Effect of calcium and potassium oxide addition on the viscosity and fragility of a calcium aluminosilicate melt
Fragility is commonly quantified as the magnitude of change in viscosity at a temperature close to the glass transition temperature (Tg). It is a critical characteristic of melts used in scientific and industrial applications. The fragility of silicate melts generally increases with the depolymeriza...
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| Published in | Journal of the American Ceramic Society Vol. 107; no. 6; pp. 3822 - 3836 |
|---|---|
| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Columbus
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01.06.2024
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| Series | Journal of the American Ceramic Society |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0002-7820 1551-2916 1551-2916 |
| DOI | 10.1111/jace.19722 |
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| Abstract | Fragility is commonly quantified as the magnitude of change in viscosity at a temperature close to the glass transition temperature (Tg). It is a critical characteristic of melts used in scientific and industrial applications. The fragility of silicate melts generally increases with the depolymerization of silicate anions upon the addition of alkali or alkaline earth oxides. However, the effects of oxide additives on the fragility of aluminosilicate melts remain unclear. In this study, the effect of CaO or K2O addition on the viscosity of the 36CaO–51SiO2–13Al2O3 (mol.%) melt for the wide viscosity range of 10−1–1012 Pa s was studied. The relationship between the logarithmic viscosity and Tg‐scaled temperature indicated that the melt fragility increased with the addition of CaO, whereas the addition of K2O reduced the fragility when the additive content of CaO or K2O was less than 10.8 mol.%. The effect of the addition of K2O on fragility cannot be explained by the depolymerization of silicate anions alone. Raman and 27Al nuclear magnetic resonance spectroscopies of the glasses indicated that a decrease in the level of distortion of the AlO4 tetrahedra decreased the fragility of the aluminosilicate melt. |
|---|---|
| AbstractList | Fragility is commonly quantified as the magnitude of change in viscosity at a temperature close to the glass transition temperature (
T
g
). It is a critical characteristic of melts used in scientific and industrial applications. The fragility of silicate melts generally increases with the depolymerization of silicate anions upon the addition of alkali or alkaline earth oxides. However, the effects of oxide additives on the fragility of aluminosilicate melts remain unclear. In this study, the effect of CaO or K
2
O addition on the viscosity of the 36CaO–51SiO
2
–13Al
2
O
3
(mol.%) melt for the wide viscosity range of 10
−1
–10
12
Pa s was studied. The relationship between the logarithmic viscosity and
T
g
‐scaled temperature indicated that the melt fragility increased with the addition of CaO, whereas the addition of K
2
O reduced the fragility when the additive content of CaO or K
2
O was less than 10.8 mol.%. The effect of the addition of K
2
O on fragility cannot be explained by the depolymerization of silicate anions alone. Raman and
27
Al nuclear magnetic resonance spectroscopies of the glasses indicated that a decrease in the level of distortion of the AlO
4
tetrahedra decreased the fragility of the aluminosilicate melt. Fragility is commonly quantified as the magnitude of change in viscosity at a temperature close to the glass transition temperature (Tg). It is a critical characteristic of melts used in scientific and industrial applications. The fragility of silicate melts generally increases with the depolymerization of silicate anions upon the addition of alkali or alkaline earth oxides. However, the effects of oxide additives on the fragility of aluminosilicate melts remain unclear. In this study, the effect of CaO or K2O addition on the viscosity of the 36CaO–51SiO2–13Al2O3 (mol.%) melt for the wide viscosity range of 10−1–1012 Pa s was studied. The relationship between the logarithmic viscosity and Tg‐scaled temperature indicated that the melt fragility increased with the addition of CaO, whereas the addition of K2O reduced the fragility when the additive content of CaO or K2O was less than 10.8 mol.%. The effect of the addition of K2O on fragility cannot be explained by the depolymerization of silicate anions alone. Raman and 27Al nuclear magnetic resonance spectroscopies of the glasses indicated that a decrease in the level of distortion of the AlO4 tetrahedra decreased the fragility of the aluminosilicate melt. Fragility is commonly quantified as the magnitude of change in viscosity at a temperature close to the glass transition temperature (Tg). It is a critical characteristic of melts used in scientific and industrial applications. The fragility of silicate melts generally increases with the depolymerization of silicate anions upon the addition of alkali or alkaline earth oxides. However, the effects of oxide additives on the fragility of aluminosilicate melts remain unclear. In this study, the effect of CaO or K2O addition on the viscosity of the 36CaO–51SiO2–13Al2O3 (mol.%) melt for the wide viscosity range of 10−1–1012 Pa s was studied. The relationship between the logarithmic viscosity and Tg‐scaled temperature indicated that the melt fragility increased with the addition of CaO, whereas the addition of K2O reduced the fragility when the additive content of CaO or K2O was less than 10.8 mol.%. The effect of the addition of K2O on fragility cannot be explained by the depolymerization of silicate anions alone. Raman and 27Al nuclear magnetic resonance spectroscopies of the glasses indicated that a decrease in the level of distortion of the AlO4 tetrahedra decreased the fragility of the aluminosilicate melt. |
| Author | Saito, Noritaka Gueguen, Yann Celarie, Fabrice Sukenaga, Sohei Rouxel, Tanguy Yoshida, Shinichiro Shibata, Hiroyuki Tashiro, Masanori Nakashima, Kunihiko |
| Author_xml | – sequence: 1 givenname: Sohei orcidid: 0000-0002-9086-2784 surname: Sukenaga fullname: Sukenaga, Sohei email: sohei.sukenaga.d3@tohoku.ac.jp organization: Tohoku University – sequence: 2 givenname: Yann orcidid: 0000-0001-6348-3060 surname: Gueguen fullname: Gueguen, Yann organization: Univ Rennes, CNRS, IPR (Institut de Physique de Rennes) ‐ UMR 6251 – sequence: 3 givenname: Fabrice surname: Celarie fullname: Celarie, Fabrice organization: Univ Rennes, CNRS, IPR (Institut de Physique de Rennes) ‐ UMR 6251 – sequence: 4 givenname: Tanguy surname: Rouxel fullname: Rouxel, Tanguy organization: Univ Rennes, CNRS, IPR (Institut de Physique de Rennes) ‐ UMR 6251 – sequence: 5 givenname: Masanori surname: Tashiro fullname: Tashiro, Masanori organization: Tohoku University – sequence: 6 givenname: Shinichiro surname: Yoshida fullname: Yoshida, Shinichiro organization: Tohoku University – sequence: 7 givenname: Noritaka surname: Saito fullname: Saito, Noritaka organization: Kyushu University – sequence: 8 givenname: Kunihiko surname: Nakashima fullname: Nakashima, Kunihiko organization: Kyushu University – sequence: 9 givenname: Hiroyuki surname: Shibata fullname: Shibata, Hiroyuki organization: Tohoku University |
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| Keywords | Viscosity Aluminosilicate Calcium oxide Calcium Mineralogy Physical chemistry Materials science Composite material Fragility Calcium aluminosilicate Oxide Organic chemistry Chemistry Inorganic chemistry Catalysis Metallurgy Potassium |
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| Snippet | Fragility is commonly quantified as the magnitude of change in viscosity at a temperature close to the glass transition temperature (Tg). It is a critical... Fragility is commonly quantified as the magnitude of change in viscosity at a temperature close to the glass transition temperature ( T g ). It is a critical... |
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| SubjectTerms | Additives Alkaline earth oxides aluminosilicate glass aluminosilicate melt Aluminosilicates Aluminum silicates Anions Calcium oxide Depolymerization Fragility Glass transition temperature Industrial applications Melts NMR Nuclear magnetic resonance Physics Potassium oxides Tetrahedra Viscosity |
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| Title | Effect of calcium and potassium oxide addition on the viscosity and fragility of a calcium aluminosilicate melt |
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