Trace amounts of poly-β-cyclodextrin wrapped carbon nanotubes for the microextraction of flavonoids in honey samples by capillary electrophoresis with light-emitting diode induced fluorescence detection
A novel dispersive micro‐SPE method with trace poly‐β‐CD wrapped multiwalled carbon nanotubes as sorbents was applied to extract flavonoids in honey samples. The analytes were then determined by CE with LED‐induced fluorescence detection. The influencing parameters, such as the sorbent concentration...
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| Published in | Electrophoresis Vol. 37; no. 13; pp. 1891 - 1901 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Germany
Blackwell Publishing Ltd
01.07.2016
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| Subjects | |
| Online Access | Get full text |
| ISSN | 0173-0835 1522-2683 1522-2683 |
| DOI | 10.1002/elps.201600016 |
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| Abstract | A novel dispersive micro‐SPE method with trace poly‐β‐CD wrapped multiwalled carbon nanotubes as sorbents was applied to extract flavonoids in honey samples. The analytes were then determined by CE with LED‐induced fluorescence detection. The influencing parameters, such as the sorbent concentration, extraction time, and eluent type, were properly optimized. The established method had the advantages of simplicity, low consumption of sorbent amount (0.009 mg) and organic solvent (100 μL), and high sensitivity, meeting the principle of green chemistry. Under the optimum conditions, the sorbents allowed the extraction and preconcentration of the flavonoids with enrichment factors in the range from 78 to 166. The recovery study performed at two different fortification levels provided an average recovery >91%. LODs for all the compounds ranged from 0.07 to 17.99 ng/mL. These results demonstrated that the proposed method could be used as a convenient and efficient extraction technique for analysis of flavonoids in different honey matrices. |
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| AbstractList | A novel dispersive micro-SPE method with trace poly- beta -CD wrapped multiwalled carbon nanotubes as sorbents was applied to extract flavonoids in honey samples. The analytes were then determined by CE with LED-induced fluorescence detection. The influencing parameters, such as the sorbent concentration, extraction time, and eluent type, were properly optimized. The established method had the advantages of simplicity, low consumption of sorbent amount (0.009 mg) and organic solvent (100 mu L), and high sensitivity, meeting the principle of green chemistry. Under the optimum conditions, the sorbents allowed the extraction and preconcentration of the flavonoids with enrichment factors in the range from 78 to 166. The recovery study performed at two different fortification levels provided an average recovery >91%. LODs for all the compounds ranged from 0.07 to 17.99 ng/mL. These results demonstrated that the proposed method could be used as a convenient and efficient extraction technique for analysis of flavonoids in different honey matrices. A novel dispersive micro-SPE method with trace poly-β-CD wrapped multiwalled carbon nanotubes as sorbents was applied to extract flavonoids in honey samples. The analytes were then determined by CE with LED-induced fluorescence detection. The influencing parameters, such as the sorbent concentration, extraction time, and eluent type, were properly optimized. The established method had the advantages of simplicity, low consumption of sorbent amount (0.009 mg) and organic solvent (100 μL), and high sensitivity, meeting the principle of green chemistry. Under the optimum conditions, the sorbents allowed the extraction and preconcentration of the flavonoids with enrichment factors in the range from 78 to 166. The recovery study performed at two different fortification levels provided an average recovery >91%. LODs for all the compounds ranged from 0.07 to 17.99 ng/mL. These results demonstrated that the proposed method could be used as a convenient and efficient extraction technique for analysis of flavonoids in different honey matrices. |
| Author | Yang, Rui An, Mingrui Xu, Jing-Jing Peng, Li-Qing Cao, Jun Ye, Li-Hong |
| Author_xml | – sequence: 1 givenname: Jing-Jing surname: Xu fullname: Xu, Jing-Jing organization: College of Material Chemistry and Chemical Engineering, Hangzhou Normal University, Hangzhou, P. R. China – sequence: 2 givenname: Mingrui surname: An fullname: An, Mingrui organization: Department of Surgery, University of Michigan Medical Center, MI, Ann Arbor, USA – sequence: 3 givenname: Rui surname: Yang fullname: Yang, Rui organization: Department of Surgery, University of Michigan Medical Center, MI, Ann Arbor, USA – sequence: 4 givenname: Jun surname: Cao fullname: Cao, Jun email: caojun91@163.com organization: College of Material Chemistry and Chemical Engineering, Hangzhou Normal University, Hangzhou, P. R. China – sequence: 5 givenname: Li-Hong surname: Ye fullname: Ye, Li-Hong organization: Department of Traditional Chinese Medicine, Hangzhou Red Cross Hospital, Hangzhou, P. R. China – sequence: 6 givenname: Li-Qing surname: Peng fullname: Peng, Li-Qing organization: College of Material Chemistry and Chemical Engineering, Hangzhou Normal University, Hangzhou, P. R. China |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/27060460$$D View this record in MEDLINE/PubMed |
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| CitedBy_id | crossref_primary_10_1002_elps_202000248 crossref_primary_10_1016_j_microc_2018_07_029 crossref_primary_10_1080_10739149_2017_1394877 crossref_primary_10_1002_elps_201700340 crossref_primary_10_1002_elps_201700321 crossref_primary_10_1021_acs_langmuir_4c01223 crossref_primary_10_1016_j_chroma_2023_464116 crossref_primary_10_1007_s00604_021_04743_y crossref_primary_10_1016_j_apmt_2017_09_008 crossref_primary_10_1007_s12161_017_0904_4 crossref_primary_10_1002_elps_201800102 crossref_primary_10_1016_j_chroma_2018_05_031 |
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| Keywords | Honey Flavonoids Dispersive micro-SPE Poly-β-CD wrapped carbon nanotubes LED-induced fluorescence detection |
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| References_xml | – reference: Xue, J., Jia, Z., Jiang, X., Wang, Y., Chen, L., Zhou, L., He, P., Zhu, X., Yan, D., Macromolecules 2006, 39, 8905-8907. – reference: Liu, W., Guo, R., Colloid Surface A 2006, 274, 192-199. – reference: Lin, J. F., Mason, C. W., Adame, A., Liu, X., Peng, X. H., Kannan, A. M., Electrochim. Acta 2010, 55, 6496-6500. – reference: Rostamnia, S., Doustkhah, E., J. Magn. Magn. Mater. 2015, 386, 111-116. – reference: Ferey, L., Delaunay, N., Rutledge, D. N., Cordella, C. B. Y., This, H., Huertas, A., Raoul, Y., Gareil, P., Talanta 2014, 119, 572-581. – reference: Stafiej, A., Pyrzynska, K., Microchem. J. 2008, 89, 29-33. – reference: Cao, W., Hu, S. S., Ye, L. H., Cao, J., Xu, J. J., Pang, X. Q., J. Chromatogr. A 2015, 1390, 13-21. – reference: Pang, J. Y., Xu, G. Y., Bai, Y., Yuan, S. L., He, F., Wang, Y. J., Sun, H. Y., Hao, A. Y., Comput. Mater. Sci. 2010, 50, 283-290. – reference: Cao, W., Hu, S. S., Li, X. Y., Pang, X. Q., Cao, J., Ye, L. H., Dai, H. 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| Snippet | A novel dispersive micro‐SPE method with trace poly‐β‐CD wrapped multiwalled carbon nanotubes as sorbents was applied to extract flavonoids in honey samples.... A novel dispersive micro-SPE method with trace poly-β-CD wrapped multiwalled carbon nanotubes as sorbents was applied to extract flavonoids in honey samples.... A novel dispersive micro-SPE method with trace poly- beta -CD wrapped multiwalled carbon nanotubes as sorbents was applied to extract flavonoids in honey... |
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| SubjectTerms | adsorbents Adsorption beta-Cyclodextrins - analysis capillary electrophoresis carbon nanotubes Dispersive micro-SPE Electrophoresis Electrophoresis, Capillary - methods Enrichment Extraction Flavonoids Flavonoids - isolation & purification Fluorescence green chemistry Honey Honey - analysis LED-induced fluorescence detection Limit of Detection microextraction Microscopy, Atomic Force Microscopy, Electron, Scanning Microscopy, Electron, Transmission Molecular Weight Nanotubes, Carbon Poly-β-CD wrapped carbon nanotubes Recovery Solid Phase Extraction - methods solvents Sorbents Spectrometry, Fluorescence - methods |
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| Title | Trace amounts of poly-β-cyclodextrin wrapped carbon nanotubes for the microextraction of flavonoids in honey samples by capillary electrophoresis with light-emitting diode induced fluorescence detection |
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