Ultrasonic-assisted condensation of chitosan with salicylaldehyde
In order to synthesize an improved adsorbent for heavy metal ions, we studied the condensation reaction of chitosan with salicylaldehyde in ethanol to form a Schiff base. The effect irradiating the reaction using an ultrasonic liquid processor was contrasted with conventional methods. The IR spectra...
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| Published in | Chinese journal of oceanology and limnology Vol. 27; no. 4; pp. 882 - 886 |
|---|---|
| Main Author | |
| Format | Journal Article |
| Language | English |
| Published |
Heidelberg
SP Science Press
01.11.2009
Springer Nature B.V Light Industry & Chemical Engineering Research Institute,South China University of Technology,Guangzhou 510640,China |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0254-4059 2096-5508 1993-5005 2523-3521 |
| DOI | 10.1007/s00343-009-9204-1 |
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| Abstract | In order to synthesize an improved adsorbent for heavy metal ions, we studied the condensation reaction of chitosan with salicylaldehyde in ethanol to form a Schiff base. The effect irradiating the reaction using an ultrasonic liquid processor was contrasted with conventional methods. The IR spectra of condensed chitosan prepared by the two methods showed that their molecular structures were identical. The reaction conditions, including solvents, ultrasonic power density and irradiation time, pH, and reactant ratio, were optimized by orthogonal design. A shorter reaction time and a higher product yield were obtained using ultrasonic-assisted synthesis compared with the traditional method. A condensation degree of 89.63% was achieved using the optimized conditions： i.e. ultrasonic irradiation at 180 W for 60 min; 95% ethanol as the solvent, pH 4.0, and salicylaldehyde：chitosan ratio of 6：1. |
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| AbstractList | In order to synthesize an improved adsorbent for heavy metal ions, we studied the condensation reaction of chitosan with salicylaldehyde in ethanol to form a Schiff base. The effect irradiating the reaction using an ultrasonic liquid processor was contrasted with conventional methods. The IR spectra of condensed chitosan prepared by the two methods showed that their molecular structures were identical. The reaction conditions, including solvents, ultrasonic power density and irradiation time, pH, and reactant ratio, were optimized by orthogonal design. A shorter reaction time and a higher product yield were obtained using ultrasonic-assisted synthesis compared with the traditional method. A condensation degree of 89.63% was achieved using the optimized conditions: i.e. ultrasonic irradiation at 180 W for 60 min; 95% ethanol as the solvent, pH 4.0, and salicylaldehyde:chitosan ratio of 6:1. [PUBLICATION ABSTRACT] In order to synthesize an improved adsorbent for heavy metal ions, we studied the condensation reaction of chitosan with salicylaldehyde in ethanol to form a Schiff base. The effect irradiating the reaction using an ultrasonic liquid processor was contrasted with conventional methods. The IR spectra of condensed chitosan prepared by the two methods showed that their molecular structures were identical. The reaction conditions, including solvents, ultrasonic power density and irradiation time, pH, and reactant ratio, were optimized by orthogonal design. A shorter reaction time and a higher product yield were obtained using ultrasonic-assisted synthesis compared with the traditional method. A condensation degree of 89.63% was achieved using the optimized conditions: i.e. ultrasonic irradiation at 180 W for 60 min; 95% ethanol as the solvent, pH 4.0, and salicylaldehyde:chitosan ratio of 6:1. In order to synthesize an improved adsorbent for heavy metal ions, we studied the condensation reaction of chitosan with salicylaldehyde in ethanol to form a Schiff base. The effect irradiating the reaction using an ultrasonic liquid processor was contrasted with conventional methods. The IR spectra of condensed chitosan prepared by the two methods showed that their molecular structures were identical. The reaction conditions, including solvents, ultrasonic power density and irradiation time, pH, and reactant ratio, were optimized by orthogonal design. A shorter reaction time and a higher product yield were obtained using ultrasonic-assisted synthesis compared with the traditional method. A condensation degree of 89.63% was achieved using the optimized conditions： i.e. ultrasonic irradiation at 180 W for 60 min; 95% ethanol as the solvent, pH 4.0, and salicylaldehyde：chitosan ratio of 6：1. P7; In order to synthesize an improved adsorbent for heavy metal ions, we studied the condensation reaction of chitosan with salicylaldehyde in ethanol to form a Schiff base. The effect irradiating the reaction using an ultrasonic liquid processor was contrasted with conventional methods. The IR spectra of condensed chitosan prepared by the two methods showed that their molecular structures were identical. The reaction conditions, including solvents, ultrasonic power density and irradiation time, pH, and reactant ratio, were optimized by orthogonal design. A shorter reaction time and a higher product yield were obtained using ultrasonic-assisted synthesis compared with the traditional method. A condensation degree of 89.63% was achieved using the optimized conditions: i.e. ultrasonic irradiation at 180 W for 60 min; 95% ethanol as the solvent, pH 4.0, and salicylaldehyde:chitosan ratio of 6:1. |
| Author | 段丽红 郭祀远 杨晋青 叶盛权 王兆梅 肖凯军 郑必胜 |
| AuthorAffiliation | Light Industry ＆ Chemical Engineering Research Institute, South China University of Technology, Guangzhou 510640, China |
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| CitedBy_id | crossref_primary_10_1016_j_jtice_2022_104354 crossref_primary_10_1007_s00343_017_6074_9 crossref_primary_10_1016_j_ijbiomac_2015_08_063 crossref_primary_10_1016_j_arabjc_2023_105317 crossref_primary_10_1016_j_carres_2023_109002 |
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| Copyright | Chinese Society for Oceanology and Limnology, Science Press and Springer Berlin Heidelberg 2009 Chinese Society for Oceanology and Limnology, Science Press and Springer Berlin Heidelberg 2009. Copyright © Wanfang Data Co. Ltd. All Rights Reserved. |
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| SubjectTerms | Adsorption Biochemistry Chemical engineering Chitosan Condensates Condensation Design optimization Earth and Environmental Science Earth Sciences Ethanol Heavy metals Imines Infrared spectroscopy Irradiation Metal ions Metals Microprocessors Molecular structure Oceanography Radiation Solvents 传统方法 壳聚糖 水杨醛 照射时间 缩合反应 超声波照射 辅助合成 重金属离子 |
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| Title | Ultrasonic-assisted condensation of chitosan with salicylaldehyde |
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