Tetraarylphosphonium Salts as Solubility-Control Groups: Phosphonium-Supported Triphenylphosphine and Azodicarboxylate Reagents
Predictable solubilities! Reagents supported on a tetraarylphosphonium group have solubilities that can be predicted. The reagents and their by‐products can be readily removed, recovered, and recycled after reaction by a precipitation/filtration sequence initiated by the addition of a low‐polarity s...
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Published in | Angewandte Chemie International Edition Vol. 45; no. 9; pp. 1415 - 1420 |
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Main Authors | , , |
Format | Journal Article |
Language | English |
Published |
Weinheim
WILEY-VCH Verlag
20.02.2006
WILEY‐VCH Verlag Wiley |
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Online Access | Get full text |
ISSN | 1433-7851 1521-3773 |
DOI | 10.1002/anie.200503599 |
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Abstract | Predictable solubilities! Reagents supported on a tetraarylphosphonium group have solubilities that can be predicted. The reagents and their by‐products can be readily removed, recovered, and recycled after reaction by a precipitation/filtration sequence initiated by the addition of a low‐polarity solvent, such as diethyl ether. Furthermore, the supported reagents are robust and exhibit reactivities similar to their parent compounds. |
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AbstractList | Predictable solubilities! Reagents supported on a tetraarylphosphonium group have solubilities that can be predicted. The reagents and their by‐products can be readily removed, recovered, and recycled after reaction by a precipitation/filtration sequence initiated by the addition of a low‐polarity solvent, such as diethyl ether. Furthermore, the supported reagents are robust and exhibit reactivities similar to their parent compounds. |
Author | Charette, André B. Boezio, Alessandro A. Poupon, Jean-Christophe |
Author_xml | – sequence: 1 givenname: Jean-Christophe surname: Poupon fullname: Poupon, Jean-Christophe organization: Département de Chimie, Université de Montréal, P.O. Box 6128, Station Downtown, Montréal, Québec H3C 3J7, Canada, Fax: (+1) 514-343-5900 – sequence: 2 givenname: Alessandro A. surname: Boezio fullname: Boezio, Alessandro A. organization: Département de Chimie, Université de Montréal, P.O. Box 6128, Station Downtown, Montréal, Québec H3C 3J7, Canada, Fax: (+1) 514-343-5900 – sequence: 3 givenname: André B. surname: Charette fullname: Charette, André B. email: andre.charette@umontreal.ca organization: Département de Chimie, Université de Montréal, P.O. Box 6128, Station Downtown, Montréal, Québec H3C 3J7, Canada, Fax: (+1) 514-343-5900 |
BackLink | https://www.ncbi.nlm.nih.gov/pubmed/16425329$$D View this record in MEDLINE/PubMed |
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Keywords | Wittig reaction ORGANIC-SYNTHESIS SOLUBLE POLYMERS RAPID PURIFICATION OLEFIN METATHESIS supported catalysts RUTHENIUM CARBENE COMPLEX FUNCTIONALIZED POLYMERS MITSUNOBU REACTION separation COMBINATORIAL SYNTHESIS RECOVERABLE CATALYSTS phosphonium ions phosphorus CHIRAL CATALYSTS |
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Notes | This work was supported by Valorisation-Recherche Québec (VRQ), Valorisation-Recherche s.e.c. (Univalor), and the Université de Montréal. A.A.B. is grateful to the NSERC (PGF B) and FCAR (B2) for postgraduate fellowships. istex:F0B1EF733CCDB233FE3E7D574B5F1D953B8709D9 ArticleID:ANIE200503599 ark:/67375/WNG-HR4DKXWM-1 This work was supported by Valorisation‐Recherche Québec (VRQ), Valorisation‐Recherche s.e.c. (Univalor), and the Université de Montréal. A.A.B. is grateful to the NSERC (PGF B) and FCAR (B2) for postgraduate fellowships. ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 23 |
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Snippet | Predictable solubilities! Reagents supported on a tetraarylphosphonium group have solubilities that can be predicted. The reagents and their by‐products can be... |
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SubjectTerms | Chemistry Chemistry, Multidisciplinary phosphonium ions phosphorus Physical Sciences Science & Technology separation supported catalysts Wittig reaction |
Title | Tetraarylphosphonium Salts as Solubility-Control Groups: Phosphonium-Supported Triphenylphosphine and Azodicarboxylate Reagents |
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