Pulsed current activated combustion synthesis and consolidation of ultrafine NbSi2 from mechanically activated powders
Dense ultrafine NbSi 2 was synthesized using the pulsed current activated combustion synthesis (PCACS) method within 2 min and in one step from mechanically activated powders of Nb and 2Si. Simultaneous combustion synthesis and densification were accomplished under the combined effects of a pulsed c...
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Published in | Metals and materials international Vol. 15; no. 3; pp. 399 - 403 |
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Main Authors | , , , , , |
Format | Journal Article |
Language | English |
Published |
Springer
The Korean Institute of Metals and Materials
01.06.2009
Springer Nature B.V 대한금속·재료학회 |
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ISSN | 1598-9623 2005-4149 |
DOI | 10.1007/s12540-009-0399-7 |
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Abstract | Dense ultrafine NbSi
2
was synthesized using the pulsed current activated combustion synthesis (PCACS) method within 2 min and in one step from mechanically activated powders of Nb and 2Si. Simultaneous combustion synthesis and densification were accomplished under the combined effects of a pulsed current and mechanical pressure. Highly dense NbSi
2
with a relative density of up to 98 % was produced under simultaneous application of a 60 MPa pressure and a pulsed current. The average grain size and mechanical properties (hardness and fracture toughness) of the compound were investigated. |
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AbstractList | Dense ultrafine NbSi
2
was synthesized using the pulsed current activated combustion synthesis (PCACS) method within 2 min and in one step from mechanically activated powders of Nb and 2Si. Simultaneous combustion synthesis and densification were accomplished under the combined effects of a pulsed current and mechanical pressure. Highly dense NbSi
2
with a relative density of up to 98 % was produced under simultaneous application of a 60 MPa pressure and a pulsed current. The average grain size and mechanical properties (hardness and fracture toughness) of the compound were investigated. Dense ultrafine NbSi^sub 2^ was synthesized using the pulsed current activated combustion synthesis (PCACS) method within 2 min and in one step from mechanically activated powders of Nb and 2Si. Simultaneous combustion synthesis and densification were accomplished under the combined effects of a pulsed current and mechanical pressure. Highly dense NbSi^sub 2^ with a relative density of up to 98 % was produced under simultaneous application of a 60 MPa pressure and a pulsed current. The average grain size and mechanical properties (hardness and fracture toughness) of the compound were investigated.[PUBLICATION ABSTRACT] Dense ultrafine NbSi2 was synthesized using the pulsed current activated combustion synthesis (PCACS) method within 2 min and in one step from mechanically activated powders of Nb and 2Si. Simultaneous combustion synthesis and densification were accomplished under the combined effects of a pulsed current and mechanical pressure. Highly dense NbSi2 with a relative density of up to 98 % was produced under simultaneous application of a 60 MPa pressure and a pulsed current. The average grain size and mechanical properties (hardness and fracture toughness) of the compound were investigated. KCI Citation Count: 13 |
Author | Lee, Byung-Soo Kim, Byung-Ryang Moon, Byung-Moon Ko, In-Yong Shon, In-Jin Nam, Kee-Seok |
Author_xml | – sequence: 1 givenname: In-Yong surname: Ko fullname: Ko, In-Yong organization: Division of Advanced Materials Engineering, the Research Center of Advanced Materials Development, Chonbuk National University – sequence: 2 givenname: Byung-Ryang surname: Kim fullname: Kim, Byung-Ryang organization: Division of Advanced Materials Engineering, the Research Center of Advanced Materials Development, Chonbuk National University – sequence: 3 givenname: Kee-Seok surname: Nam fullname: Nam, Kee-Seok organization: Korea Institute of Materials Science – sequence: 4 givenname: Byung-Moon surname: Moon fullname: Moon, Byung-Moon organization: Liquid Processing & Casting Technology R&D Department, Korea Institute of Indusrial Technology – sequence: 5 givenname: Byung-Soo surname: Lee fullname: Lee, Byung-Soo organization: Division of Advanced Materials Engineering, the Research Center of Advanced Materials Development, Chonbuk National University – sequence: 6 givenname: In-Jin surname: Shon fullname: Shon, In-Jin email: ijshon@chonbuk.ac.kr organization: Division of Advanced Materials Engineering, the Research Center of Advanced Materials Development, Chonbuk National University, Department of Hydrogen and Fuel Cells Engineering, Specialized Graduate School, Chonbuk National University |
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Cites_doi | 10.1016/0921-5093(92)90312-O 10.1016/j.ijrmhm.2004.08.003 10.1016/S0254-0584(98)80014-X 10.1016/S0925-8388(00)00692-7 10.1016/0966-9795(95)98929-3 10.1016/j.ijrmhm.2005.11.004 10.1016/S1359-6462(01)00668-6 10.1007/BF00724706 10.3365/met.mat.2008.10.593 10.1016/S0263-4368(01)00069-5 10.1016/S0079-6425(97)00021-2 10.1016/0263-4368(95)92675-A 10.1007/978-1-4899-0148-4 10.4028/www.scientific.net/MSF.534-536.525 10.1016/j.msea.2004.05.071 10.1016/j.jallcom.2004.10.072 |
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Keywords | pulsed current activated combustion intermetallic nanophase sintering mechanical properties NbSi |
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Snippet | Dense ultrafine NbSi
2
was synthesized using the pulsed current activated combustion synthesis (PCACS) method within 2 min and in one step from mechanically... Dense ultrafine NbSi^sub 2^ was synthesized using the pulsed current activated combustion synthesis (PCACS) method within 2 min and in one step from... Dense ultrafine NbSi2 was synthesized using the pulsed current activated combustion synthesis (PCACS) method within 2 min and in one step from mechanically... |
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SubjectTerms | Alloys Characterization and Evaluation of Materials Chemistry and Materials Science Engineering Thermodynamics Grain size Heat and Mass Transfer Machines Magnetic Materials Magnetism Manufacturing Materials Science Metallic Materials Metallurgy Processes Solid Mechanics 재료공학 |
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Title | Pulsed current activated combustion synthesis and consolidation of ultrafine NbSi2 from mechanically activated powders |
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