Chemical recycling of carbon fibre reinforced composites in nearcritical and supercritical water

The potential for recycling of carbon fibre reinforced epoxy composites in water at supercritical or nearcritical conditions was studied. Experiments were devised in order to identify the significant process parameters that affect fibre reinforced composite recovery potential including temperature,...

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Published in	Composites. Part A, Applied science and manufacturing Vol. 39; no. 3; pp. 454 - 461
Main Authors	Piñero-Hernanz, Raul, Dodds, Christopher, Hyde, Jason, García-Serna, Juan, Poliakoff, Martyn, Lester, Edward, Cocero, María José, Kingman, Sam, Pickering, Stephen, Wong, Kok Hoong
Format	Journal Article
Language	English
Published	Oxford Elsevier Ltd 01.03.2008 Elsevier
Subjects	A. Carbon fibre A. Recycling A. Thermosetting resin Applied sciences Exact sciences and technology O. Supercritical water Polymer industry, paints, wood Technology of polymers Waste treatment A. Thermosetting resin A. Recycling O. Supercritical water A. Carbon fibre Material recovery Fiber reinforced material Thermooxidative degradation Epoxy resin Mechanical properties Experimental study Mineral fiber Composite material Tensile strength Supercritical solvent Processing parameter Kinetics Recycling Carbon fiber
Online Access	Get full text
ISSN	1359-835X 1878-5840
DOI	10.1016/j.compositesa.2008.01.001

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Abstract	The potential for recycling of carbon fibre reinforced epoxy composites in water at supercritical or nearcritical conditions was studied. Experiments were devised in order to identify the significant process parameters that affect fibre reinforced composite recovery potential including temperature, time, oxidant and catalyst concentration. Experiments were performed in a batch-type reactor (10 mL) without stirring, with temperatures ranging from 523 to 673 K, pressures from 4.0 to 27.0 MPa and reaction times from 1 to 30 min. The efficiency of resin removal reached ca. 79.3 wt.% under supercritical water conditions with further improvement through the use of potassium hydroxide as alkali catalyst (up to 95.3 wt.%). The tensile strength of the reclaimed fibres was between 90% and 98% than that of the virgin fibres. A second-order kinetic equation was implemented to model the reactive extraction process.
AbstractList	The potential for recycling of carbon fibre reinforced epoxy composites in water at supercritical or nearcritical conditions was studied. Experiments were devised in order to identify the significant process parameters that affect fibre reinforced composite recovery potential including temperature, time, oxidant and catalyst concentration. Experiments were performed in a batch-type reactor (10mL) without stirring, with temperatures ranging from 523 to 673K, pressures from 4.0 to 27.0MPa and reaction times from 1 to 30min. The efficiency of resin removal reached ca. 79.3wt.% under supercritical water conditions with further improvement through the use of potassium hydroxide as alkali catalyst (up to 95.3wt.%). The tensile strength of the reclaimed fibres was between 90% and 98% than that of the virgin fibres. A second-order kinetic equation was implemented to model the reactive extraction process. The potential for recycling of carbon fibre reinforced epoxy composites in water at supercritical or nearcritical conditions was studied. Experiments were devised in order to identify the significant process parameters that affect fibre reinforced composite recovery potential including temperature, time, oxidant and catalyst concentration. Experiments were performed in a batch-type reactor (10 mL) without stirring, with temperatures ranging from 523 to 673 K, pressures from 4.0 to 27.0 MPa and reaction times from 1 to 30 min. The efficiency of resin removal reached ca. 79.3 wt.% under supercritical water conditions with further improvement through the use of potassium hydroxide as alkali catalyst (up to 95.3 wt.%). The tensile strength of the reclaimed fibres was between 90% and 98% than that of the virgin fibres. A second-order kinetic equation was implemented to model the reactive extraction process.
Author	Pickering, Stephen Cocero, María José Kingman, Sam García-Serna, Juan Poliakoff, Martyn Piñero-Hernanz, Raul Lester, Edward Dodds, Christopher Hyde, Jason Wong, Kok Hoong
Author_xml	– sequence: 1 givenname: Raul surname: Piñero-Hernanz fullname: Piñero-Hernanz, Raul organization: Department of Chemical Engineering and Environmental Technology, University of Valladolid, c/Prado de la Magdalena s/n 47011-Valladolid, Spain – sequence: 2 givenname: Christopher surname: Dodds fullname: Dodds, Christopher organization: School of Chemical, Environmental and Mining Engineering, University of Nottingham, University Park, Nottingham NG7 2RD, UK – sequence: 3 givenname: Jason surname: Hyde fullname: Hyde, Jason organization: School of Chemistry, University of Nottingham, University Park, Nottingham NG7 2RD, UK – sequence: 4 givenname: Juan surname: García-Serna fullname: García-Serna, Juan email: jgserna@iq.uva.es organization: Department of Chemical Engineering and Environmental Technology, University of Valladolid, c/Prado de la Magdalena s/n 47011-Valladolid, Spain – sequence: 5 givenname: Martyn surname: Poliakoff fullname: Poliakoff, Martyn organization: School of Chemistry, University of Nottingham, University Park, Nottingham NG7 2RD, UK – sequence: 6 givenname: Edward surname: Lester fullname: Lester, Edward email: Edward.Lester@nottingham.ac.uk organization: School of Chemical, Environmental and Mining Engineering, University of Nottingham, University Park, Nottingham NG7 2RD, UK – sequence: 7 givenname: María José surname: Cocero fullname: Cocero, María José organization: Department of Chemical Engineering and Environmental Technology, University of Valladolid, c/Prado de la Magdalena s/n 47011-Valladolid, Spain – sequence: 8 givenname: Sam surname: Kingman fullname: Kingman, Sam organization: School of Chemical, Environmental and Mining Engineering, University of Nottingham, University Park, Nottingham NG7 2RD, UK – sequence: 9 givenname: Stephen surname: Pickering fullname: Pickering, Stephen organization: School of Mechanical, Materials and Manufacturing Engineering, University of Nottingham, University Park, Nottingham NG7 2RD, UK – sequence: 10 givenname: Kok Hoong surname: Wong fullname: Wong, Kok Hoong organization: School of Mechanical, Materials and Manufacturing Engineering, University of Nottingham, University Park, Nottingham NG7 2RD, UK
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Snippet	The potential for recycling of carbon fibre reinforced epoxy composites in water at supercritical or nearcritical conditions was studied. Experiments were...
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SubjectTerms	A. Carbon fibre A. Recycling A. Thermosetting resin Applied sciences Exact sciences and technology O. Supercritical water Polymer industry, paints, wood Technology of polymers Waste treatment
Title	Chemical recycling of carbon fibre reinforced composites in nearcritical and supercritical water
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