电喷雾-傅立叶变换离子回旋共振质谱分析原油中的碱性氮化物
电喷雾电离源（ESI）可选择性地电离石油中的碱性氮化物,与具有超高质量分辨率和质量精度的傅立叶变换离子回旋共振质谱仪（FTICRMS）结合,可直接用于分析原油中的碱性氮化物而不需要预先分离。通过此方法考察了3种原油中碱性氮化物的类型分布和碳数分布,结果表明,原油中主要碱性氮化物为含N1,N2,NO,NS,NO2,NO3等杂原子的碱性氮化物,共检测到约100类不同缩合度的碱性氮化物,各类碱性氮化物的碳数分布范围为15～70。不同基属原油中的碱性氮化物在种类分布和碳数分布上存在一定的差异。...
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| Published in | Fēnxī huàxué Vol. 38; no. 4; pp. 564 - 568 |
|---|---|
| Main Author | |
| Format | Journal Article |
| Language | Chinese |
| Published |
中国石化股份有限公司,石油化工科学研究院,北京,100083
2010
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| Subjects | |
| Online Access | Get full text |
| ISSN | 0253-3820 |
| DOI | 10.3724/SP.J.1096.2010.00564 |
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| Abstract | 电喷雾电离源（ESI）可选择性地电离石油中的碱性氮化物,与具有超高质量分辨率和质量精度的傅立叶变换离子回旋共振质谱仪（FTICRMS）结合,可直接用于分析原油中的碱性氮化物而不需要预先分离。通过此方法考察了3种原油中碱性氮化物的类型分布和碳数分布,结果表明,原油中主要碱性氮化物为含N1,N2,NO,NS,NO2,NO3等杂原子的碱性氮化物,共检测到约100类不同缩合度的碱性氮化物,各类碱性氮化物的碳数分布范围为15～70。不同基属原油中的碱性氮化物在种类分布和碳数分布上存在一定的差异。 |
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| AbstractList | O6; 电喷雾电离源(ESI)可选择性地电离石油中的碱性氮化物,与具有超高质量分辨率和质量精度的傅立叶变换离子回旋共振质谱仪(FTICR MS)结合,可直接用于分析原油中的碱性氮化物而不需要预先分离.通过此方法考察了3种原油中碱性氮化物的类型分布和碳数分布,结果表明,原油中主要碱性氮化物为含N1, N2, NO, NS, NO2, NO3等杂原子的碱性氮化物,共检测到约100类不同缩合度的碱性氮化物,各类碱性氮化物的碳数分布范围为15～70.不同基属原油中的碱性氮化物在种类分布和碳数分布上存在一定的差异. 电喷雾电离源（ESI）可选择性地电离石油中的碱性氮化物,与具有超高质量分辨率和质量精度的傅立叶变换离子回旋共振质谱仪（FTICRMS）结合,可直接用于分析原油中的碱性氮化物而不需要预先分离。通过此方法考察了3种原油中碱性氮化物的类型分布和碳数分布,结果表明,原油中主要碱性氮化物为含N1,N2,NO,NS,NO2,NO3等杂原子的碱性氮化物,共检测到约100类不同缩合度的碱性氮化物,各类碱性氮化物的碳数分布范围为15～70。不同基属原油中的碱性氮化物在种类分布和碳数分布上存在一定的差异。 |
| Author | 胡秋玲 刘颖荣 刘泽龙 田松柏 徐振洪 |
| AuthorAffiliation | 中国石化股份有限公司石油化工科学研究院,北京100083 |
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| Author_FL | LIU Ying-Rong TIAN Song-Bai LIU Ze-Long HU Qiu-Ling XU Zheng-Hong |
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| DocumentTitleAlternate | Characterization of Basic Nitrogen Compounds in Crude Oil by Electrospray Fourier Transform Ion Cyclotron Resonance-Mass Spectrometry |
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| Keywords | 原油 碱性氮化物 傅立叶变换离子回旋共振质谱 电喷雾电离 |
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| Notes | Fourier transform ion cyclotron resonance-mass spectrometry 22-1125/O6 Crude oil Electrospray ionization TE626.24 Fourier transform ion cyclotron resonance-mass spectrometry; Electrospray ionization; Crude oil; Basic nitrogen compounds Basic nitrogen compounds |
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| Snippet | 电喷雾电离源（ESI）可选择性地电离石油中的碱性氮化物,与具有超高质量分辨率和质量精度的傅立叶变换离子回旋共振质谱仪（FTICRMS）结合,可直接用于分析原油中的碱性氮化... O6; 电喷雾电离源(ESI)可选择性地电离石油中的碱性氮化物,与具有超高质量分辨率和质量精度的傅立叶变换离子回旋共振质谱仪(FTICR MS)结合,可直接用于分析原油中的碱性氮化... |
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| SubjectTerms | 傅立叶变换离子回旋共振质谱 原油 电喷雾电离 碱性氮化物 |
| Title | 电喷雾-傅立叶变换离子回旋共振质谱分析原油中的碱性氮化物 |
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