Immobilization mechanism of Se oxyanions in geopolymer: Effects of alkaline activators and calcined hydrotalcite additive

[Display omitted] •The immobilization of selenite and selenate in geopolymer was explored.•Two kinds of activators were used for geopolymer synthesis.•The effect of calcined hydrotalcite on the Se leaching was discussed.•Electrostatic interaction is the main association mode of selenium in geopolyme...

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Published inJournal of hazardous materials Vol. 387; p. 121994
Main Authors Tian, Quanzhi, Guo, Binglin, Sasaki, Keiko
Format Journal Article
LanguageEnglish
Published Netherlands Elsevier B.V 05.04.2020
Subjects
Activator
Calcined hydrotalcite
electrostatic interactions
Fourier transform infrared spectroscopy
Geopolymer
hydrotalcite
Immobilization
leaching
nitrogen
nuclear magnetic resonance spectroscopy
oxyanions
pollutants
polymers
selenates
Selenium
sodium hydroxide
thermogravimetry
X-ray diffraction
Calcined hydrotalcite
Immobilization
Geopolymer
Selenium
Activator
Online AccessGet full text
ISSN0304-3894
1873-3336
1873-3336
DOI10.1016/j.jhazmat.2019.121994

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Abstract [Display omitted] •The immobilization of selenite and selenate in geopolymer was explored.•Two kinds of activators were used for geopolymer synthesis.•The effect of calcined hydrotalcite on the Se leaching was discussed.•Electrostatic interaction is the main association mode of selenium in geopolymer.•Compactness of geopolymer plays a critical role in the immobilization of selenium. Geopolymers have been widely adopted to stabilize the cationic pollutants. However, few studies have focused on the immobilization of anionic species. In this study, the immobilization of SeO32– and SeO42– was explored for the first time using geopolymer activated by different alkaline solutions (NaOH and Na2SiO3) with and without calcined hydrotalcite (CHT), characterized by TCLP, XRD, FTIR, TG, NMR, XAFS, and N2 adsorption-desorption isotherm. Na2SiO3-activated geopolymers without CHT additive showed lower leaching percentages of SeO32– and SeO42– (approximately 10 % and 18 %) than NaOH-activated geopolymers (approximately 58 % and 74 %). It has been proven that electrostatic interaction is the main association mode of SeO32– and SeO42– in both NaOH- and Na2SiO3-activated geopolymers. Hence, compactness plays a vital role in the Se leaching from geopolymer. The addition of CHT reduced the compactnesses of both NaOH- and Na2SiO3-geopolymers. Due to the formation of hydrotalcite, the CHT additive contributed to immobilize SeO32– and SeO42– in NaOH-activated geopolymers. However, this phenomenon was not observed in Na2SiO3-activated geopolymers. Thus, the leaching amount of Se greatly increased from Na2SiO3-activated geopolymers with CHT additive. This study provides new insights on the application of geopolymer to immobilize anionic pollutants.
AbstractList Geopolymers have been widely adopted to stabilize the cationic pollutants. However, few studies have focused on the immobilization of anionic species. In this study, the immobilization of SeO₃²– and SeO₄²– was explored for the first time using geopolymer activated by different alkaline solutions (NaOH and Na₂SiO₃) with and without calcined hydrotalcite (CHT), characterized by TCLP, XRD, FTIR, TG, NMR, XAFS, and N₂ adsorption-desorption isotherm. Na₂SiO₃-activated geopolymers without CHT additive showed lower leaching percentages of SeO₃²– and SeO₄²– (approximately 10 % and 18 %) than NaOH-activated geopolymers (approximately 58 % and 74 %). It has been proven that electrostatic interaction is the main association mode of SeO₃²– and SeO₄²– in both NaOH- and Na₂SiO₃-activated geopolymers. Hence, compactness plays a vital role in the Se leaching from geopolymer. The addition of CHT reduced the compactnesses of both NaOH- and Na₂SiO₃-geopolymers. Due to the formation of hydrotalcite, the CHT additive contributed to immobilize SeO₃²– and SeO₄²– in NaOH-activated geopolymers. However, this phenomenon was not observed in Na₂SiO₃-activated geopolymers. Thus, the leaching amount of Se greatly increased from Na₂SiO₃-activated geopolymers with CHT additive. This study provides new insights on the application of geopolymer to immobilize anionic pollutants.
Geopolymers have been widely adopted to stabilize the cationic pollutants. However, few studies have focused on the immobilization of anionic species. In this study, the immobilization of SeO and SeO was explored for the first time using geopolymer activated by different alkaline solutions (NaOH and Na SiO ) with and without calcined hydrotalcite (CHT), characterized by TCLP, XRD, FTIR, TG, NMR, XAFS, and N adsorption-desorption isotherm. Na SiO -activated geopolymers without CHT additive showed lower leaching percentages of SeO and SeO (approximately 10 % and 18 %) than NaOH-activated geopolymers (approximately 58 % and 74 %). It has been proven that electrostatic interaction is the main association mode of SeO and SeO in both NaOH- and Na SiO -activated geopolymers. Hence, compactness plays a vital role in the Se leaching from geopolymer. The addition of CHT reduced the compactnesses of both NaOH- and Na SiO -geopolymers. Due to the formation of hydrotalcite, the CHT additive contributed to immobilize SeO and SeO in NaOH-activated geopolymers. However, this phenomenon was not observed in Na SiO -activated geopolymers. Thus, the leaching amount of Se greatly increased from Na SiO -activated geopolymers with CHT additive. This study provides new insights on the application of geopolymer to immobilize anionic pollutants.
Geopolymers have been widely adopted to stabilize the cationic pollutants. However, few studies have focused on the immobilization of anionic species. In this study, the immobilization of SeO32- and SeO42- was explored for the first time using geopolymer activated by different alkaline solutions (NaOH and Na2SiO3) with and without calcined hydrotalcite (CHT), characterized by TCLP, XRD, FTIR, TG, NMR, XAFS, and N2 adsorption-desorption isotherm. Na2SiO3-activated geopolymers without CHT additive showed lower leaching percentages of SeO32- and SeO42- (approximately 10 % and 18 %) than NaOH-activated geopolymers (approximately 58 % and 74 %). It has been proven that electrostatic interaction is the main association mode of SeO32- and SeO42- in both NaOH- and Na2SiO3-activated geopolymers. Hence, compactness plays a vital role in the Se leaching from geopolymer. The addition of CHT reduced the compactnesses of both NaOH- and Na2SiO3-geopolymers. Due to the formation of hydrotalcite, the CHT additive contributed to immobilize SeO32- and SeO42- in NaOH-activated geopolymers. However, this phenomenon was not observed in Na2SiO3-activated geopolymers. Thus, the leaching amount of Se greatly increased from Na2SiO3-activated geopolymers with CHT additive. This study provides new insights on the application of geopolymer to immobilize anionic pollutants.Geopolymers have been widely adopted to stabilize the cationic pollutants. However, few studies have focused on the immobilization of anionic species. In this study, the immobilization of SeO32- and SeO42- was explored for the first time using geopolymer activated by different alkaline solutions (NaOH and Na2SiO3) with and without calcined hydrotalcite (CHT), characterized by TCLP, XRD, FTIR, TG, NMR, XAFS, and N2 adsorption-desorption isotherm. Na2SiO3-activated geopolymers without CHT additive showed lower leaching percentages of SeO32- and SeO42- (approximately 10 % and 18 %) than NaOH-activated geopolymers (approximately 58 % and 74 %). It has been proven that electrostatic interaction is the main association mode of SeO32- and SeO42- in both NaOH- and Na2SiO3-activated geopolymers. Hence, compactness plays a vital role in the Se leaching from geopolymer. The addition of CHT reduced the compactnesses of both NaOH- and Na2SiO3-geopolymers. Due to the formation of hydrotalcite, the CHT additive contributed to immobilize SeO32- and SeO42- in NaOH-activated geopolymers. However, this phenomenon was not observed in Na2SiO3-activated geopolymers. Thus, the leaching amount of Se greatly increased from Na2SiO3-activated geopolymers with CHT additive. This study provides new insights on the application of geopolymer to immobilize anionic pollutants.
[Display omitted] •The immobilization of selenite and selenate in geopolymer was explored.•Two kinds of activators were used for geopolymer synthesis.•The effect of calcined hydrotalcite on the Se leaching was discussed.•Electrostatic interaction is the main association mode of selenium in geopolymer.•Compactness of geopolymer plays a critical role in the immobilization of selenium. Geopolymers have been widely adopted to stabilize the cationic pollutants. However, few studies have focused on the immobilization of anionic species. In this study, the immobilization of SeO32– and SeO42– was explored for the first time using geopolymer activated by different alkaline solutions (NaOH and Na2SiO3) with and without calcined hydrotalcite (CHT), characterized by TCLP, XRD, FTIR, TG, NMR, XAFS, and N2 adsorption-desorption isotherm. Na2SiO3-activated geopolymers without CHT additive showed lower leaching percentages of SeO32– and SeO42– (approximately 10 % and 18 %) than NaOH-activated geopolymers (approximately 58 % and 74 %). It has been proven that electrostatic interaction is the main association mode of SeO32– and SeO42– in both NaOH- and Na2SiO3-activated geopolymers. Hence, compactness plays a vital role in the Se leaching from geopolymer. The addition of CHT reduced the compactnesses of both NaOH- and Na2SiO3-geopolymers. Due to the formation of hydrotalcite, the CHT additive contributed to immobilize SeO32– and SeO42– in NaOH-activated geopolymers. However, this phenomenon was not observed in Na2SiO3-activated geopolymers. Thus, the leaching amount of Se greatly increased from Na2SiO3-activated geopolymers with CHT additive. This study provides new insights on the application of geopolymer to immobilize anionic pollutants.
ArticleNumber 121994
Author Tian, Quanzhi
Guo, Binglin
Sasaki, Keiko
Author_xml – sequence: 1
  givenname: Quanzhi
  orcidid: 0000-0001-7729-253X
  surname: Tian
  fullname: Tian, Quanzhi
  email: tianqz0502@foxmail.com
– sequence: 2
  givenname: Binglin
  orcidid: 0000-0002-9060-0872
  surname: Guo
  fullname: Guo, Binglin
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  givenname: Keiko
  surname: Sasaki
  fullname: Sasaki, Keiko
  email: keikos@mine.kyushu-u.ac.jp
BackLink https://www.ncbi.nlm.nih.gov/pubmed/31901840$$D View this record in MEDLINE/PubMed
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Keywords Calcined hydrotalcite
Immobilization
Geopolymer
Selenium
Activator
Language English
License Copyright © 2019 Elsevier B.V. All rights reserved.
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Snippet [Display omitted] •The immobilization of selenite and selenate in geopolymer was explored.•Two kinds of activators were used for geopolymer synthesis.•The...
Geopolymers have been widely adopted to stabilize the cationic pollutants. However, few studies have focused on the immobilization of anionic species. In this...
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StartPage 121994
SubjectTerms Activator
Calcined hydrotalcite
electrostatic interactions
Fourier transform infrared spectroscopy
Geopolymer
hydrotalcite
Immobilization
leaching
nitrogen
nuclear magnetic resonance spectroscopy
oxyanions
pollutants
polymers
selenates
Selenium
sodium hydroxide
thermogravimetry
X-ray diffraction
Title Immobilization mechanism of Se oxyanions in geopolymer: Effects of alkaline activators and calcined hydrotalcite additive
URI https://dx.doi.org/10.1016/j.jhazmat.2019.121994
https://www.ncbi.nlm.nih.gov/pubmed/31901840
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