Using second-order calibration method based on trilinear decomposition algorithms coupled with high performance liquid chromatography with diode array detector for determination of quinolones in honey samples

A novel strategy that combines the second-order calibration method based on the trilinear decomposition algorithms with high performance liquid chromatography with diode array detector (HPLC-DAD) was developed to mathematically separate the overlapped peaks and to quantify quinolones in honey sample...

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Published in	Talanta (Oxford) Vol. 85; no. 3; pp. 1549 - 1559
Main Authors	Yu, Yong-Jie, Wu, Hai-Long, Shao, Sheng-Zhi, Kang, Chao, Zhao, Juan, Wang, Yu, Zhu, Shao-Hua, Yu, Ru-Qin
Format	Journal Article
Language	English
Published	Amsterdam Elsevier B.V 15.09.2011 Elsevier
Subjects	Algorithms Analytical chemistry Calibration Chemistry Chromatographic methods and physical methods associated with chromatography Chromatography, High Pressure Liquid - instrumentation Chromatography, High Pressure Liquid - methods Exact sciences and technology General, instrumentation High performance liquid chromatography honey Honey - analysis Honey samples Molecular Structure multiresidue analysis Other chromatographic methods Quinolones Quinolones - analysis Quinolones - chemistry Reproducibility of Results Second-order calibration Trilinear decomposition Honey samples Trilinear decomposition High performance liquid chromatography Second-order calibration Quinolones Performance evaluation Second order Sample HPLC chromatography Instrumentation Time Calibration Method Algorithm Honey Residue Chemical decomposition Diode array Strategy Peak Limit Sensor array Figure of merit Quantitative analysis
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ISSN	0039-9140 1873-3573 1873-3573
DOI	10.1016/j.talanta.2011.06.044

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Abstract	A novel strategy that combines the second-order calibration method based on the trilinear decomposition algorithms with high performance liquid chromatography with diode array detector (HPLC-DAD) was developed to mathematically separate the overlapped peaks and to quantify quinolones in honey samples. The HPLC-DAD data were obtained within a short time in isocratic mode. The developed method could be applied to determine 12 quinolones at the same time even in the presence of uncalibrated interfering components in complex background. To access the performance of the proposed strategy for the determination of quinolones in honey samples, the figures of merit were employed. The limits of quantitation for all analytes were within the range 1.2–56.7μgkg−1. The work presented in this paper illustrated the suitability and interesting potential of combining second-order calibration method with second-order analytical instrument for multi-residue analysis in honey samples.
AbstractList	A novel strategy that combines the second-order calibration method based on the trilinear decomposition algorithms with high performance liquid chromatography with diode array detector (HPLC-DAD) was developed to mathematically separate the overlapped peaks and to quantify quinolones in honey samples. The HPLC-DAD data were obtained within a short time in isocratic mode. The developed method could be applied to determine 12 quinolones at the same time even in the presence of uncalibrated interfering components in complex background. To access the performance of the proposed strategy for the determination of quinolones in honey samples, the figures of merit were employed. The limits of quantitation for all analytes were within the range 1.2–56.7μgkg⁻¹. The work presented in this paper illustrated the suitability and interesting potential of combining second-order calibration method with second-order analytical instrument for multi-residue analysis in honey samples. A novel strategy that combines the second-order calibration method based on the trilinear decomposition algorithms with high performance liquid chromatography with diode array detector (HPLC-DAD) was developed to mathematically separate the overlapped peaks and to quantify quinolones in honey samples. The HPLC-DAD data were obtained within a short time in isocratic mode. The developed method could be applied to determine 12 quinolones at the same time even in the presence of uncalibrated interfering components in complex background. To access the performance of the proposed strategy for the determination of quinolones in honey samples, the figures of merit were employed. The limits of quantitation for all analytes were within the range 1.2–56.7μgkg−1. The work presented in this paper illustrated the suitability and interesting potential of combining second-order calibration method with second-order analytical instrument for multi-residue analysis in honey samples. A novel strategy that combines the second-order calibration method based on the trilinear decomposition algorithms with high performance liquid chromatography with diode array detector (HPLC-DAD) was developed to mathematically separate the overlapped peaks and to quantify quinolones in honey samples. The HPLC-DAD data were obtained within a short time in isocratic mode. The developed method could be applied to determine 12 quinolones at the same time even in the presence of uncalibrated interfering components in complex background. To access the performance of the proposed strategy for the determination of quinolones in honey samples, the figures of merit were employed. The limits of quantitation for all analytes were within the range 1.2-56.7 μg kg(-1). The work presented in this paper illustrated the suitability and interesting potential of combining second-order calibration method with second-order analytical instrument for multi-residue analysis in honey samples.A novel strategy that combines the second-order calibration method based on the trilinear decomposition algorithms with high performance liquid chromatography with diode array detector (HPLC-DAD) was developed to mathematically separate the overlapped peaks and to quantify quinolones in honey samples. The HPLC-DAD data were obtained within a short time in isocratic mode. The developed method could be applied to determine 12 quinolones at the same time even in the presence of uncalibrated interfering components in complex background. To access the performance of the proposed strategy for the determination of quinolones in honey samples, the figures of merit were employed. The limits of quantitation for all analytes were within the range 1.2-56.7 μg kg(-1). The work presented in this paper illustrated the suitability and interesting potential of combining second-order calibration method with second-order analytical instrument for multi-residue analysis in honey samples. A novel strategy that combines the second-order calibration method based on the trilinear decomposition algorithms with high performance liquid chromatography with diode array detector (HPLC-DAD) was developed to mathematically separate the overlapped peaks and to quantify quinolones in honey samples. The HPLC-DAD data were obtained within a short time in isocratic mode. The developed method could be applied to determine 12 quinolones at the same time even in the presence of uncalibrated interfering components in complex background. To access the performance of the proposed strategy for the determination of quinolones in honey samples, the figures of merit were employed. The limits of quantitation for all analytes were within the range 1.2-56.7 μg kg(-1). The work presented in this paper illustrated the suitability and interesting potential of combining second-order calibration method with second-order analytical instrument for multi-residue analysis in honey samples.
Author	Yu, Ru-Qin Wang, Yu Wu, Hai-Long Zhao, Juan Zhu, Shao-Hua Kang, Chao Shao, Sheng-Zhi Yu, Yong-Jie
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Keywords	Honey samples Trilinear decomposition High performance liquid chromatography Second-order calibration Quinolones Performance evaluation Second order Sample HPLC chromatography Instrumentation Time Calibration Method Algorithm Honey Residue Chemical decomposition Diode array Strategy Peak Limit Sensor array Figure of merit Quantitative analysis
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SubjectTerms	Algorithms Analytical chemistry Calibration Chemistry Chromatographic methods and physical methods associated with chromatography Chromatography, High Pressure Liquid - instrumentation Chromatography, High Pressure Liquid - methods Exact sciences and technology General, instrumentation High performance liquid chromatography honey Honey - analysis Honey samples Molecular Structure multiresidue analysis Other chromatographic methods Quinolones Quinolones - analysis Quinolones - chemistry Reproducibility of Results Second-order calibration Trilinear decomposition
Title	Using second-order calibration method based on trilinear decomposition algorithms coupled with high performance liquid chromatography with diode array detector for determination of quinolones in honey samples
URI	https://dx.doi.org/10.1016/j.talanta.2011.06.044 https://www.ncbi.nlm.nih.gov/pubmed/21807221 https://www.proquest.com/docview/1710238997 https://www.proquest.com/docview/880998301
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