耐高温双马来酰亚胺树脂的固化反应动力学和TTT图
采用动态DSC法对耐高温双马来酰亚胺树脂的固化反应动力学进行研究,根据Kissinger方程和Crane方程,拟合得到树脂的固化动力学参数,并建立树脂的唯象模型。此外,采用恒温DSC法,根据DiBenedetto方程,建立树脂的玻璃化转变温度与固化度之间的函数关系。采用凝胶盘法,获得树脂在不同温度下的凝胶时间,建立凝胶时间和凝胶温度之间的函数关系,最终得到树脂的TTT图。结果表明：根据TTT图确定合适的加压时机,可以有效排除夹杂于预浸料层内层间的气体,从而制备内部质量完好的复合材料。...
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| Published in | 材料工程 Vol. 44; no. 9; pp. 44 - 51 |
|---|---|
| Main Author | |
| Format | Journal Article |
| Language | Chinese |
| Published |
中航复合材料有限责任公司,北京,101300%核工业理化工程研究院,天津,300180%空军驻北京地区军事代表室,北京,101300
2016
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| Subjects | |
| Online Access | Get full text |
| ISSN | 1001-4381 1001-4381 |
| DOI | 10.11868/j.issn.1001-4381.2016.09.007 |
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| Abstract | 采用动态DSC法对耐高温双马来酰亚胺树脂的固化反应动力学进行研究,根据Kissinger方程和Crane方程,拟合得到树脂的固化动力学参数,并建立树脂的唯象模型。此外,采用恒温DSC法,根据DiBenedetto方程,建立树脂的玻璃化转变温度与固化度之间的函数关系。采用凝胶盘法,获得树脂在不同温度下的凝胶时间,建立凝胶时间和凝胶温度之间的函数关系,最终得到树脂的TTT图。结果表明：根据TTT图确定合适的加压时机,可以有效排除夹杂于预浸料层内层间的气体,从而制备内部质量完好的复合材料。 |
|---|---|
| AbstractList | TB332; 采用动态DSC法对耐高温双马来酰亚胺树脂的固化反应动力学进行研究,根据Kissinger方程和Crane方程,拟合得到树脂的固化动力学参数,并建立树脂的唯象模型.此外,采用恒温DSC法,根据DiBenedetto方程,建立树脂的玻璃化转变温度与固化度之间的函数关系.采用凝胶盘法,获得树脂在不同温度下的凝胶时间,建立凝胶时间和凝胶温度之间的函数关系,最终得到树脂的TTT图.结果表明:根据TTT图确定合适的加压时机,可以有效排除夹杂于预浸料层内层间的气体,从而制备内部质量完好的复合材料. 采用动态DSC法对耐高温双马来酰亚胺树脂的固化反应动力学进行研究,根据Kissinger方程和Crane方程,拟合得到树脂的固化动力学参数,并建立树脂的唯象模型。此外,采用恒温DSC法,根据DiBenedetto方程,建立树脂的玻璃化转变温度与固化度之间的函数关系。采用凝胶盘法,获得树脂在不同温度下的凝胶时间,建立凝胶时间和凝胶温度之间的函数关系,最终得到树脂的TTT图。结果表明：根据TTT图确定合适的加压时机,可以有效排除夹杂于预浸料层内层间的气体,从而制备内部质量完好的复合材料。 |
| Author | 李伟东 张金栋 李韶亮 刘刚 钟翔屿 包建文 |
| AuthorAffiliation | 中航复合材料有限责任公司,北京101300 核工业理化工程研究院,天津300180 空军驻北京地区军事代表室,北京101300 |
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| Author_FL | LI Shao-liang ZHANG Jin-dong BAO Jian-wen LIU Gang LI Wei-dong ZHONG Xiang-yu |
| Author_FL_xml | – sequence: 1 fullname: LI Wei-dong – sequence: 2 fullname: ZHANG Jin-dong – sequence: 3 fullname: LI Shao-liang – sequence: 4 fullname: LIU Gang – sequence: 5 fullname: ZHONG Xiang-yu – sequence: 6 fullname: BAO Jian-wen |
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| ClassificationCodes | TB332 |
| ContentType | Journal Article |
| Copyright | Copyright © Wanfang Data Co. Ltd. All Rights Reserved. |
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| DOI | 10.11868/j.issn.1001-4381.2016.09.007 |
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| DocumentTitleAlternate | Curing Kinetics and TTT Diagram of High Temperature Resistance Bismaleimide Resin |
| DocumentTitle_FL | Curing Kinetics and TTT Diagram of High Temperature Resistance Bismaleimide Resin |
| EISSN | 1001-4381 |
| EndPage | 51 |
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| Issue | 9 |
| Keywords | 工艺优化 双马来酰亚胺树脂 TTT diagram process optimization 固化反应动力学 curing kinetics bismaleimide resin TTT图 |
| Language | Chinese |
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| Notes | 11-1800/TB bismaleimide resin; curing kinetics; TTT diagram; process optimization The curing kinetics of high temperature resistance bismaleimide resin was studied by dynamic DSC analysis,and the parameters of the curing reaction were obtained to establish a phenomenological model based on Kissinger and Crane equations.The relationship between glass transition temperature and curing degree was analyzed with isothermal DSC method based on DiBenedetto equation.Moreover,the relationship between gel-time and temperature was investigated by gelation disk.Finally,the time-temperature-transition（TTT）diagram was built to guide the process of the resin.Results show that appropriate pressure timing can be determined according to the TTT diagram.Thus,air in or between layers of prepreg can be eliminated effectively to prepare composites with good internal quality. LI Wei-dong1 , ZHANG Jin-dong2 , LI Shao-liang3 , LIU Gang1 ,ZHONG Xiang-yu1 ,BAO Jian-wen1 （ 1 AVIC Composite Corporation Ltd., Beijing 101300, China ; 2 Resear |
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| PublicationTitle | 材料工程 |
| PublicationTitleAlternate | Journal of Materials Engineering |
| PublicationTitle_FL | Journal of Materials Engineering |
| PublicationYear | 2016 |
| Publisher | 中航复合材料有限责任公司,北京,101300%核工业理化工程研究院,天津,300180%空军驻北京地区军事代表室,北京,101300 |
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| Snippet | 采用动态DSC法对耐高温双马来酰亚胺树脂的固化反应动力学进行研究,根据Kissinger方程和Crane方程,拟合得到树脂的固化动力学参数,并建立树脂的唯象模型。此外,采用恒温DSC... TB332; 采用动态DSC法对耐高温双马来酰亚胺树脂的固化反应动力学进行研究,根据Kissinger方程和Crane方程,拟合得到树脂的固化动力学参数,并建立树脂的唯象模型.此外,采用恒... |
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| SubjectTerms | TTT图 双马来酰亚胺树脂 固化反应动力学 工艺优化 |
| Title | 耐高温双马来酰亚胺树脂的固化反应动力学和TTT图 |
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