Studies on epoxy blends modified with a hyperbranched polyester
Thermomechanical and rheological properties of epoxy blends modified with different percentages of a hyperbranched polymer have been reported. The addition of the hyperbranched modifier did not alter the rheological behavior of the blend. This effect is particularly advantageous for some composite m...
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| Published in | Polymer engineering and science Vol. 48; no. 12; pp. 2382 - 2388 |
|---|---|
| Main Authors | , |
| Format | Journal Article |
| Language | English |
| Published |
Hoboken
Wiley Subscription Services, Inc., A Wiley Company
01.12.2008
Wiley Society of Plastics Engineers, Inc Blackwell Publishing Ltd |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0032-3888 1548-2634 |
| DOI | 10.1002/pen.21192 |
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| Abstract | Thermomechanical and rheological properties of epoxy blends modified with different percentages of a hyperbranched polymer have been reported. The addition of the hyperbranched modifier did not alter the rheological behavior of the blend. This effect is particularly advantageous for some composite manufacturing techniques because it allows for the establishment of low viscosity during processing. Morphological development was studied under curing by hot stage microscopy. The cryo‐fractured surfaces of the cured samples were analyzed by scanning electron microscopy. The morphological analysis showed that the blends did not phase separate at any modifier percentage. This result was further supported by dynamic mechanical testing (DMTA) on cured samples. In fact, DMTA showed a single relaxation peak for all the formulations studied. The dynamic testing was also used to assess the damping properties of the systems. The blends of this study were also compared with similar systems modified with poly(ε‐caprolactone), which were the subjects of a previous article. POLYM. ENG. SCI., 2008. © 2008 Society of Plastics Engineers |
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| AbstractList | Thermomechanical and rheological properties of epoxy blends modified with different percentages of a hyperbranched polymer have been reported. The addition of the hyperbranched modifier did not alter the rheological behavior of the blend. This effect is particularly advantageous for some composite manufacturing techniques because it allows for the establishment of low viscosity during processing. Morphological development was studied under curing by hot stage microscopy. The cryo‐fractured surfaces of the cured samples were analyzed by scanning electron microscopy. The morphological analysis showed that the blends did not phase separate at any modifier percentage. This result was further supported by dynamic mechanical testing (DMTA) on cured samples. In fact, DMTA showed a single relaxation peak for all the formulations studied. The dynamic testing was also used to assess the damping properties of the systems. The blends of this study were also compared with similar systems modified with poly(ε‐caprolactone), which were the subjects of a previous article. POLYM. ENG. SCI., 2008. © 2008 Society of Plastics Engineers Thermomechanical and rheological properties of epoxy blends modified with different percentages of a hyper- branched polymer have been reported. The addition of the hyperbranched modifier did not alter the rheologi- cal behavior of the blend. This effect is particularly advantageous for some composite manufacturing techniques because it allows for the establishment of low viscosity during processing. Morphological de- velopment was studied under curing by hot stage microscopy. The cryo-fractured surfaces of the cured samples were analyzed by scanning electron micros- copy. The morphological analysis showed that the blends did not phase separate at any modifier percent- age. This result was further supported by dynamic mechanical testing (DMTA) on cured samples. In fact, DMTA showed a single relaxation peak for all the for- mulations studied. The dynamic testing was also used to assess the damping properties of the systems. The blends of this study were also compared with similar systems modified with poly(c-caprolactone), which were the subjects of a previous article. [PUBLICATION ABSTRACT] Thermomechanical and rheological properties of epoxy blends modified with different percentages of a hyperbranched polymer have been reported. The addition of the hyperbranched modifier did not alter the rheological behavior of the blend. This effect is particularly advantageous for some composite manufacturing techniques because it allows for the establishment of low viscosity during processing. Morphological development was studied under curing by hot stage microscopy. The cryo-fractured surfaces of the cured samples were analyzed by scanning electron microscopy. The morphological analysis showed that the blends did not phase separate at any modifier percentage. This result was further supported by dynamic mechanical testing (DMTA) on cured samples. In fact, DMTA showed a single relaxation peak for all the formulations studied. The dynamic testing was also used to assess the damping properties of the systems. The blends of this study were also compared with similar systems modified with poly(-caprolactone), which were the subjects of a previous article. POLYM. ENG. SCI., 2008. Thermechanical and rheological properties of epoxy blends modified with different percentages of a hyperbranched polymer have been reported. The addition of the hyperbranched modifier did not alter the rheological behavior of the blend. This effect is particularly advantageous for some composite manufacturing techniques because it allows for the establishment of low viscosity during processing. Morphological development was studied under curing by hot stage microscopy. The cryo-fractured surfaces of the cured samples were analyzed by scanning election microscopy. The morphological analysis showed that the blends did not phase separate at any modifier percentage. This result was further supported by dynamic mechanical testing (DMTA) on cured samples. In fact, DMTA showed a single relaxation peak for all the formulations studied. The dynamic testing was also used to assess the damping properties of the systems. The blends of this study were also compared with similar systems modified with poly (ζ-caprolactone), which were the subjects of a previous article. POLYM. ENG. SCI., 48:2382-2388, 2008. [C] 2008 society of plastics Engineers |
| Audience | Academic |
| Author | Cicala, G. Recca, G. |
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| Cites_doi | 10.1021/ba-1993-0233 10.1016/S0032-3861(98)00464-9 10.1002/pen.20447 10.1002/pen.20604 10.1016/j.compositesa.2007.08.009 10.1002/app.20678 10.1002/app.25285 10.1016/0032-3861(94)90703-X 10.1002/pen.760230411 10.1016/0032-3861(93)90051-B 10.1021/bk-1989-0395 10.1016/S0032-3861(00)00798-9 10.1016/S0266-3538(01)00022-7 10.1016/j.polymer.2005.10.142 10.1002/app.23275 10.1016/0032-3861(89)90107-9 10.1016/0032-3861(92)90110-I 10.1016/0032-3861(93)90251-5 10.1016/j.polymer.2005.04.051 10.1007/978-94-011-2932-9 10.1016/S0266-3538(00)00169-X 10.1016/0014-3057(92)90136-P 10.1002/(SICI)1097-4628(19991010)74:2<328::AID-APP14>3.0.CO;2-W 10.1002/pen.20242 10.1002/polb.1994.090320302 10.1201/9781482277739 10.1533/9781845695446 |
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| Keywords | Polymer blends Branched polymer Ester polymer Epoxy resin Composition effect Curing (plastics) Experimental study Lactone polymer Dynamic mechanical properties Morphology Aliphatic polymer Polycaprolactone Rheological properties |
| Language | English |
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| References_xml | – reference: D. Ratna, Polymer., 42, 4209( 2001). – reference: B. Ellis, Chemistry and Technology of Epoxy Resins, Blackie Academic & Professional, Glagow( 1993). – reference: J.D. Ferry, Viscoelastic Properties of Polymers, Wiley, New York ( 1970). – reference: Y. Ni and S. Zheng, Polymer., 46, 5828( 2005). – reference: M. Murali,D. Ratna,A.B. Samui, and B.C. Chakraborty, J.Appl. Polym. Sci., 103, 1723( 2007). – reference: C.B. Bucknall,C.M. Gomez, and I. Quintard, Polymer., 35, 353( 1994). – reference: G. Cicala,R. La Spina,S. Sturiale, and A. Recca, J. Appl. Polym. Sci., 101, 250( 2006). – reference: Y.C. Chern,S. M. Tseng, and K. H. Hsieh, J. Appl. Polym. Sci., 74, 328( 1999). – reference: D.J. Hourstone and J.M. Lane, Polymer., 33, 1379( 1992). – reference: T. Ohsako,K. Natura, and I. Nozue, Polymer., 34, 5080( 1993). – reference: E. Žagar,M. Žigon, and S. Podzimek, Polymer., 47, 166( 2006). – reference: C. Carfagna,V. Ambrogi,G. Cicala,A. Pollicino,A. 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| Snippet | Thermomechanical and rheological properties of epoxy blends modified with different percentages of a hyperbranched polymer have been reported. The addition of... Thermechanical and rheological properties of epoxy blends modified with different percentages of a hyperbranched polymer have been reported. The addition of... Thermomechanical and rheological properties of epoxy blends modified with different percentages of a hyper- branched polymer have been reported. The addition... |
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| SubjectTerms | Applied sciences Chemical properties Epoxy resins Exact sciences and technology Mechanical properties Polyesters Polymer industry, paints, wood Polymers Properties and testing Rheology Technology of polymers |
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| Title | Studies on epoxy blends modified with a hyperbranched polyester |
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