前处理技术结合气相色谱-串联质谱法检测炔螨特的含量,来考察橙汁商业化加工过程对炔螨特残留的影响。结果表明：炔螨特残留主要分布于甜橙果皮中,果肉中炔螨特的残留量不足全果的5%。清洗能除去全果中32.5%的炔螨特残留。初榨果汁、精滤果汁、非浓缩橙汁（NFC橙汁）和浓缩橙汁中的残留量分别为原料果的1.98%、1.95%、1.73%、1.37%,其中NFC橙汁和浓缩橙汁的加工因子分别为0.0173和0.0137,但炔螨特在果渣和精油...

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Bibliographic Details
Published in农业工程学报 Vol. 28; no. 9; pp. 270 - 275
Main Author 李云成 张耀海 陈卫军 赵其阳 单炜力 刘光学 王成秋 焦必宁
Format Journal Article
LanguageChinese
Published 中国农业科学院柑橘研究所/西南大学柑橘研究所,重庆400712%中国农业科学院柑橘研究所/西南大学柑橘研究所,重庆,400712%农业部农药检定所,北京,100125 2012
西南大学食品科学学院,重庆400715
Subjects
农产品
农药
加工
橙汁
残留
炔螨特
农药
炔螨特
农产品
残留
橙汁
加工
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ISSN1002-6819
DOI10.3969/j.issn.1002-6819.2012.09.044

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Summary:为弄清橙汁加工过程中农药炔螨特残留的动态,通过田间喷施浓度为5倍于最高推荐剂量的农药溶液以强化炔螨特在甜橙上的残留,然后按照橙汁商业化加工过程进行加工,采用QuEChERS前处理技术结合气相色谱-串联质谱法检测炔螨特的含量,来考察橙汁商业化加工过程对炔螨特残留的影响。结果表明：炔螨特残留主要分布于甜橙果皮中,果肉中炔螨特的残留量不足全果的5%。清洗能除去全果中32.5%的炔螨特残留。初榨果汁、精滤果汁、非浓缩橙汁（NFC橙汁）和浓缩橙汁中的残留量分别为原料果的1.98%、1.95%、1.73%、1.37%,其中NFC橙汁和浓缩橙汁的加工因子分别为0.0173和0.0137,但炔螨特在果渣和精油中发生富集,加工因子分别为1.2822和18.4947。研究结果为橙汁加工工艺的优化和炔螨特残留的膳食暴露评估提供参考。
Bibliography:11-2047/S
processing; pesticides; agricultural products; propargite; residues; orange juice
The objective of this study was to evaluate the effects of commercial processing techniques on propargite residues in orange juice and its by-products. In order to assess the persistence during juice processing, the field trials were carried out by spraying with the solution of 5-fold the concentration of the maximum recommended dosages. Propargite residues were determined by Gas Chromatography-tandem Mass Spectrometry based on QuEChERS extraction. The results indicated that the propargite was mainly distributed in orange peels, and the residual level in orange pulps was less than 5% compared to the raw materials. Propargite residues could be partially removed by washing, and the reduction was 32.5%. The residual levels in squeezed juice, filtrated juice, NFC juice and concentrated juice were 1.98%, 1.95%, 1.73%, and 1.37% of the raw material, respectively, and the processing factors of NFC juice and concentrated juice w
ISSN:1002-6819
DOI:10.3969/j.issn.1002-6819.2012.09.044