Miscibility and hydrolytic degradation in alkaline solution of poly( l-lactide) and poly( p-vinyl phenol) blends

Poly( l-lactide) (PLLA) was melt-blended with poly( p-vinyl phenol) (PVPh) using a two-roll mill, and the miscibility between PLLA and PVPh and degradation of the blend films were investigated. It was found that PLLA/PVPh blend has miscibility in the amorphous state because only single T g was obser...

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Published in	Polymer Degradation and Stability Vol. 92; no. 8; pp. 1626 - 1631
Main Authors	Shirahase, Tomoko, Komatsu, Yoichi, Marubayashi, Hironori, Tominaga, Yoichi, Asai, Shigeo, Sumita, Masao
Format	Journal Article
Language	English
Published	Oxford Elsevier Ltd 01.08.2007 Elsevier BV Elsevier Science
Subjects	Applied sciences Chemical reactions and properties Degradation Exact sciences and technology Heat resistance improvement Miscible blend Organic polymers Physicochemistry of polymers Poly( l-lactide) Polymer blend Degradation Poly( l-lactide) Heat resistance improvement Polymer blend Miscible blend Elastic modulus Polymer blends Property composition relationship Mechanical properties Chemical degradation Poly(L-lactide) Experimental study Lactone polymer Styrene(hydroxy) polymer Hydrolysis Hydrolysis resistance Lactic acid polymer Morphology Aliphatic polymer Miscibility Basic medium Chemical properties Thermodynamic properties
Online Access	Get full text
ISSN	0141-3910 1873-2321
DOI	10.1016/j.polymdegradstab.2007.04.003

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Abstract	Poly( l-lactide) (PLLA) was melt-blended with poly( p-vinyl phenol) (PVPh) using a two-roll mill, and the miscibility between PLLA and PVPh and degradation of the blend films were investigated. It was found that PLLA/PVPh blend has miscibility in the amorphous state because only single T g was observed in the DSC and DMA measurements. The T g of the PLLA/PVPh blend could be controlled in the temperature range from 55 °C to 117 °C by changing the PVPh weight fraction. In alkaline solution, degradation rate of PLLA/PVPh blends was faster than that of neat PLLA because PVPh could dissolve in alkaline solution. The surface morphology of degraded PLLA and PLLA/PVPh blend were observed by SEM. The surface morphology of degraded PLLA/PVPh blend was finer than that of PLLA. Young's modulus of PLLA/PVPh blend increased with increasing PVPh content. Yield stress of PLLA/PVPh blends whose PVPh content was less than 30 wt% kept the level of about 55 MPa and that of PLLA/PVPh blend whose PVPh content was 40 wt% is much lower than that of neat PLLA.
AbstractList	Poly( l-lactide) (PLLA) was melt-blended with poly( p-vinyl phenol) (PVPh) using a two-roll mill, and the miscibility between PLLA and PVPh and degradation of the blend films were investigated. It was found that PLLA/PVPh blend has miscibility in the amorphous state because only single T g was observed in the DSC and DMA measurements. The T g of the PLLA/PVPh blend could be controlled in the temperature range from 55 °C to 117 °C by changing the PVPh weight fraction. In alkaline solution, degradation rate of PLLA/PVPh blends was faster than that of neat PLLA because PVPh could dissolve in alkaline solution. The surface morphology of degraded PLLA and PLLA/PVPh blend were observed by SEM. The surface morphology of degraded PLLA/PVPh blend was finer than that of PLLA. Young's modulus of PLLA/PVPh blend increased with increasing PVPh content. Yield stress of PLLA/PVPh blends whose PVPh content was less than 30 wt% kept the level of about 55 MPa and that of PLLA/PVPh blend whose PVPh content was 40 wt% is much lower than that of neat PLLA. Poly(l-lactide) (PLLA) was melt-blended with poly(p-vinyl phenol) (PVPh) using a two-roll mill, and the miscibility between PLLA and PVPh and degradation of the blend films were investigated. It was found that PLLA/PVPh blend has miscibility in the amorphous state because only single Tg was observed in the DSC and DMA measurements. The Tg of the PLLA/PVPh blend could be controlled in the temperature range from 55 deg C to 117 deg C by changing the PVPh weight fraction. In alkaline solution, degradation rate of PLLA/PVPh blends was faster than that of neat PLLA because PVPh could dissolve in alkaline solution. The surface morphology of degraded PLLA and PLLA/PVPh blend were observed by SEM. The surface morphology of degraded PLLA/PVPh blend was finer than that of PLLA. Young's modulus of PLLA/PVPh blend increased with increasing PVPh content. Yield stress of PLLA/PVPh blends whose PVPh content was less than 30wt% kept the level of about 55MPa and that of PLLA/PVPh blend whose PVPh content was 40wt% is much lower than that of neat PLLA.
Author	Sumita, Masao Tominaga, Yoichi Komatsu, Yoichi Shirahase, Tomoko Marubayashi, Hironori Asai, Shigeo
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Keywords	Degradation Poly( l-lactide) Heat resistance improvement Polymer blend Miscible blend Elastic modulus Polymer blends Property composition relationship Mechanical properties Chemical degradation Poly(L-lactide) Experimental study Lactone polymer Styrene(hydroxy) polymer Hydrolysis Hydrolysis resistance Lactic acid polymer Morphology Aliphatic polymer Miscibility Basic medium Chemical properties Thermodynamic properties
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Snippet	Poly( l-lactide) (PLLA) was melt-blended with poly( p-vinyl phenol) (PVPh) using a two-roll mill, and the miscibility between PLLA and PVPh and degradation of... Poly(l-lactide) (PLLA) was melt-blended with poly(p-vinyl phenol) (PVPh) using a two-roll mill, and the miscibility between PLLA and PVPh and degradation of...
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SubjectTerms	Applied sciences Chemical reactions and properties Degradation Exact sciences and technology Heat resistance improvement Miscible blend Organic polymers Physicochemistry of polymers Poly( l-lactide) Polymer blend
Title	Miscibility and hydrolytic degradation in alkaline solution of poly( l-lactide) and poly( p-vinyl phenol) blends
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