Investigating the Fluid–Solid Interaction of Acid Nonionic Nanoemulsion with Carbonate Porous Media
The subject of rock–fluid interaction is important in cases where flow through porous media is occurring. One special case is when the fluid reacts with the porous matrix. In this case, the mass transfer and reaction rate control the dissolution pattern. This article aimed to study the interaction b...
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| Published in | Molecules Vol. 25; no. 6; p. 1475 |
|---|---|
| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Switzerland
MDPI AG
24.03.2020
MDPI |
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| Online Access | Get full text |
| ISSN | 1420-3049 1433-1373 1420-3049 1433-1373 |
| DOI | 10.3390/molecules25061475 |
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| Abstract | The subject of rock–fluid interaction is important in cases where flow through porous media is occurring. One special case is when the fluid reacts with the porous matrix. In this case, the mass transfer and reaction rate control the dissolution pattern. This article aimed to study the interaction between an acid nanoemulsion system and a carbonate porous media. Nanoemulsions were developed to retard the rock’s dissolution and to promote the formation of conductivity channels. Nanoemulsions were prepared using ALK100 (alkyl alcohol ethoxylate) and RNX110 (alkylphenol ethoxylate) (nonionic surfactants), sec-butanol (co-surfactant), xylene isomers (oil phase), and a solution of HCl (aqueous phase). The obtained systems were characterized in terms of surface tension, droplet diameter, and reactivity. X-ray fluorescence/diffraction (XRF/XRD) and X-ray microtomography (microCT) were performed on carbonate porous media samples treated with the acid systems in order to observe the effects of the fluid–rock interaction. The results showed that the acid nanoemulsion, presenting a low oil content formulation, showed the low surface tension and droplet size characteristic of nanoemulsions. It was experimentally verified that the reactivity in the nanoemulsion media was mass-transfer-retarded, and that the wormhole pattern was verified under the studied conditions. |
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| AbstractList | The subject of rock–fluid interaction is important in cases where flow through porous media is occurring. One special case is when the fluid reacts with the porous matrix. In this case, the mass transfer and reaction rate control the dissolution pattern. This article aimed to study the interaction between an acid nanoemulsion system and a carbonate porous media. Nanoemulsions were developed to retard the rock’s dissolution and to promote the formation of conductivity channels. Nanoemulsions were prepared using ALK100 (alkyl alcohol ethoxylate) and RNX110 (alkylphenol ethoxylate) (nonionic surfactants), sec-butanol (co-surfactant), xylene isomers (oil phase), and a solution of HCl (aqueous phase). The obtained systems were characterized in terms of surface tension, droplet diameter, and reactivity. X-ray fluorescence/diffraction (XRF/XRD) and X-ray microtomography (microCT) were performed on carbonate porous media samples treated with the acid systems in order to observe the effects of the fluid–rock interaction. The results showed that the acid nanoemulsion, presenting a low oil content formulation, showed the low surface tension and droplet size characteristic of nanoemulsions. It was experimentally verified that the reactivity in the nanoemulsion media was mass-transfer-retarded, and that the wormhole pattern was verified under the studied conditions. The subject of rock−fluid interaction is important in cases where flow through porous media is occurring. One special case is when the fluid reacts with the porous matrix. In this case, the mass transfer and reaction rate control the dissolution pattern. This article aimed to study the interaction between an acid nanoemulsion system and a carbonate porous media. Nanoemulsions were developed to retard the rock's dissolution and to promote the formation of conductivity channels. Nanoemulsions were prepared using ALK100 (alkyl alcohol ethoxylate) and RNX110 (alkylphenol ethoxylate) (nonionic surfactants), sec-butanol (co-surfactant), xylene isomers (oil phase), and a solution of HCl (aqueous phase). The obtained systems were characterized in terms of surface tension, droplet diameter, and reactivity. X-ray fluorescence/diffraction (XRF/XRD) and X-ray microtomography (microCT) were performed on carbonate porous media samples treated with the acid systems in order to observe the effects of the fluid−rock interaction. The results showed that the acid nanoemulsion, presenting a low oil content formulation, showed the low surface tension and droplet size characteristic of nanoemulsions. It was experimentally verified that the reactivity in the nanoemulsion media was mass-transfer-retarded, and that the wormhole pattern was verified under the studied conditions. The subject of rock-fluid interaction is important in cases where flow through porous media is occurring. One special case is when the fluid reacts with the porous matrix. In this case, the mass transfer and reaction rate control the dissolution pattern. This article aimed to study the interaction between an acid nanoemulsion system and a carbonate porous media. Nanoemulsions were developed to retard the rock's dissolution and to promote the formation of conductivity channels. Nanoemulsions were prepared using ALK100 (alkyl alcohol ethoxylate) and RNX110 (alkylphenol ethoxylate) (nonionic surfactants), sec-butanol (co-surfactant), xylene isomers (oil phase), and a solution of HCl (aqueous phase). The obtained systems were characterized in terms of surface tension, droplet diameter, and reactivity. X-ray fluorescence/diffraction (XRF/XRD) and X-ray microtomography (microCT) were performed on carbonate porous media samples treated with the acid systems in order to observe the effects of the fluid-rock interaction. The results showed that the acid nanoemulsion, presenting a low oil content formulation, showed the low surface tension and droplet size characteristic of nanoemulsions. It was experimentally verified that the reactivity in the nanoemulsion media was mass-transfer-retarded, and that the wormhole pattern was verified under the studied conditions.The subject of rock-fluid interaction is important in cases where flow through porous media is occurring. One special case is when the fluid reacts with the porous matrix. In this case, the mass transfer and reaction rate control the dissolution pattern. This article aimed to study the interaction between an acid nanoemulsion system and a carbonate porous media. Nanoemulsions were developed to retard the rock's dissolution and to promote the formation of conductivity channels. Nanoemulsions were prepared using ALK100 (alkyl alcohol ethoxylate) and RNX110 (alkylphenol ethoxylate) (nonionic surfactants), sec-butanol (co-surfactant), xylene isomers (oil phase), and a solution of HCl (aqueous phase). The obtained systems were characterized in terms of surface tension, droplet diameter, and reactivity. X-ray fluorescence/diffraction (XRF/XRD) and X-ray microtomography (microCT) were performed on carbonate porous media samples treated with the acid systems in order to observe the effects of the fluid-rock interaction. The results showed that the acid nanoemulsion, presenting a low oil content formulation, showed the low surface tension and droplet size characteristic of nanoemulsions. It was experimentally verified that the reactivity in the nanoemulsion media was mass-transfer-retarded, and that the wormhole pattern was verified under the studied conditions. |
| Author | Araújo, Elayne Andrade Aum, Yanne Katiussy Pereira Gurgel Castro Dantas, Tereza Neuma de Sousa, Talles Nóbrega Araújo, Edson de Andrade Lucas, Cláudio Regis dos Santos Aum, Pedro Tupã Pandava |
| AuthorAffiliation | 3 Chemical Engineering Department, Federal University of Amazonas—UFAM, Manaus 69080-900, Brazil; yanne@ufam.edu.br 2 Petroleum Science and Engineering Postgraduate Program, Federal University of Rio Grande do Norte—UFRN, Natal 59075-000, Brazil 4 Chemical Engineering Department, Federal University of Rio Grande do Norte—UFRN, Natal 59075-000, Brazil; terezaneuma1011@yahoo.com.br (T.N.d.C.D.); elaynea_@hotmail.com (E.A.A.); talles22@hotmail.com (T.N.S.) 1 Petroleum Engineering Faculty, Campus Salinópolis, Federal University of Pará—UFPA, Salinópolis 68721-000, Brazil; claudiolucaseq@yahoo.com.br (C.R.d.S.L.); edsonandradesp@gmail.com (E.d.A.A.) |
| AuthorAffiliation_xml | – name: 2 Petroleum Science and Engineering Postgraduate Program, Federal University of Rio Grande do Norte—UFRN, Natal 59075-000, Brazil – name: 3 Chemical Engineering Department, Federal University of Amazonas—UFAM, Manaus 69080-900, Brazil; yanne@ufam.edu.br – name: 1 Petroleum Engineering Faculty, Campus Salinópolis, Federal University of Pará—UFPA, Salinópolis 68721-000, Brazil; claudiolucaseq@yahoo.com.br (C.R.d.S.L.); edsonandradesp@gmail.com (E.d.A.A.) – name: 4 Chemical Engineering Department, Federal University of Rio Grande do Norte—UFRN, Natal 59075-000, Brazil; terezaneuma1011@yahoo.com.br (T.N.d.C.D.); elaynea_@hotmail.com (E.A.A.); talles22@hotmail.com (T.N.S.) |
| Author_xml | – sequence: 1 givenname: Cláudio Regis dos Santos orcidid: 0000-0001-5443-462X surname: Lucas fullname: Lucas, Cláudio Regis dos Santos – sequence: 2 givenname: Yanne Katiussy Pereira Gurgel orcidid: 0000-0002-8547-0241 surname: Aum fullname: Aum, Yanne Katiussy Pereira Gurgel – sequence: 3 givenname: Edson de Andrade surname: Araújo fullname: Araújo, Edson de Andrade – sequence: 4 givenname: Tereza Neuma de surname: Castro Dantas fullname: Castro Dantas, Tereza Neuma de – sequence: 5 givenname: Elayne Andrade surname: Araújo fullname: Araújo, Elayne Andrade – sequence: 6 givenname: Talles Nóbrega surname: Sousa fullname: Sousa, Talles Nóbrega – sequence: 7 givenname: Pedro Tupã Pandava orcidid: 0000-0002-2339-9865 surname: Aum fullname: Aum, Pedro Tupã Pandava |
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| CitedBy_id | crossref_primary_10_1080_10916466_2024_2304789 crossref_primary_10_3390_molecules25153385 crossref_primary_10_3390_en17112600 crossref_primary_10_1016_j_colsurfa_2022_129821 crossref_primary_10_1016_j_geoen_2023_212096 crossref_primary_10_1016_j_scitotenv_2024_174598 crossref_primary_10_1016_j_fuel_2020_120045 crossref_primary_10_1016_j_oceram_2023_100348 crossref_primary_10_1103_PhysRevLett_133_266202 crossref_primary_10_1080_10916466_2023_2252450 crossref_primary_10_1016_j_petrol_2020_108100 crossref_primary_10_1080_01932691_2021_1880932 crossref_primary_10_1016_j_fuel_2023_127806 |
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| Keywords | microCT imaging O/W acid nanoemulsion carbonate porous-media retarded reaction |
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| Snippet | The subject of rock–fluid interaction is important in cases where flow through porous media is occurring. One special case is when the fluid reacts with the... The subject of rock-fluid interaction is important in cases where flow through porous media is occurring. One special case is when the fluid reacts with the... The subject of rock−fluid interaction is important in cases where flow through porous media is occurring. One special case is when the fluid reacts with the... |
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| SubjectTerms | carbonate porous-media Emulsions - chemistry Energy Experiments Fluids microct imaging Microemulsions Nanoemulsions o/w acid nanoemulsion Permeability Porosity retarded reaction Surface-Active Agents - chemistry Surfactants X-Ray Microtomography |
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| Title | Investigating the Fluid–Solid Interaction of Acid Nonionic Nanoemulsion with Carbonate Porous Media |
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