Overview of Liquid Sample Preparation Techniques for Analysis, Using Metal-Organic Frameworks as Sorbents

The preparation of samples for instrumental analysis is the most essential and time-consuming stage of the entire analytical process; it also has the greatest impact on the analysis results. Concentrating the sample, changing its matrix, and removing interferents are often necessary. Techniques for...

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Published inMolecules (Basel, Switzerland) Vol. 29; no. 19; p. 4752
Main Authors Woźniak, Jakub, Nawała, Jakub, Dziedzic, Daniel, Popiel, Stanisław
Format Journal Article
LanguageEnglish
Published Switzerland MDPI AG 01.10.2024
MDPI
Subjects
Efficiency
Laboratories
Ligands
magnetic solid-phase extraction (MSPE)
metal-organic frameworks (MOFs)
micro-solid-phase extraction (µ-SPE)
pipette-tip solid-phase extraction (PT-SPE)
Porous materials
Review
solid-phase extraction (SPE)
solid-phase microextraction (SPME)
Sorbents
Zeolites
Israel
matrix solid-phase dispersion (MSPD)
micro-solid-phase extraction (µ-SPE)
solid-phase microextraction (SPME)
pipette-tip solid-phase extraction (PT-SPE)
magnetic solid-phase extraction (MSPE)
metal-organic frameworks (MOFs)
stir-bar sorptive extraction (SBSE)
solid-phase extraction (SPE)
Online AccessGet full text
ISSN1420-3049
1420-3049
DOI10.3390/molecules29194752

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Abstract The preparation of samples for instrumental analysis is the most essential and time-consuming stage of the entire analytical process; it also has the greatest impact on the analysis results. Concentrating the sample, changing its matrix, and removing interferents are often necessary. Techniques for preparing samples for analysis are constantly being developed and modified to meet new challenges, facilitate work, and enable the determination of analytes in the most comprehensive concentration range possible. This paper focuses on using metal-organic frameworks (MOFs) as sorbents in the most popular techniques for preparing liquid samples for analysis, based on liquid-solid extraction. An increase in interest in MOFs-type materials has been observed for about 20 years, mainly due to their sorption properties, resulting, among others, from the high specific surface area, tunable pore size, and the theoretically wide possibility of their modification. This paper presents certain advantages and disadvantages of the most popular sample preparation techniques based on liquid-solid extraction, the newest trends in the application of MOFs as sorbents in those techniques, and, most importantly, presents the reader with a summary, which a specific technique and MOF for the desired application. To make a tailor-made and well-informed choice as to the extraction technique.
AbstractList The preparation of samples for instrumental analysis is the most essential and time-consuming stage of the entire analytical process; it also has the greatest impact on the analysis results. Concentrating the sample, changing its matrix, and removing interferents are often necessary. Techniques for preparing samples for analysis are constantly being developed and modified to meet new challenges, facilitate work, and enable the determination of analytes in the most comprehensive concentration range possible. This paper focuses on using metal-organic frameworks (MOFs) as sorbents in the most popular techniques for preparing liquid samples for analysis, based on liquid-solid extraction. An increase in interest in MOFs-type materials has been observed for about 20 years, mainly due to their sorption properties, resulting, among others, from the high specific surface area, tunable pore size, and the theoretically wide possibility of their modification. This paper presents certain advantages and disadvantages of the most popular sample preparation techniques based on liquid-solid extraction, the newest trends in the application of MOFs as sorbents in those techniques, and, most importantly, presents the reader with a summary, which a specific technique and MOF for the desired application. To make a tailor-made and well-informed choice as to the extraction technique.
The preparation of samples for instrumental analysis is the most essential and time-consuming stage of the entire analytical process; it also has the greatest impact on the analysis results. Concentrating the sample, changing its matrix, and removing interferents are often necessary. Techniques for preparing samples for analysis are constantly being developed and modified to meet new challenges, facilitate work, and enable the determination of analytes in the most comprehensive concentration range possible. This paper focuses on using metal-organic frameworks (MOFs) as sorbents in the most popular techniques for preparing liquid samples for analysis, based on liquid-solid extraction. An increase in interest in MOFs-type materials has been observed for about 20 years, mainly due to their sorption properties, resulting, among others, from the high specific surface area, tunable pore size, and the theoretically wide possibility of their modification. This paper presents certain advantages and disadvantages of the most popular sample preparation techniques based on liquid-solid extraction, the newest trends in the application of MOFs as sorbents in those techniques, and, most importantly, presents the reader with a summary, which a specific technique and MOF for the desired application. To make a tailor-made and well-informed choice as to the extraction technique.The preparation of samples for instrumental analysis is the most essential and time-consuming stage of the entire analytical process; it also has the greatest impact on the analysis results. Concentrating the sample, changing its matrix, and removing interferents are often necessary. Techniques for preparing samples for analysis are constantly being developed and modified to meet new challenges, facilitate work, and enable the determination of analytes in the most comprehensive concentration range possible. This paper focuses on using metal-organic frameworks (MOFs) as sorbents in the most popular techniques for preparing liquid samples for analysis, based on liquid-solid extraction. An increase in interest in MOFs-type materials has been observed for about 20 years, mainly due to their sorption properties, resulting, among others, from the high specific surface area, tunable pore size, and the theoretically wide possibility of their modification. This paper presents certain advantages and disadvantages of the most popular sample preparation techniques based on liquid-solid extraction, the newest trends in the application of MOFs as sorbents in those techniques, and, most importantly, presents the reader with a summary, which a specific technique and MOF for the desired application. To make a tailor-made and well-informed choice as to the extraction technique.
Audience Academic
Author Nawała, Jakub
Popiel, Stanisław
Dziedzic, Daniel
Woźniak, Jakub
AuthorAffiliation Faculty of Advanced Technologies and Chemistry, Institute of Chemistry, Military University of Technology, Kaliskiego Str. 2, 00-908 Warsaw, Poland; jakub.wozniak.116@gmail.com (J.W.); jakub.nawala@wat.edu.pl (J.N.); daniel.dziedzic@wat.edu.pl (D.D.)
AuthorAffiliation_xml – name: Faculty of Advanced Technologies and Chemistry, Institute of Chemistry, Military University of Technology, Kaliskiego Str. 2, 00-908 Warsaw, Poland; jakub.wozniak.116@gmail.com (J.W.); jakub.nawala@wat.edu.pl (J.N.); daniel.dziedzic@wat.edu.pl (D.D.)
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  orcidid: 0000-0002-1662-5406
  surname: Woźniak
  fullname: Woźniak, Jakub
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  givenname: Jakub
  surname: Nawała
  fullname: Nawała, Jakub
– sequence: 3
  givenname: Daniel
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  surname: Dziedzic
  fullname: Dziedzic, Daniel
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  givenname: Stanisław
  orcidid: 0000-0001-5557-5061
  surname: Popiel
  fullname: Popiel, Stanisław
BackLink https://www.ncbi.nlm.nih.gov/pubmed/39407677$$D View this record in MEDLINE/PubMed
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Keywords matrix solid-phase dispersion (MSPD)
micro-solid-phase extraction (µ-SPE)
solid-phase microextraction (SPME)
pipette-tip solid-phase extraction (PT-SPE)
magnetic solid-phase extraction (MSPE)
metal-organic frameworks (MOFs)
stir-bar sorptive extraction (SBSE)
solid-phase extraction (SPE)
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Snippet The preparation of samples for instrumental analysis is the most essential and time-consuming stage of the entire analytical process; it also has the greatest...
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SubjectTerms Efficiency
Laboratories
Ligands
magnetic solid-phase extraction (MSPE)
metal-organic frameworks (MOFs)
micro-solid-phase extraction (µ-SPE)
pipette-tip solid-phase extraction (PT-SPE)
Porous materials
Review
solid-phase extraction (SPE)
solid-phase microextraction (SPME)
Sorbents
Zeolites
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Title Overview of Liquid Sample Preparation Techniques for Analysis, Using Metal-Organic Frameworks as Sorbents
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Volume 29
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