二次微分简易示波伏安法用于安乃近测定

O657.1; 根据安乃近在0.1 mol·L-1 KNO3底液中产生切口(-1.2 V(vs.SCE))的示波特性,建立了安乃近的二次微分简易示波伏安测定法,并对安乃近片剂中的含量进行了直接测定.校正曲线的线性范围为5.0×10-6～5.0×10-5 mol·L-1,检出限为2×10-6 mol·L-1,对3.000×10-5 mo1·L-1安乃近五次测定结果的相对标准偏差为2.1%.本法具有仪器装置简单、经济,方法简便、快速,无需通氮除氧以及不必滤除赋形剂等优点....

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Published in电化学 Vol. 8; no. 2; pp. 224 - 227
Main Authors 陶福芳, 张宏芳, 熊迅宇, 郑建斌
Format Journal Article
LanguageChinese
Published 西北大学电分析化学研究所,陕西,西安,710069 2002
Subjects
示波分析
二次微分简易示波伏安法
安乃近
Online AccessGet full text
ISSN1006-3471
DOI10.3969/j.issn.1006-3471.2002.02.018

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Abstract O657.1; 根据安乃近在0.1 mol·L-1 KNO3底液中产生切口(-1.2 V(vs.SCE))的示波特性,建立了安乃近的二次微分简易示波伏安测定法,并对安乃近片剂中的含量进行了直接测定.校正曲线的线性范围为5.0×10-6～5.0×10-5 mol·L-1,检出限为2×10-6 mol·L-1,对3.000×10-5 mo1·L-1安乃近五次测定结果的相对标准偏差为2.1%.本法具有仪器装置简单、经济,方法简便、快速,无需通氮除氧以及不必滤除赋形剂等优点.
AbstractList O657.1; 根据安乃近在0.1 mol·L-1 KNO3底液中产生切口(-1.2 V(vs.SCE))的示波特性,建立了安乃近的二次微分简易示波伏安测定法,并对安乃近片剂中的含量进行了直接测定.校正曲线的线性范围为5.0×10-6～5.0×10-5 mol·L-1,检出限为2×10-6 mol·L-1,对3.000×10-5 mo1·L-1安乃近五次测定结果的相对标准偏差为2.1%.本法具有仪器装置简单、经济,方法简便、快速,无需通氮除氧以及不必滤除赋形剂等优点.
Author 郑建斌
张宏芳
陶福芳
熊迅宇
AuthorAffiliation 西北大学电分析化学研究所,陕西,西安,710069
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Keywords 示波分析
二次微分简易示波伏安法
安乃近
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Snippet O657.1; 根据安乃近在0.1 mol·L-1 KNO3底液中产生切口(-1.2 V(vs.SCE))的示波特性,建立了安乃近的二次微分简易示波伏安测定法,并对安乃近片剂中的含量进行了直接测定.校正...
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Title 二次微分简易示波伏安法用于安乃近测定
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