射干异黄酮的NMR波谱研究
为研究中药射干（Belamcanda chinensis）的化学成分，应用多种柱色谱方法对其乙醇提取物进行分离和纯化，并得到了11个异黄酮化合物，通过^1HNMR、^13C NMR及HMBC、HSQC、^1H-^1H COSY、NOESY等波谱手段解析化学结构，发现一个新化合物，命名为异野鸢尾苷,对这些化合物的^3H NMR和^13C NMR进行了完全归属，并探讨了取代基对^1H、^13C化学位移的影响．...
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| Published in | Bopuxue zazhi Vol. 23; no. 4; pp. 443 - 449 |
|---|---|
| Main Author | |
| Format | Journal Article |
| Language | Chinese |
| Published |
烟台大学,药学院,山东,烟台,264005
2006
山东绿叶制药有限公司,山东,烟台,264003%山东绿叶制药有限公司,山东,烟台,264003 |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1000-4556 |
| DOI | 10.3969/j.issn.1000-4556.2006.04.003 |
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| Abstract | 为研究中药射干（Belamcanda chinensis）的化学成分，应用多种柱色谱方法对其乙醇提取物进行分离和纯化，并得到了11个异黄酮化合物，通过^1HNMR、^13C NMR及HMBC、HSQC、^1H-^1H COSY、NOESY等波谱手段解析化学结构，发现一个新化合物，命名为异野鸢尾苷,对这些化合物的^3H NMR和^13C NMR进行了完全归属，并探讨了取代基对^1H、^13C化学位移的影响． |
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| AbstractList | 为研究中药射干（Belamcanda chinensis）的化学成分，应用多种柱色谱方法对其乙醇提取物进行分离和纯化，并得到了11个异黄酮化合物，通过^1HNMR、^13C NMR及HMBC、HSQC、^1H-^1H COSY、NOESY等波谱手段解析化学结构，发现一个新化合物，命名为异野鸢尾苷,对这些化合物的^3H NMR和^13C NMR进行了完全归属，并探讨了取代基对^1H、^13C化学位移的影响． O6; 为研究中药射干(Belamcanda chinensis)的化学成分,应用多种柱色谱方法对其乙醇提取物进行分离和纯化,并得到了11个异黄酮化合物,通过1H NMR、13C NMR及HMBC、HSQC、1H-1 H COSY、NOESY等波谱手段解析化学结构,发现一个新化合物,命名为异野鸢尾苷.对这些化合物的1H NMR和13C NMR进行了完全归属,并探讨了取代基对1H、13C化学位移的影响. |
| Author | 邱鹰昆 徐碧霞 高玉白 刘珂 |
| AuthorAffiliation | 烟台大学药学院,山东烟台264005 山东绿叶制药有限公司,山东烟台264003 |
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| Author_FL | QIU Ying-kun XU Bi-xia GAO Yu-bai LIU Ke |
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| DocumentTitleAlternate | An NMR Study of Isoflavones Extracted from Belamcanda Chinensis |
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| Keywords | 核磁共振 化学位移 异黄酮 射干 异野鸢尾苷 |
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| Publisher | 烟台大学,药学院,山东,烟台,264005 山东绿叶制药有限公司,山东,烟台,264003%山东绿叶制药有限公司,山东,烟台,264003 |
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| Snippet | 为研究中药射干（Belamcanda chinensis）的化学成分，应用多种柱色谱方法对其乙醇提取物进行分离和纯化，并得到了11个异黄酮化合物，通过^1HNMR、^13C NMR... O6; 为研究中药射干(Belamcanda chinensis)的化学成分,应用多种柱色谱方法对其乙醇提取物进行分离和纯化,并得到了11个异黄酮化合物,通过1H NMR、13C NMR及HMBC、HSQC、1H-1 H... |
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| StartPage | 443 |
| SubjectTerms | 化学位移 射干 异野鸢尾苷 异黄酮 核磁共振 |
| Title | 射干异黄酮的NMR波谱研究 |
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