Electro-synthesis of ammonia from nitrogen at ambient temperature and pressure in ionic liquids
Ammonia as the source of most fertilizers has become one of the most important chemicals globally. It also is being increasingly considered as an easily transported carrier of hydrogen energy that can be generated from "stranded" renewable-energy resources. However, the traditional Haber-B...
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| Published in | Energy & environmental science Vol. 1; no. 12; pp. 2516 - 252 |
|---|---|
| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Cambridge
Royal Society of Chemistry
01.01.2017
|
| Subjects | |
| Online Access | Get full text |
| ISSN | 1754-5692 1754-5706 |
| DOI | 10.1039/c7ee02716h |
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| Abstract | Ammonia as the source of most fertilizers has become one of the most important chemicals globally. It also is being increasingly considered as an easily transported carrier of hydrogen energy that can be generated from "stranded" renewable-energy resources. However, the traditional Haber-Bosch process for the production of ammonia from atmospheric nitrogen and fossil fuels is a high temperature and pressure process that is energy intensive, currently producing more than 1.6% of global CO
2
emissions. An ambient temperature, electrochemical synthesis of ammonia is an attractive alternative approach, but has, to date, not been achieved at high efficiency. We report in this work the use of ionic liquids that have high N
2
solubility as electrolytes to achieve high conversion efficiency of 60% for N
2
electro-reduction to ammonia on a nanostructured iron catalyst under ambient conditions.
High faradaic efficiency reduction of N
2
to NH
3
is achieved in ionic liquid media under ambient conditions. |
|---|---|
| AbstractList | Ammonia as the source of most fertilizers has become one of the most important chemicals globally. It also is being increasingly considered as an easily transported carrier of hydrogen energy that can be generated from “stranded” renewable-energy resources. However, the traditional Haber–Bosch process for the production of ammonia from atmospheric nitrogen and fossil fuels is a high temperature and pressure process that is energy intensive, currently producing more than 1.6% of global CO
2
emissions. An ambient temperature, electrochemical synthesis of ammonia is an attractive alternative approach, but has, to date, not been achieved at high efficiency. We report in this work the use of ionic liquids that have high N
2
solubility as electrolytes to achieve high conversion efficiency of 60% for N
2
electro-reduction to ammonia on a nanostructured iron catalyst under ambient conditions. Ammonia as the source of most fertilizers has become one of the most important chemicals globally. It also is being increasingly considered as an easily transported carrier of hydrogen energy that can be generated from "stranded" renewable-energy resources. However, the traditional Haber-Bosch process for the production of ammonia from atmospheric nitrogen and fossil fuels is a high temperature and pressure process that is energy intensive, currently producing more than 1.6% of global CO 2 emissions. An ambient temperature, electrochemical synthesis of ammonia is an attractive alternative approach, but has, to date, not been achieved at high efficiency. We report in this work the use of ionic liquids that have high N 2 solubility as electrolytes to achieve high conversion efficiency of 60% for N 2 electro-reduction to ammonia on a nanostructured iron catalyst under ambient conditions. High faradaic efficiency reduction of N 2 to NH 3 is achieved in ionic liquid media under ambient conditions. Ammonia as the source of most fertilizers has become one of the most important chemicals globally. It also is being increasingly considered as an easily transported carrier of hydrogen energy that can be generated from “stranded” renewable-energy resources. However, the traditional Haber–Bosch process for the production of ammonia from atmospheric nitrogen and fossil fuels is a high temperature and pressure process that is energy intensive, currently producing more than 1.6% of global CO2 emissions. An ambient temperature, electrochemical synthesis of ammonia is an attractive alternative approach, but has, to date, not been achieved at high efficiency. We report in this work the use of ionic liquids that have high N2 solubility as electrolytes to achieve high conversion efficiency of 60% for N2 electro-reduction to ammonia on a nanostructured iron catalyst under ambient conditions. |
| Author | Azofra, Luis Miguel McDonnell-Worth, Ciaran Kar, Mega Zhang, Xinyi Sun, Chenghua MacFarlane, Douglas R Ali, Muataz Zhou, Fengling Simonov, Alexandr N |
| AuthorAffiliation | Monash University ARC Centre of Excellence for Electromaterials Science and School of Chemistry Clayton |
| AuthorAffiliation_xml | – sequence: 0 name: ARC Centre of Excellence for Electromaterials Science and School of Chemistry – sequence: 0 name: Monash University – sequence: 0 name: Clayton |
| Author_xml | – sequence: 1 givenname: Fengling surname: Zhou fullname: Zhou, Fengling – sequence: 2 givenname: Luis Miguel surname: Azofra fullname: Azofra, Luis Miguel – sequence: 3 givenname: Muataz surname: Ali fullname: Ali, Muataz – sequence: 4 givenname: Mega surname: Kar fullname: Kar, Mega – sequence: 5 givenname: Alexandr N surname: Simonov fullname: Simonov, Alexandr N – sequence: 6 givenname: Ciaran surname: McDonnell-Worth fullname: McDonnell-Worth, Ciaran – sequence: 7 givenname: Chenghua surname: Sun fullname: Sun, Chenghua – sequence: 8 givenname: Xinyi surname: Zhang fullname: Zhang, Xinyi – sequence: 9 givenname: Douglas R surname: MacFarlane fullname: MacFarlane, Douglas R |
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| Snippet | Ammonia as the source of most fertilizers has become one of the most important chemicals globally. It also is being increasingly considered as an easily... |
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| SubjectTerms | Ambient temperature Ammonia Carbon dioxide Carbon dioxide emissions Chemical synthesis Electrochemistry Energy resources Energy sources Fertilizers Fossil fuels Haber Bosch process High temperature Hydrogen-based energy Ionic liquids Ions Nitrogen Pressure Renewable energy Temperature effects |
| Title | Electro-synthesis of ammonia from nitrogen at ambient temperature and pressure in ionic liquids |
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