Antifouling, adsorption and reversible flux properties of zwitterionic grafted PVDF membrane prepared via physisorbed free radical polymerization
Zwitterionic monomer carboxybetaine methacrylate (CBMA) is well known as an excellent hydrophilic and ion adsorption material. Herein, we created a PCBMA layer on PVDF membrane surface via physisorbed free radical polymerization grafting technique (P-FFPG) to improve its hydrophilicity, antifouling...
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| Published in | Desalination Vol. 337; pp. 6 - 15 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Amsterdam
Elsevier B.V
01.03.2014
Elsevier |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0011-9164 1873-4464 |
| DOI | 10.1016/j.desal.2014.01.006 |
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| Abstract | Zwitterionic monomer carboxybetaine methacrylate (CBMA) is well known as an excellent hydrophilic and ion adsorption material. Herein, we created a PCBMA layer on PVDF membrane surface via physisorbed free radical polymerization grafting technique (P-FFPG) to improve its hydrophilicity, antifouling and inorganic salts separation property. The key factors of monomer concentration and reaction time which influence grafted density (GD) were investigated in the present work. Attenuated total reflectance-Fourier transform infrared spectroscopy (ATR-FTIR) confirmed that the CBMA monomer was grafted onto the membrane successfully. The surface chemistry composition was conducted via X-ray photoelectron spectroscopy (XPS). Scanning electron microscopy (SEM) analysis clearly showed that the PCBMA layer formed on the membrane surface, and its grafted degree increased with the monomer concentration. The water static contact measurement confirmed that modified PVDF membranes obtained stable enhanced hydrophilicity and superior water adsorption ability. The static protein adsorption at different pH showed a partly pH sensitivity and an improving antifouling ability almost in the whole pH range. The ultrafiltration experiments suggested that the anti-protein fouling of the grafted membranes was significantly improved. The modified membrane possessed a stable initial sodium chloride (NaCl) rejection ratio and reversible flux behavior.
•Modified PVDF membrane via free radical polymerization grafting technique•Great improvement for the hydrophilicity of modified membrane•The zwitterionic membrane exhibits excellent protein antifouling property.•The zwitterionic membrane showed high salt initial rejection ability.•The zwitterionic membrane possessed a reversible flux behavior. |
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| AbstractList | Zwitterionic monomer carboxybetaine methacrylate (CBMA) is well known as an excellent hydrophilic and ion adsorption material. Herein, we created a PCBMA layer on PVDF membrane surface via physisorbed free radical polymerization grafting technique (P-FFPG) to improve its hydrophilicity, antifouling and inorganic salts separation property. The key factors of monomer concentration and reaction time which influence grafted density (GD) were investigated in the present work. Attenuated total reflectance-Fourier transform infrared spectroscopy (ATR-FTIR) confirmed that the CBMA monomer was grafted onto the membrane successfully. The surface chemistry composition was conducted via X-ray photoelectron spectroscopy (XPS). Scanning electron microscopy (SEM) analysis clearly showed that the PCBMA layer formed on the membrane surface, and its grafted degree increased with the monomer concentration. The water static contact measurement confirmed that modified PVDF membranes obtained stable enhanced hydrophilicity and superior water adsorption ability. The static protein adsorption at different pH showed a partly pH sensitivity and an improving antifouling ability almost in the whole pH range. The ultrafiltration experiments suggested that the anti-protein fouling of the grafted membranes was significantly improved. The modified membrane possessed a stable initial sodium chloride (NaCl) rejection ratio and reversible flux behavior.
•Modified PVDF membrane via free radical polymerization grafting technique•Great improvement for the hydrophilicity of modified membrane•The zwitterionic membrane exhibits excellent protein antifouling property.•The zwitterionic membrane showed high salt initial rejection ability.•The zwitterionic membrane possessed a reversible flux behavior. Zwitterionic monomer carboxybetaine methacrylate (CBMA) is well known as an excellent hydrophilic and ion adsorption material. Herein, we created a PCBMA layer on PVDF membrane surface via physisorbed free radical polymerization grafting technique (P-FFPG) to improve its hydrophilicity, antifouling and inorganic salts separation property. The key factors of monomer concentration and reaction time which influence grafted density (GD) were investigated in the present work. Attenuated total reflectance-Fourier transform infrared spectroscopy (ATR-FTIR) confirmed that the CBMA monomer was grafted onto the membrane successfully. The surface chemistry composition was conducted via X-ray photoelectron spectroscopy (XPS). Scanning electron microscopy (SEM) analysis clearly showed that the PCBMA layer formed on the membrane surface, and its grafted degree increased with the monomer concentration. The water static contact measurement confirmed that modified PVDF membranes obtained stable enhanced hydrophilicity and superior water adsorption ability. The static protein adsorption at different pH showed a partly pH sensitivity and an improving antifouling ability almost in the whole pH range. The ultrafiltration experiments suggested that the anti-protein fouling of the grafted membranes was significantly improved. The modified membrane possessed a stable initial sodium chloride (NaCl) rejection ratio and reversible flux behavior. |
| Author | Zhou, Qing Li, Jian-Hua Zhang, Qi-Qing Yan, Bang-Feng Lei, Xiao-Ping |
| Author_xml | – sequence: 1 givenname: Qing surname: Zhou fullname: Zhou, Qing email: zq880520@126.com organization: Institute of Biomedical and Pharmaceutical Technology and College of Chemistry and Chemical Engineering, Fuzhou University, Fuzhou 350001, China – sequence: 2 givenname: Xiao-Ping surname: Lei fullname: Lei, Xiao-Ping organization: Institute of Biomedical and Pharmaceutical Technology and College of Chemistry and Chemical Engineering, Fuzhou University, Fuzhou 350001, China – sequence: 3 givenname: Jian-Hua surname: Li fullname: Li, Jian-Hua organization: Institute of Biomedical and Pharmaceutical Technology and College of Chemistry and Chemical Engineering, Fuzhou University, Fuzhou 350001, China – sequence: 4 givenname: Bang-Feng surname: Yan fullname: Yan, Bang-Feng organization: Institute of Biomedical and Pharmaceutical Technology and College of Chemistry and Chemical Engineering, Fuzhou University, Fuzhou 350001, China – sequence: 5 givenname: Qi-Qing surname: Zhang fullname: Zhang, Qi-Qing email: zhangqi_q@126.com organization: Institute of Biomedical and Pharmaceutical Technology and College of Chemistry and Chemical Engineering, Fuzhou University, Fuzhou 350001, China |
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| Keywords | Zwitterionic polymer Salt rejection PVDF membrane CBMA Antifouling Surface grafted Scanning electron microscopy Sensitivity analysis Fouling Density Grafting Rejection Membrane separation Free radical polymerization Ultrafiltration Adsorption pH Fourier-transformed infrared spectrometry Reflectance |
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| Snippet | Zwitterionic monomer carboxybetaine methacrylate (CBMA) is well known as an excellent hydrophilic and ion adsorption material. Herein, we created a PCBMA layer... |
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| SubjectTerms | Adsorption Antifouling Applied sciences CBMA Chemical engineering Exact sciences and technology Grafting Membrane separation (reverse osmosis, dialysis...) Membranes Monomers Organic polymers Physicochemistry of polymers Pollution Polymerization Polyvinylidene fluorides Preparation, kinetics, thermodynamics, mechanism and catalysts PVDF membrane Salt rejection Surface chemistry Surface grafted Zwitterionic polymer |
| Title | Antifouling, adsorption and reversible flux properties of zwitterionic grafted PVDF membrane prepared via physisorbed free radical polymerization |
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