Paal–Knorr reaction catalyzed by metal–organic framework IRMOF-3 as an efficient and reusable heterogeneous catalyst

[Display omitted] ► IRMOF-3 was synthesized and characterized. ► IRMOF-3 was used as catalyst for the Paal–Knorr reaction. ► High conversions were achieved using catalytic amounts of the IRMOF-3. ► The catalyst could be reused. A highly porous metal–organic framework (IRMOF-3) was synthesized from t...

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Published inJournal of molecular catalysis. A, Chemical Vol. 363-364; pp. 178 - 185
Main Authors Phan, Nam T.S., Nguyen, Tung T., Luu, Quang H., Nguyen, Lien T.L.
Format Journal Article
LanguageEnglish
Published Amsterdam Elsevier B.V 01.11.2012
Elsevier
Subjects
atomic absorption spectrometry
Catalysis
catalysts
catalytic activity
Chemistry
Colloidal state and disperse state
Exact sciences and technology
Fourier transform infrared spectroscopy
General and physical chemistry
Heterogeneous catalyst
IRMOF-3
Metal–organic framework
nitrates
nitrogen
Paal–Knorr reaction
Porous materials
Recyclable
scanning electron microscopes
scanning electron microscopy
Surface physical chemistry
Theory of reactions, general kinetics. Catalysis. Nomenclature, chemical documentation, computer chemistry
thermogravimetry
transmission electron microscopy
X-ray diffraction
zinc
Metal–organic framework
Heterogeneous catalyst
Paal–Knorr reaction
IRMOF-3
Recyclable
Paal-Knorr reaction
Zinc nitrate
Porous material
Physisorption
Powder
Characterization
Degradation
Scanning microscope
Absorption
Amine
Metal organic framework
Scanning electron microscopy
Catalytic reaction
Transition element compounds
Reuse
Thermogravimetry
Nitrogen
Electron microscopy
Conversion
X ray diffraction
Infrared spectrometry
Heterogeneous catalysis
Transmission electron microscopy
Acids
Metal-organic framework
Spectrophotometry
Catalyst
Online AccessGet full text
ISSN1381-1169
1873-314X
DOI10.1016/j.molcata.2012.06.007

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Abstract [Display omitted] ► IRMOF-3 was synthesized and characterized. ► IRMOF-3 was used as catalyst for the Paal–Knorr reaction. ► High conversions were achieved using catalytic amounts of the IRMOF-3. ► The catalyst could be reused. A highly porous metal–organic framework (IRMOF-3) was synthesized from the reaction of zinc nitrate hexahydrate and 2-amino-1,4-benzenedicarboxylic acid by solvothermal method. Physical characterizations of the material were achieved by using a variety of different techniques, including X-ray powder diffraction (XRD), scanning electron microscope (SEM), transmission electron microscopy (TEM), thermogravimetric analysis (TGA), Fourier transform infrared (FT-IR), atomic absorption spectrophotometry (AAS), and nitrogen physisorption measurements. The IRMOF-3 was used as an efficient heterogeneous catalyst for the Paal–Knorr reaction of benzyl amine with 2,5-hexanedione. Excellent conversions were obtained under mild conditions in the presence of 3mol% catalyst. The IRMOF-3 catalyst could be reused several times without a significant degradation in catalytic activity.
AbstractList A highly porous metal–organic framework (IRMOF-3) was synthesized from the reaction of zinc nitrate hexahydrate and 2-amino-1,4-benzenedicarboxylic acid by solvothermal method. Physical characterizations of the material were achieved by using a variety of different techniques, including X-ray powder diffraction (XRD), scanning electron microscope (SEM), transmission electron microscopy (TEM), thermogravimetric analysis (TGA), Fourier transform infrared (FT-IR), atomic absorption spectrophotometry (AAS), and nitrogen physisorption measurements. The IRMOF-3 was used as an efficient heterogeneous catalyst for the Paal–Knorr reaction of benzyl amine with 2,5-hexanedione. Excellent conversions were obtained under mild conditions in the presence of 3mol% catalyst. The IRMOF-3 catalyst could be reused several times without a significant degradation in catalytic activity.
[Display omitted] ► IRMOF-3 was synthesized and characterized. ► IRMOF-3 was used as catalyst for the Paal–Knorr reaction. ► High conversions were achieved using catalytic amounts of the IRMOF-3. ► The catalyst could be reused. A highly porous metal–organic framework (IRMOF-3) was synthesized from the reaction of zinc nitrate hexahydrate and 2-amino-1,4-benzenedicarboxylic acid by solvothermal method. Physical characterizations of the material were achieved by using a variety of different techniques, including X-ray powder diffraction (XRD), scanning electron microscope (SEM), transmission electron microscopy (TEM), thermogravimetric analysis (TGA), Fourier transform infrared (FT-IR), atomic absorption spectrophotometry (AAS), and nitrogen physisorption measurements. The IRMOF-3 was used as an efficient heterogeneous catalyst for the Paal–Knorr reaction of benzyl amine with 2,5-hexanedione. Excellent conversions were obtained under mild conditions in the presence of 3mol% catalyst. The IRMOF-3 catalyst could be reused several times without a significant degradation in catalytic activity.
Author Phan, Nam T.S.
Luu, Quang H.
Nguyen, Lien T.L.
Nguyen, Tung T.
Author_xml – sequence: 1
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  fullname: Phan, Nam T.S.
  email: ptsnam@hcmut.edu.vn, ptsnam@yahoo.com, ptsnam@gmail.com
– sequence: 2
  givenname: Tung T.
  surname: Nguyen
  fullname: Nguyen, Tung T.
– sequence: 3
  givenname: Quang H.
  surname: Luu
  fullname: Luu, Quang H.
– sequence: 4
  givenname: Lien T.L.
  surname: Nguyen
  fullname: Nguyen, Lien T.L.
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Keywords Metal–organic framework
Heterogeneous catalyst
Paal–Knorr reaction
IRMOF-3
Recyclable
Paal-Knorr reaction
Zinc nitrate
Porous material
Physisorption
Powder
Characterization
Degradation
Scanning microscope
Absorption
Amine
Metal organic framework
Scanning electron microscopy
Catalytic reaction
Transition element compounds
Reuse
Thermogravimetry
Nitrogen
Electron microscopy
Conversion
X ray diffraction
Infrared spectrometry
Heterogeneous catalysis
Transmission electron microscopy
Acids
Metal-organic framework
Spectrophotometry
Catalyst
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SSID ssj0004341
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Snippet [Display omitted] ► IRMOF-3 was synthesized and characterized. ► IRMOF-3 was used as catalyst for the Paal–Knorr reaction. ► High conversions were achieved...
A highly porous metal–organic framework (IRMOF-3) was synthesized from the reaction of zinc nitrate hexahydrate and 2-amino-1,4-benzenedicarboxylic acid by...
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SubjectTerms atomic absorption spectrometry
Catalysis
catalysts
catalytic activity
Chemistry
Colloidal state and disperse state
Exact sciences and technology
Fourier transform infrared spectroscopy
General and physical chemistry
Heterogeneous catalyst
IRMOF-3
Metal–organic framework
nitrates
nitrogen
Paal–Knorr reaction
Porous materials
Recyclable
scanning electron microscopes
scanning electron microscopy
Surface physical chemistry
Theory of reactions, general kinetics. Catalysis. Nomenclature, chemical documentation, computer chemistry
thermogravimetry
transmission electron microscopy
X-ray diffraction
zinc
Title Paal–Knorr reaction catalyzed by metal–organic framework IRMOF-3 as an efficient and reusable heterogeneous catalyst
URI https://dx.doi.org/10.1016/j.molcata.2012.06.007
https://www.proquest.com/docview/1733559324
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