Development of a novel monolith frit-based solid-phase microextraction method for determination of hexanal and heptanal in human serum samples
In this paper, a polypropylene frit with porous network structure and high area‐to‐thickness ratio (4.8 mm diameter, 1.6 mm thickness, 20 mm pore size) was utilized as a mould of monolith. Poly(methacrylic acid‐ethlyene glycol dimethacrylate) (MAA‐EGDMA) monolith was in situ synthesized in the micro...
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| Published in | Journal of separation science Vol. 35; no. 5-6; pp. 713 - 720 |
|---|---|
| Main Authors | , , |
| Format | Journal Article |
| Language | English |
| Published |
Weinheim
Blackwell Publishing Ltd
01.03.2012
Wiley |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1615-9306 1615-9314 1615-9314 |
| DOI | 10.1002/jssc.201100908 |
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| Abstract | In this paper, a polypropylene frit with porous network structure and high area‐to‐thickness ratio (4.8 mm diameter, 1.6 mm thickness, 20 mm pore size) was utilized as a mould of monolith. Poly(methacrylic acid‐ethlyene glycol dimethacrylate) (MAA‐EGDMA) monolith was in situ synthesized in the micro‐channel of frit by photopolymerization. A monolith frit‐based solid‐phase microextraction method (SPME) was developed for the determination of hexanal and heptanal in serum samples by combining with high‐performance liquid chromatography. 2,4‐Dinitrophenylhydrazine (DNPH) as the derivatizing reagent was absorbed on a monolith frit, then its derivatization reaction with aldehydes and the absorption of formed hydrazones on the monolith disk occurred simultaneously. The condition parameters for polymerization, derivatization and extraction were optimized systematically. Under the optimum conditions, rigid structure, low back‐pressure and high column capacity were achieved for the monolith frit. The limits of detection for hexanal and heptanal were 1.86 and 1.38 nmol/L, respectively. The inter‐ and intra‐day relative standard deviations were less than 7.7% (n = 6). This method was applied successfully to aldehydes analysis in human serum samples. The method possesses advantages such as simplicity, efficiency, low cost and good biocompatibility. It provides an alternative approach for quantification of aldehydes in complex biological samples. |
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| AbstractList | In this paper, a polypropylene frit with porous network structure and high area‐to‐thickness ratio (4.8 mm diameter, 1.6 mm thickness, 20 mm pore size) was utilized as a mould of monolith. Poly(methacrylic acid‐ethlyene glycol dimethacrylate) (MAA‐EGDMA) monolith was in situ synthesized in the micro‐channel of frit by photopolymerization. A monolith frit‐based solid‐phase microextraction method (SPME) was developed for the determination of hexanal and heptanal in serum samples by combining with high‐performance liquid chromatography. 2,4‐Dinitrophenylhydrazine (DNPH) as the derivatizing reagent was absorbed on a monolith frit, then its derivatization reaction with aldehydes and the absorption of formed hydrazones on the monolith disk occurred simultaneously. The condition parameters for polymerization, derivatization and extraction were optimized systematically. Under the optimum conditions, rigid structure, low back‐pressure and high column capacity were achieved for the monolith frit. The limits of detection for hexanal and heptanal were 1.86 and 1.38 nmol/L, respectively. The inter‐ and intra‐day relative standard deviations were less than 7.7% (n = 6). This method was applied successfully to aldehydes analysis in human serum samples. The method possesses advantages such as simplicity, efficiency, low cost and good biocompatibility. It provides an alternative approach for quantification of aldehydes in complex biological samples. In this paper, a polypropylene frit with porous network structure and high area‐to‐thickness ratio (4.8 mm diameter, 1.6 mm thickness, 20 mm pore size) was utilized as a mould of monolith. Poly(methacrylic acid‐ethlyene glycol dimethacrylate) (MAA‐EGDMA) monolith was in situ synthesized in the micro‐channel of frit by photopolymerization. A monolith frit‐based solid‐phase microextraction method (SPME) was developed for the determination of hexanal and heptanal in serum samples by combining with high‐performance liquid chromatography. 2,4‐Dinitrophenylhydrazine (DNPH) as the derivatizing reagent was absorbed on a monolith frit, then its derivatization reaction with aldehydes and the absorption of formed hydrazones on the monolith disk occurred simultaneously. The condition parameters for polymerization, derivatization and extraction were optimized systematically. Under the optimum conditions, rigid structure, low back‐pressure and high column capacity were achieved for the monolith frit. The limits of detection for hexanal and heptanal were 1.86 and 1.38 nmol/L, respectively. The inter‐ and intra‐day relative standard deviations were less than 7.7% ( n = 6). This method was applied successfully to aldehydes analysis in human serum samples. The method possesses advantages such as simplicity, efficiency, low cost and good biocompatibility. It provides an alternative approach for quantification of aldehydes in complex biological samples. In this paper, a polypropylene frit with porous network structure and high area-to-thickness ratio (4.8 mm diameter, 1.6 mm thickness, 20 mm pore size) was utilized as a mould of monolith. Poly(methacrylic acid-ethlyene glycol dimethacrylate) (MAA-EGDMA) monolith was in situ synthesized in the micro-channel of frit by photopolymerization. A monolith frit-based solid-phase microextraction method (SPME) was developed for the determination of hexanal and heptanal in serum samples by combining with high-performance liquid chromatography. 2,4-Dinitrophenylhydrazine (DNPH) as the derivatizing reagent was absorbed on a monolith frit, then its derivatization reaction with aldehydes and the absorption of formed hydrazones on the monolith disk occurred simultaneously. The condition parameters for polymerization, derivatization and extraction were optimized systematically. Under the optimum conditions, rigid structure, low back-pressure and high column capacity were achieved for the monolith frit. The limits of detection for hexanal and heptanal were 1.86 and 1.38 nmol/L, respectively. The inter- and intra-day relative standard deviations were less than 7.7% (n = 6). This method was applied successfully to aldehydes analysis in human serum samples. The method possesses advantages such as simplicity, efficiency, low cost and good biocompatibility. It provides an alternative approach for quantification of aldehydes in complex biological samples.In this paper, a polypropylene frit with porous network structure and high area-to-thickness ratio (4.8 mm diameter, 1.6 mm thickness, 20 mm pore size) was utilized as a mould of monolith. Poly(methacrylic acid-ethlyene glycol dimethacrylate) (MAA-EGDMA) monolith was in situ synthesized in the micro-channel of frit by photopolymerization. A monolith frit-based solid-phase microextraction method (SPME) was developed for the determination of hexanal and heptanal in serum samples by combining with high-performance liquid chromatography. 2,4-Dinitrophenylhydrazine (DNPH) as the derivatizing reagent was absorbed on a monolith frit, then its derivatization reaction with aldehydes and the absorption of formed hydrazones on the monolith disk occurred simultaneously. The condition parameters for polymerization, derivatization and extraction were optimized systematically. Under the optimum conditions, rigid structure, low back-pressure and high column capacity were achieved for the monolith frit. The limits of detection for hexanal and heptanal were 1.86 and 1.38 nmol/L, respectively. The inter- and intra-day relative standard deviations were less than 7.7% (n = 6). This method was applied successfully to aldehydes analysis in human serum samples. The method possesses advantages such as simplicity, efficiency, low cost and good biocompatibility. It provides an alternative approach for quantification of aldehydes in complex biological samples. In this paper, a polypropylene frit with porous network structure and high area-to-thickness ratio (4.8 mm diameter, 1.6 mm thickness, 20 um pore size) was utilized as a mould of monolith. Poly(methacrylic acid-ethlyene glycol dimethacrylate) (MAA-EGDMA) monolith was in situ synthesized in the micro-channel of frit by photopolymerization. A monolith frit-based solid-phase microextraction method (SPME) was developed for the determination of hexanal and heptanal in serum samples by combining with high-performance liquid chromatography. 2,4-Dinitrophenylhydrazine (DNPH) as the deriva-tizing reagent was absorbed on a monolith frit, then its derivatization reaction with aldehydes and the absorption of formed hydrazones on the monolith disk occurred simultaneously. The condition parameters for polymerization, derivatization and extraction were optimized systematically. Under the optimum conditions, rigid structure, low back-pressure and high column capacity were achieved for the monolith frit. The limits of detection for hexanal and heptanal were 1.86 and 1.38 nmol/L, respectively. The inter- and intra-day relative standard deviations were less than 7.7% (n = 6). This method was applied successfully to aldehydes analysis in human serum samples. The method possesses advantages such as simplicity, efficiency, low cost and good biocompatibility. It provides an alternative approach for quantification of aldehydes in complex biological samples. |
| Author | Yan, Zhihua Xu, Hui Song, Dandan |
| Author_xml | – sequence: 1 givenname: Hui surname: Xu fullname: Xu, Hui email: huixu@mail.ccnu.edu.cn organization: Key Laboratory of Pesticide & Chemical Biology, Ministry of Education, College of Chemistry, Central China Normal University, Wuhan, P. R. China – sequence: 2 givenname: Zhihua surname: Yan fullname: Yan, Zhihua – sequence: 3 givenname: Dandan surname: Song fullname: Song, Dandan |
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| CitedBy_id | crossref_primary_10_1016_j_jpba_2018_06_052 crossref_primary_10_1016_j_snb_2019_04_065 crossref_primary_10_1039_c2ay25918d crossref_primary_10_1016_j_chroma_2013_11_041 crossref_primary_10_1016_j_talanta_2013_10_052 crossref_primary_10_1016_j_talanta_2015_01_003 crossref_primary_10_1089_ars_2019_7955 |
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| Keywords | Biological fluid Chemical analysis Lung cancer HPLC chromatography Solid-phase microextraction Derivatization Aldehydes Blood Chemical enrichment Surface structure Characterization Crosslinked copolymer Methacrylic acid copolymer Sample preparation Clinical biology Bronchus disease Serum analysis Adsorbent Quantitative analysis Photochemical copolymerization Trace analysis Human Lung disease Scanning electron microscopy Healthy subject Respiratory disease Aliphatic compound Propylene polymer Monolithic column Monolith frit Patient Malignant tumor Aldehyde High-performance liquid chromatography Solid phase microextraction Ultraviolet detector Morphology Preparation Blood serum Cancer |
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| Snippet | In this paper, a polypropylene frit with porous network structure and high area‐to‐thickness ratio (4.8 mm diameter, 1.6 mm thickness, 20 mm pore size) was... In this paper, a polypropylene frit with porous network structure and high area-to-thickness ratio (4.8 mm diameter, 1.6 mm thickness, 20 mm pore size) was... In this paper, a polypropylene frit with porous network structure and high area-to-thickness ratio (4.8 mm diameter, 1.6 mm thickness, 20 um pore size) was... |
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| SubjectTerms | Adsorption Aldehydes Aldehydes - blood Aldehydes - isolation & purification Aldehydes / Monolith frit / High-performance liquid chromatography / Serum analysis / Solid-phase microextraction Biological and medical sciences Chromatography, High Pressure Liquid Columnar structure Frit Human Humans Hydrazones Investigative techniques, diagnostic techniques (general aspects) Liquid chromatography Medical sciences Miscellaneous. Technology Pathology. Cytology. Biochemistry. Spectrometry. Miscellaneous investigative techniques Polymerization Polypropylenes - chemistry Serums Solid Phase Microextraction - instrumentation Solid Phase Microextraction - methods |
| Title | Development of a novel monolith frit-based solid-phase microextraction method for determination of hexanal and heptanal in human serum samples |
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