Adsorptive scavenging of cationic dyes from aquatic phase by H3PO4 activated Indian jujube (Ziziphus mauritiana) seeds based activated carbon: Isotherm, kinetics, and thermodynamic study
In the present work, a cost-effective Indian jujube seeds derived activated carbon (IJSAC) prepared via o-phosphoric acid chemical activation, is studied for the sequestration of acriflavine (AF) and Victoria blue B (VB) from the aquatic environment. The activated carbon is characterized by Fourier...
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| Published in | Journal of Saudi Chemical Society Vol. 26; no. 2; p. 101417 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.03.2022
Elsevier |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1319-6103 |
| DOI | 10.1016/j.jscs.2021.101417 |
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| Abstract | In the present work, a cost-effective Indian jujube seeds derived activated carbon (IJSAC) prepared via o-phosphoric acid chemical activation, is studied for the sequestration of acriflavine (AF) and Victoria blue B (VB) from the aquatic environment. The activated carbon is characterized by Fourier transform infrared spectroscopy, N2-adsorption/desorption isotherm, scanning electron microscopy techniques and point of zero-charge measurement. The specific surface area (SBET) of 571 m2/g with a pore radius of 22.45 Å specifies mesoporous nature of the IJSAC. The implication of operational conditions on the adsorption of both dyes onto IJSAC assessed by batch methodology, establish the optimal conditions as dosage (1.5 and 2.5 g/L), contact time (60 min), pH (8 and 10), and initial concentration (130 and 140 mg/L) for AF and VB uptake, respectively. The Freundlich adsorption isotherm model (R2 = 0.99) appropriates the equilibrium data suggesting multilayer adsorption onto heterogeneous surface sites, while pseudo-second order (R2 = 0.95–0.99) is the best fit kinetic model. The liquid film and intraparticle diffusion modelling demonstrate that the adsorption process of these dyes is governed by both the steps. Maximum Langmuir adsorption capacity is 113.6 mg/g for acriflavine and 92.78 mg/g for Victoria blue B. Thermodynamic studies indicate endothermic and spontaneous adsorption of dyes. The adsorption mechanism for the uptake of AF and VB by IJSAC most probably involves hydrogen bonding, electrostatic and π-π interactions. Based on its high adsorption capacity, relatively faster kinetics, and reusability, IJSAC can be perceived as a proficient and effective adsorbent for cationic dyes removal from the liquid waste. |
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| AbstractList | In the present work, a cost-effective Indian jujube seeds derived activated carbon (IJSAC) prepared via o-phosphoric acid chemical activation, is studied for the sequestration of acriflavine (AF) and Victoria blue B (VB) from the aquatic environment. The activated carbon is characterized by Fourier transform infrared spectroscopy, N2-adsorption/desorption isotherm, scanning electron microscopy techniques and point of zero-charge measurement. The specific surface area (SBET) of 571 m2/g with a pore radius of 22.45 Å specifies mesoporous nature of the IJSAC. The implication of operational conditions on the adsorption of both dyes onto IJSAC assessed by batch methodology, establish the optimal conditions as dosage (1.5 and 2.5 g/L), contact time (60 min), pH (8 and 10), and initial concentration (130 and 140 mg/L) for AF and VB uptake, respectively. The Freundlich adsorption isotherm model (R2 = 0.99) appropriates the equilibrium data suggesting multilayer adsorption onto heterogeneous surface sites, while pseudo-second order (R2 = 0.95–0.99) is the best fit kinetic model. The liquid film and intraparticle diffusion modelling demonstrate that the adsorption process of these dyes is governed by both the steps. Maximum Langmuir adsorption capacity is 113.6 mg/g for acriflavine and 92.78 mg/g for Victoria blue B. Thermodynamic studies indicate endothermic and spontaneous adsorption of dyes. The adsorption mechanism for the uptake of AF and VB by IJSAC most probably involves hydrogen bonding, electrostatic and π-π interactions. Based on its high adsorption capacity, relatively faster kinetics, and reusability, IJSAC can be perceived as a proficient and effective adsorbent for cationic dyes removal from the liquid waste. |
| ArticleNumber | 101417 |
| Author | Dua, Divya Khan, Suhail Ayoub Khan, Tabrez Alam Nouman, Md Alharthi, Salman S. |
| Author_xml | – sequence: 1 givenname: Tabrez Alam surname: Khan fullname: Khan, Tabrez Alam email: takhan@jmi.ac.in organization: Department of Chemistry, Jamia Millia Islamia, Jamia Nagar, New Delhi 110 025, India – sequence: 2 givenname: Md surname: Nouman fullname: Nouman, Md organization: Department of Chemistry, Jamia Millia Islamia, Jamia Nagar, New Delhi 110 025, India – sequence: 3 givenname: Divya surname: Dua fullname: Dua, Divya organization: Department of Chemistry, Jamia Millia Islamia, Jamia Nagar, New Delhi 110 025, India – sequence: 4 givenname: Suhail Ayoub surname: Khan fullname: Khan, Suhail Ayoub organization: Department of Chemistry, Jamia Millia Islamia, Jamia Nagar, New Delhi 110 025, India – sequence: 5 givenname: Salman S. surname: Alharthi fullname: Alharthi, Salman S. organization: Department of Chemistry, College of Science, Taif University, P.O. Box 110999, Taif 21944, Saudi Arabia |
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| Keywords | Adsorption Isotherms Activated carbon Victoria blue B Indian jujube seeds Kinetics Acriflavine |
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| Snippet | In the present work, a cost-effective Indian jujube seeds derived activated carbon (IJSAC) prepared via o-phosphoric acid chemical activation, is studied for... |
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| SubjectTerms | Acriflavine Activated carbon Adsorption Indian jujube seeds Isotherms Kinetics Victoria blue B |
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| Title | Adsorptive scavenging of cationic dyes from aquatic phase by H3PO4 activated Indian jujube (Ziziphus mauritiana) seeds based activated carbon: Isotherm, kinetics, and thermodynamic study |
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