Atom probe study of irradiation-enhanced α′ precipitation in neutron-irradiated Fe–Cr model alloys
Atom probe tomography (APT) was performed to study the effects of Cr concentrations, irradiation doses and irradiation temperatures on α′ phase formation in Fe–Cr model alloys (10–16at.%) irradiated at 300 and 450°C to 0.01, 0.1 and 1dpa. For 1dpa specimens, α′ precipitates with an average radius of...
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| Published in | Journal of nuclear materials Vol. 462; no. C; pp. 242 - 249 |
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| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
United States
Elsevier B.V
01.07.2015
Elsevier |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0022-3115 1873-4820 1873-4820 |
| DOI | 10.1016/j.jnucmat.2015.04.005 |
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| Abstract | Atom probe tomography (APT) was performed to study the effects of Cr concentrations, irradiation doses and irradiation temperatures on α′ phase formation in Fe–Cr model alloys (10–16at.%) irradiated at 300 and 450°C to 0.01, 0.1 and 1dpa. For 1dpa specimens, α′ precipitates with an average radius of 1.0–1.3nm were observed. The precipitate density varied significantly from 1.1×1023 to 2.7×10241/m3, depending on Cr concentrations and irradiation temperatures. The volume fraction of α′ phase in 1dpa specimens qualitatively agreed with the phase diagram prediction. For 0.01dpa and 0.1dpa, frequency distribution analysis detected slight Cr segregation in high-Cr specimens, but not in Fe–10Cr specimens. Proximity histogram analysis showed that the radial Cr concentration was highest at the center of α′ precipitates. For most precipitates, the Cr contents were significantly lower than that predicted by the phase diagram. The Cr concentration at precipitate center increased with increasing precipitate size. |
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| AbstractList | Atom probe tomography (APT) was performed to study the effects of Cr concentrations, irradiation doses and irradiation temperatures on alpha ' phase formation in Fe-Cr model alloys (10-16 at.%) irradiated at 300 and 450 [degrees]C to 0.01, 0.1 and 1 dpa. For 1 dpa specimens, alpha ' precipitates with an average radius of 1.0-1.3 nm were observed. The precipitate density varied significantly from 1.1 x 10 super(23) to 2.7 x 10 super(24) 1/m super(3), depending on Cr concentrations and irradiation temperatures. The volume fraction of alpha ' phase in 1 dpa specimens qualitatively agreed with the phase diagram prediction. For 0.01 dpa and 0.1 dpa, frequency distribution analysis detected slight Cr segregation in high-Cr specimens, but not in Fe-10Cr specimens. Proximity histogram analysis showed that the radial Cr concentration was highest at the center of alpha ' precipitates. For most precipitates, the Cr contents were significantly lower than that predicted by the phase diagram. The Cr concentration at precipitate center increased with increasing precipitate size. Atom probe tomography (APT) was performed to study the effects of Cr concentrations, irradiation doses and irradiation temperatures on a' phase formation in Fe-Cr model alloys (10-16 at.%) irradiated at 300 and 450°C to 0.01, 0.1 and 1 dpa. For 1 dpa specimens, α' precipitates with an average radius of 1.0-1.3 nm were observed. The precipitate density varied significantly from 1.1x10²³ to 2.7x10²⁴ 1/m³, depending on Cr concentrations and irradiation temperatures. The volume fraction of α' phase in 1 dpa specimens qualitatively agreed with the phase diagram prediction. For 0.01 dpa and 0.1 dpa, frequency distribution analysis detected slight Cr segregation in high-Cr specimens, but not in Fe-10Cr specimens. Proximity histogram analysis showed that the radial Cr concentration was highest at the center of a' precipitates. For most precipitates, the Cr contents were significantly lower than that predicted by the phase diagram. The Cr concentration at precipitate center increased with increasing precipitate size. Atom probe tomography (APT) was performed to study the effects of Cr concentrations, irradiation doses and irradiation temperatures on α′ phase formation in Fe–Cr model alloys (10–16at.%) irradiated at 300 and 450°C to 0.01, 0.1 and 1dpa. For 1dpa specimens, α′ precipitates with an average radius of 1.0–1.3nm were observed. The precipitate density varied significantly from 1.1×1023 to 2.7×10241/m3, depending on Cr concentrations and irradiation temperatures. The volume fraction of α′ phase in 1dpa specimens qualitatively agreed with the phase diagram prediction. For 0.01dpa and 0.1dpa, frequency distribution analysis detected slight Cr segregation in high-Cr specimens, but not in Fe–10Cr specimens. Proximity histogram analysis showed that the radial Cr concentration was highest at the center of α′ precipitates. For most precipitates, the Cr contents were significantly lower than that predicted by the phase diagram. The Cr concentration at precipitate center increased with increasing precipitate size. |
| Author | Gan, Jian Wu, Yaqiao Maloy, Stuart A. Chen, Wei-Ying Miao, Yinbin Mo, Kun Stubbins, James F. Tomchik, Carolyn A. Okuniewski, Maria A. |
| Author_xml | – sequence: 1 givenname: Wei-Ying surname: Chen fullname: Chen, Wei-Ying organization: Department of Nuclear, Plasma and Radiological Engineering, University of Illinois, Urbana, IL 61801, USA – sequence: 2 givenname: Yinbin surname: Miao fullname: Miao, Yinbin organization: Department of Nuclear, Plasma and Radiological Engineering, University of Illinois, Urbana, IL 61801, USA – sequence: 3 givenname: Yaqiao surname: Wu fullname: Wu, Yaqiao organization: Department of Materials Science and Engineering, Boise State University, Boise, ID 83725, USA – sequence: 4 givenname: Carolyn A. surname: Tomchik fullname: Tomchik, Carolyn A. organization: Department of Nuclear, Plasma and Radiological Engineering, University of Illinois, Urbana, IL 61801, USA – sequence: 5 givenname: Kun surname: Mo fullname: Mo, Kun organization: Department of Nuclear, Plasma and Radiological Engineering, University of Illinois, Urbana, IL 61801, USA – sequence: 6 givenname: Jian surname: Gan fullname: Gan, Jian organization: Idaho National Laboratory, Idaho Falls, ID 83401, USA – sequence: 7 givenname: Maria A. surname: Okuniewski fullname: Okuniewski, Maria A. organization: Idaho National Laboratory, Idaho Falls, ID 83401, USA – sequence: 8 givenname: Stuart A. surname: Maloy fullname: Maloy, Stuart A. organization: Los Alamos National Laboratory, Los Alamos, NM 87544, USA – sequence: 9 givenname: James F. surname: Stubbins fullname: Stubbins, James F. organization: Department of Nuclear, Plasma and Radiological Engineering, University of Illinois, Urbana, IL 61801, USA |
| BackLink | https://www.osti.gov/biblio/1182694$$D View this record in Osti.gov |
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| SubjectTerms | ABUNDANCE Alloys atom probe ATOMIC DISPLACEMENTS ATOMS BINARY ALLOY SYSTEMS CHROMIUM CHROMIUM ALLOYS CONCENTRATION RATIO DENSITY Fe-Cr model alloy Ferrous alloys IRON BASE ALLOYS IRRADIATION MATERIALS SCIENCE neutron irradiated NEUTRONS Nuclear engineering PHASE DIAGRAMS PHYSICAL RADIATION EFFECTS Precipitates PRECIPITATION PROBES RADIATION DOSES SEGREGATION TEMPERATURE DEPENDENCE TEMPERATURE RANGE 0400-1000 K TOMOGRAPHY α' precipitation |
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| Title | Atom probe study of irradiation-enhanced α′ precipitation in neutron-irradiated Fe–Cr model alloys |
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