Effect of gelatinization and additives on morphology and thermal behavior of corn starch/PVA blend films

► Starch/polyvinyl alcohol blend films were prepared by the solution casting method. ► The effects of gelatinization on the properties of the films were investigated. ► The effects of additives on the properties of the films were investigated. ► A conceptual model of hydrogen bonding interactions wa...

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Published inCarbohydrate polymers Vol. 90; no. 4; pp. 1595 - 1600
Main Authors Luo, Xuegang, Li, Jiwei, Lin, Xiaoyan
Format Journal Article
LanguageEnglish
Published Kidlington Elsevier Ltd 06.11.2012
Elsevier
Subjects
Additive
additives
Applied sciences
Biocompatible Materials - chemistry
Calorimetry, Differential Scanning
corn starch
Exact sciences and technology
Gelatin - chemistry
Gelatinization
glycerol
Glycerol - chemistry
Glycerol - pharmacology
Hydrogen Bonding
melting point
Microscopy, Electron, Scanning
Morphology
Natural polymers
Organic polymers
Physicochemistry of polymers
Polyvinyl alcohol
Polyvinyl Alcohol - chemistry
Properties and characterization
Solvents - chemistry
Solvents - pharmacology
Starch
Starch - chemistry
Starch and polysaccharides
Temperature
Thermal and thermodynamic properties
Thermal behavior
thermal properties
Thermogravimetry
urea
Urea - chemistry
Urea - pharmacology
Zea mays
Additive
Polyvinyl alcohol
Gelatinization
Starch
Morphology
Thermal behavior
Polymer blends
Glycerol
Experimental study
Corn starch
Heterogeneous mixture
Thermal stability
Transformation temperature
Intermolecular interaction
Polyvinylalcohol
Urea
Heat of transformation
Plasticizer
Oside polymer
Hydrogen bond
Online AccessGet full text
ISSN0144-8617
1879-1344
1879-1344
DOI10.1016/j.carbpol.2012.07.036

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Abstract ► Starch/polyvinyl alcohol blend films were prepared by the solution casting method. ► The effects of gelatinization on the properties of the films were investigated. ► The effects of additives on the properties of the films were investigated. ► A conceptual model of hydrogen bonding interactions was established. The blend films of ungelatinized and gelatinized starch/polyvinyl alcohol (PVA) were prepared with a solution casting method by the introduction of additives (glycerol/urea) or not. The phase morphologies and thermal behaviors of the blends were carefully analyzed. A droplet phase was observed in the blends containing ungelatinized starch and a laminated phase was observed in the blends containing gelatinized starch. For both ungelatinized and gelatinized starch/PVA blends, the melting temperature (Tm) (210–230°C) of PVA was detected, and the Tm of gelatinized starch/PVA blends was higher than that of the ungelatinized starch/PVA blends. Blend films containing 16.8wt% of glycerol or urea exhibited a decreased Tm. The introduction of additives (glycerol or urea) reduced the decomposition onset temperature of the blend films. These various morphologies and thermal behaviors could be attributed to the different hydrogen bonding interaction characteristics between starch and polyvinyl alcohol at different conditions.
AbstractList The blend films of ungelatinized and gelatinized starch/polyvinyl alcohol (PVA) were prepared with a solution casting method by the introduction of additives (glycerol/urea) or not. The phase morphologies and thermal behaviors of the blends were carefully analyzed. A droplet phase was observed in the blends containing ungelatinized starch and a laminated phase was observed in the blends containing gelatinized starch. For both ungelatinized and gelatinized starch/PVA blends, the melting temperature (Tₘ) (210–230°C) of PVA was detected, and the Tₘ of gelatinized starch/PVA blends was higher than that of the ungelatinized starch/PVA blends. Blend films containing 16.8wt% of glycerol or urea exhibited a decreased Tₘ. The introduction of additives (glycerol or urea) reduced the decomposition onset temperature of the blend films. These various morphologies and thermal behaviors could be attributed to the different hydrogen bonding interaction characteristics between starch and polyvinyl alcohol at different conditions.
The blend films of ungelatinized and gelatinized starch/polyvinyl alcohol (PVA) were prepared with a solution casting method by the introduction of additives (glycerol/urea) or not. The phase morphologies and thermal behaviors of the blends were carefully analyzed. A droplet phase was observed in the blends containing ungelatinized starch and a laminated phase was observed in the blends containing gelatinized starch. For both ungelatinized and gelatinized starch/PVA blends, the melting temperature (T(m)) (210-230 °C) of PVA was detected, and the T(m) of gelatinized starch/PVA blends was higher than that of the ungelatinized starch/PVA blends. Blend films containing 16.8 wt% of glycerol or urea exhibited a decreased T(m). The introduction of additives (glycerol or urea) reduced the decomposition onset temperature of the blend films. These various morphologies and thermal behaviors could be attributed to the different hydrogen bonding interaction characteristics between starch and polyvinyl alcohol at different conditions.
The blend films of ungelatinized and gelatinized starch/polyvinyl alcohol (PVA) were prepared with a solution casting method by the introduction of additives (glycerol/urea) or not. The phase morphologies and thermal behaviors of the blends were carefully analyzed. A droplet phase was observed in the blends containing ungelatinized starch and a laminated phase was observed in the blends containing gelatinized starch. For both ungelatinized and gelatinized starch/PVA blends, the melting temperature (T(m)) (210-230 °C) of PVA was detected, and the T(m) of gelatinized starch/PVA blends was higher than that of the ungelatinized starch/PVA blends. Blend films containing 16.8 wt% of glycerol or urea exhibited a decreased T(m). The introduction of additives (glycerol or urea) reduced the decomposition onset temperature of the blend films. These various morphologies and thermal behaviors could be attributed to the different hydrogen bonding interaction characteristics between starch and polyvinyl alcohol at different conditions.The blend films of ungelatinized and gelatinized starch/polyvinyl alcohol (PVA) were prepared with a solution casting method by the introduction of additives (glycerol/urea) or not. The phase morphologies and thermal behaviors of the blends were carefully analyzed. A droplet phase was observed in the blends containing ungelatinized starch and a laminated phase was observed in the blends containing gelatinized starch. For both ungelatinized and gelatinized starch/PVA blends, the melting temperature (T(m)) (210-230 °C) of PVA was detected, and the T(m) of gelatinized starch/PVA blends was higher than that of the ungelatinized starch/PVA blends. Blend films containing 16.8 wt% of glycerol or urea exhibited a decreased T(m). The introduction of additives (glycerol or urea) reduced the decomposition onset temperature of the blend films. These various morphologies and thermal behaviors could be attributed to the different hydrogen bonding interaction characteristics between starch and polyvinyl alcohol at different conditions.
► Starch/polyvinyl alcohol blend films were prepared by the solution casting method. ► The effects of gelatinization on the properties of the films were investigated. ► The effects of additives on the properties of the films were investigated. ► A conceptual model of hydrogen bonding interactions was established. The blend films of ungelatinized and gelatinized starch/polyvinyl alcohol (PVA) were prepared with a solution casting method by the introduction of additives (glycerol/urea) or not. The phase morphologies and thermal behaviors of the blends were carefully analyzed. A droplet phase was observed in the blends containing ungelatinized starch and a laminated phase was observed in the blends containing gelatinized starch. For both ungelatinized and gelatinized starch/PVA blends, the melting temperature (Tm) (210–230°C) of PVA was detected, and the Tm of gelatinized starch/PVA blends was higher than that of the ungelatinized starch/PVA blends. Blend films containing 16.8wt% of glycerol or urea exhibited a decreased Tm. The introduction of additives (glycerol or urea) reduced the decomposition onset temperature of the blend films. These various morphologies and thermal behaviors could be attributed to the different hydrogen bonding interaction characteristics between starch and polyvinyl alcohol at different conditions.
Author Lin, Xiaoyan
Li, Jiwei
Luo, Xuegang
Author_xml – sequence: 1
  givenname: Xuegang
  surname: Luo
  fullname: Luo, Xuegang
  email: lxg@swust.edu.cn, lxg-2007@163.com
  organization: Engineering Research Center of Biomass Materials, Ministry of Education, Southwest University of Science and Technology, Mianyang, Sichuan 621010, China
– sequence: 2
  givenname: Jiwei
  surname: Li
  fullname: Li, Jiwei
  organization: Engineering Research Center of Biomass Materials, Ministry of Education, Southwest University of Science and Technology, Mianyang, Sichuan 621010, China
– sequence: 3
  givenname: Xiaoyan
  surname: Lin
  fullname: Lin, Xiaoyan
  organization: Engineering Research Center of Biomass Materials, Ministry of Education, Southwest University of Science and Technology, Mianyang, Sichuan 621010, China
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Issue 4
Keywords Additive
Polyvinyl alcohol
Gelatinization
Starch
Morphology
Thermal behavior
Polymer blends
Glycerol
Experimental study
Corn starch
Heterogeneous mixture
Thermal stability
Transformation temperature
Intermolecular interaction
Polyvinylalcohol
Urea
Heat of transformation
Plasticizer
Oside polymer
Hydrogen bond
Language English
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CC BY 4.0
Crown Copyright © 2012. Published by Elsevier Ltd. All rights reserved.
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– name: Elsevier
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Snippet ► Starch/polyvinyl alcohol blend films were prepared by the solution casting method. ► The effects of gelatinization on the properties of the films were...
The blend films of ungelatinized and gelatinized starch/polyvinyl alcohol (PVA) were prepared with a solution casting method by the introduction of additives...
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SubjectTerms Additive
additives
Applied sciences
Biocompatible Materials - chemistry
Calorimetry, Differential Scanning
corn starch
Exact sciences and technology
Gelatin - chemistry
Gelatinization
glycerol
Glycerol - chemistry
Glycerol - pharmacology
Hydrogen Bonding
melting point
Microscopy, Electron, Scanning
Morphology
Natural polymers
Organic polymers
Physicochemistry of polymers
Polyvinyl alcohol
Polyvinyl Alcohol - chemistry
Properties and characterization
Solvents - chemistry
Solvents - pharmacology
Starch
Starch - chemistry
Starch and polysaccharides
Temperature
Thermal and thermodynamic properties
Thermal behavior
thermal properties
Thermogravimetry
urea
Urea - chemistry
Urea - pharmacology
Zea mays
Title Effect of gelatinization and additives on morphology and thermal behavior of corn starch/PVA blend films
URI https://dx.doi.org/10.1016/j.carbpol.2012.07.036
https://www.ncbi.nlm.nih.gov/pubmed/22944421
https://www.proquest.com/docview/1038070188
https://www.proquest.com/docview/2000034302
Volume 90
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