Galvanic Replacement Reactions in Metal Oxide Nanocrystals
Galvanic replacement reactions provide a simple and versatile route for producing hollow nanostructures with controllable pore structures and compositions. However, these reactions have previously been limited to the chemical transformation of metallic nanostructures. We demonstrated galvanic replac...
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| Published in | Science (American Association for the Advancement of Science) Vol. 340; no. 6135; pp. 964 - 968 |
|---|---|
| Main Authors | , , , , , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Washington, DC
American Association for the Advancement of Science
24.05.2013
The American Association for the Advancement of Science |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0036-8075 1095-9203 1095-9203 |
| DOI | 10.1126/science.1234751 |
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| Abstract | Galvanic replacement reactions provide a simple and versatile route for producing hollow nanostructures with controllable pore structures and compositions. However, these reactions have previously been limited to the chemical transformation of metallic nanostructures. We demonstrated galvanic replacement reactions in metal oxide nanocrystals as well. When manganese oxide (Mn₃O₄) nanocrystals were reacted with iron(ll) perchlorate, hollow box-shaped nanocrystals of Mn₃O₄/γ-Fw₂O₃ ("nanoboxes") were produced. These nanoboxes ultimately transformed into hollow cagelike nanocrystals of γ-Fe₂O₃ ("nanocages"). Because of their nonequilibrium compositions and hollow structures, these nanoboxes and nanocages exhibited good performance as anode materials for lithium ion batteries. The generality of this approach was demonstrated with other metal pairs, including Co₃O₄/SnO₂ and Mn₃O₄/SnO₂. |
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| AbstractList | Hollowing Out Metal Oxide Nanoparticles Corrosion is normally a problem, but it can be useful, for example, when you wish to create hollow metal nanoparticles, whereby the reduction of one metal species in solution drives the dissolution of the core of the particle. Oh et al. (p. 964; see the Perspective by Ibáñez and Cabot) adapted this approach to metal oxide nanoparticles by placing Mn ₃O ₄ nanocrystals in solution with Fe ²⁺ ions, which replaces the nanocrystal exterior with γ-Fe ₂O ₃. At sufficiently high Fe ²⁺ concentrations, hollow γ-Fe ₂O ₃ nanocages formed. These hollow structures could be used as anode materials for lithium ion batteries. Hollowing Out Metal Oxide NanoparticlesCorrosion is normally a problem, but it can be useful, for example, when you wish to create hollow metal nanoparticles, whereby the reduction of one metal species in solution drives the dissolution of the core of the particle. Oh et al. (p. 964; see the Perspective by Ibanez and Cabot) adapted this approach to metal oxide nanoparticles by placing Mn3O4 nanocrystals in solution with Fe2+ ions, which replaces the nanocrystal exterior with gamma -Fe2O3. At sufficiently high Fe2+ concentrations, hollow gamma -Fe2O3 nanocages formed. These hollow structures could be used as anode materials for lithium ion batteries. Galvanic replacement reactions provide a simple and versatile route for producing hollow nanostructures with controllable pore structures and compositions. However, these reactions have previously been limited to the chemical transformation of metallic nanostructures. We demonstrated galvanic replacement reactions in metal oxide nanocrystals as well. When manganese oxide (Mn3O4) nanocrystals were reacted with iron(II) perchlorate, hollow box-shaped nanocrystals of Mn3O4/γ-Fe2O3 ("nanoboxes") were produced. These nanoboxes ultimately transformed into hollow cagelike nanocrystals of γ-Fe2O3 ("nanocages"). Because of their nonequilibrium compositions and hollow structures, these nanoboxes and nanocages exhibited good performance as anode materials for lithium ion batteries. The generality of this approach was demonstrated with other metal pairs, including Co3O4/SnO2 and Mn3O4/SnO2.Galvanic replacement reactions provide a simple and versatile route for producing hollow nanostructures with controllable pore structures and compositions. However, these reactions have previously been limited to the chemical transformation of metallic nanostructures. We demonstrated galvanic replacement reactions in metal oxide nanocrystals as well. When manganese oxide (Mn3O4) nanocrystals were reacted with iron(II) perchlorate, hollow box-shaped nanocrystals of Mn3O4/γ-Fe2O3 ("nanoboxes") were produced. These nanoboxes ultimately transformed into hollow cagelike nanocrystals of γ-Fe2O3 ("nanocages"). Because of their nonequilibrium compositions and hollow structures, these nanoboxes and nanocages exhibited good performance as anode materials for lithium ion batteries. The generality of this approach was demonstrated with other metal pairs, including Co3O4/SnO2 and Mn3O4/SnO2. Corrosion is normally a problem, but it can be useful, for example, when you wish to create hollow metal nanoparticles, whereby the reduction of one metal species in solution drives the dissolution of the core of the particle. Oh et al. (p. 964; see the Perspective by Ibáñez and Cabot ) adapted this approach to metal oxide nanoparticles by placing Mn3O4 nanocrystals in solution with Fe2+ ions, which replaces the nanocrystal exterior with γ-Fe2O3. At sufficiently high Fe2+ concentrations, hollow γ-Fe2O3 nanocages formed. These hollow structures could be used as anode materials for lithium ion batteries. [PUBLICATION ABSTRACT] Galvanic replacement reactions provide a simple and versatile route for producing hollow nanostructures with controllable pore structures and compositions. However, these reactions have previously been limited to the chemical transformation of metallic nanostructures. We demonstrated galvanic replacement reactions in metal oxide nanocrystals as well. When manganese oxide (Mn3O4) nanocrystals were reacted with iron(II) perchlorate, hollow box-shaped nanocrystals of Mn3O4/γ-Fe2O3 ("nanoboxes") were produced. These nanoboxes ultimately transformed into hollow cagelike nanocrystals of γ-Fe2O3 ("nanocages"). Because of their nonequilibrium compositions and hollow structures, these nanoboxes and nanocages exhibited good performance as anode materials for lithium ion batteries. The generality of this approach was demonstrated with other metal pairs, including Co3O4/SnO2 and Mn3O4/SnO2. [PUBLICATION ABSTRACT] Galvanic replacement reactions provide a simple and versatile route for producing hollow nanostructures with controllable pore structures and compositions. However, these reactions have previously been limited to the chemical transformation of metallic nanostructures. We demonstrated galvanic replacement reactions in metal oxide nanocrystals as well. When manganese oxide (Mn3O4) nanocrystals were reacted with iron(II) perchlorate, hollow box-shaped nanocrystals of Mn3O4/γ-Fe2O3 ("nanoboxes") were produced. These nanoboxes ultimately transformed into hollow cagelike nanocrystals of γ-Fe2O3 ("nanocages"). Because of their nonequilibrium compositions and hollow structures, these nanoboxes and nanocages exhibited good performance as anode materials for lithium ion batteries. The generality of this approach was demonstrated with other metal pairs, including Co3O4/SnO2 and Mn3O4/SnO2. Galvanic replacement reactions provide a simple and versatile route for producing hollow nanostructures with controllable pore structures and compositions. However, these reactions have previously been limited to the chemical transformation of metallic nanostructures. We demonstrated galvanic replacement reactions in metal oxide nanocrystals as well. When manganese oxide (Mn₃O₄) nanocrystals were reacted with iron(ll) perchlorate, hollow box-shaped nanocrystals of Mn₃O₄/γ-Fw₂O₃ ("nanoboxes") were produced. These nanoboxes ultimately transformed into hollow cagelike nanocrystals of γ-Fe₂O₃ ("nanocages"). Because of their nonequilibrium compositions and hollow structures, these nanoboxes and nanocages exhibited good performance as anode materials for lithium ion batteries. The generality of this approach was demonstrated with other metal pairs, including Co₃O₄/SnO₂ and Mn₃O₄/SnO₂. Corrosion is normally a problem, but it can be useful, for example, when you wish to create hollow metal nanoparticles, whereby the reduction of one metal species in solution drives the dissolution of the core of the particle. Oh et al. (p. 964 ; see the Perspective by Ibáñez and Cabot ) adapted this approach to metal oxide nanoparticles by placing Mn 3 O 4 nanocrystals in solution with Fe 2+ ions, which replaces the nanocrystal exterior with γ-Fe 2 O 3 . At sufficiently high Fe 2+ concentrations, hollow γ-Fe 2 O 3 nanocages formed. These hollow structures could be used as anode materials for lithium ion batteries. Hollow mixed-metal oxide nanoparticles can be made by replacing the metal cations through redox reactions in solution. [Also see Perspective by Ibáñez and Cabot ] Galvanic replacement reactions provide a simple and versatile route for producing hollow nanostructures with controllable pore structures and compositions. However, these reactions have previously been limited to the chemical transformation of metallic nanostructures. We demonstrated galvanic replacement reactions in metal oxide nanocrystals as well. When manganese oxide (Mn 3 O 4 ) nanocrystals were reacted with iron(II) perchlorate, hollow box-shaped nanocrystals of Mn 3 O 4 /γ-Fe 2 O 3 (“nanoboxes”) were produced. These nanoboxes ultimately transformed into hollow cagelike nanocrystals of γ-Fe 2 O 3 (“nanocages”). Because of their nonequilibrium compositions and hollow structures, these nanoboxes and nanocages exhibited good performance as anode materials for lithium ion batteries. The generality of this approach was demonstrated with other metal pairs, including Co 3 O 4 /SnO 2 and Mn 3 O 4 /SnO 2 . |
| Author | Ko, Kyung-Tae Pinna, Nicola Kim, Byung Hyo Cho, Min Gee Lim, Byungkwon Oh, Myoung Hwan Yu, Taekyung Willinger, Marc-Georg Yu, Seung-Ho Seo, Dong-Hwa Hyeon, Taeghwan Kang, Kisuk Sung, Yung-Eun Park, Jae-Hoon |
| Author_xml | – sequence: 1 givenname: Myoung Hwan surname: Oh fullname: Oh, Myoung Hwan – sequence: 2 givenname: Taekyung surname: Yu fullname: Yu, Taekyung – sequence: 3 givenname: Seung-Ho surname: Yu fullname: Yu, Seung-Ho – sequence: 4 givenname: Byungkwon surname: Lim fullname: Lim, Byungkwon – sequence: 5 givenname: Kyung-Tae surname: Ko fullname: Ko, Kyung-Tae – sequence: 6 givenname: Marc-Georg surname: Willinger fullname: Willinger, Marc-Georg – sequence: 7 givenname: Dong-Hwa surname: Seo fullname: Seo, Dong-Hwa – sequence: 8 givenname: Byung Hyo surname: Kim fullname: Kim, Byung Hyo – sequence: 9 givenname: Min Gee surname: Cho fullname: Cho, Min Gee – sequence: 10 givenname: Jae-Hoon surname: Park fullname: Park, Jae-Hoon – sequence: 11 givenname: Kisuk surname: Kang fullname: Kang, Kisuk – sequence: 12 givenname: Yung-Eun surname: Sung fullname: Sung, Yung-Eun – sequence: 13 givenname: Nicola surname: Pinna fullname: Pinna, Nicola – sequence: 14 givenname: Taeghwan surname: Hyeon fullname: Hyeon, Taeghwan |
| BackLink | http://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=27400786$$DView record in Pascal Francis https://www.ncbi.nlm.nih.gov/pubmed/23704569$$D View this record in MEDLINE/PubMed |
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| Snippet | Galvanic replacement reactions provide a simple and versatile route for producing hollow nanostructures with controllable pore structures and compositions.... Corrosion is normally a problem, but it can be useful, for example, when you wish to create hollow metal nanoparticles, whereby the reduction of one metal... Hollowing Out Metal Oxide NanoparticlesCorrosion is normally a problem, but it can be useful, for example, when you wish to create hollow metal nanoparticles,... Hollowing Out Metal Oxide Nanoparticles Corrosion is normally a problem, but it can be useful, for example, when you wish to create hollow metal nanoparticles,... |
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| SubjectTerms | Anodes batteries Chemical composition Chemical reactions CMOS Cobalt - chemistry corrosion Cross-disciplinary physics: materials science; rheology Dissolution Exact sciences and technology Exteriors Ferric Compounds - chemistry Ions iron Lithium Lithium batteries Manganese Manganese Compounds - chemistry Manganese oxides Materials science Metal Nanoparticles - chemistry Metal Nanoparticles - ultrastructure Metal oxides Metals Methods of nanofabrication Microscopy, Electron, Transmission Nanocrystalline materials Nanocrystals Nanoparticles Nanoscale materials and structures: fabrication and characterization Nanostructure Nanostructures Oxides Oxides - chemistry Perchlorate Perchlorates Perchlorates - chemistry Physics Placing Replacement reactions Research universities Tin Compounds - chemistry |
| Title | Galvanic Replacement Reactions in Metal Oxide Nanocrystals |
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