A photochemical synthesis route to typical transition metal sulfides as highly efficient cocatalyst for hydrogen evolution: from the case of NiS/g-C3N4
[Display omitted] •Photochemical rapid preparation of NiS was realized for the first time.•One of the most robust NiS/g-C3N4 based composite photocatalysts.•A possible mechanism on the enhanced photocatalytic activity was proposed. Precise deposition of cocatalysts on the outlet points of photo-gene...
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| Published in | Applied catalysis. B, Environmental Vol. 225; pp. 284 - 290 |
|---|---|
| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
05.06.2018
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| Subjects | |
| Online Access | Get full text |
| ISSN | 0926-3373 1873-3883 |
| DOI | 10.1016/j.apcatb.2017.11.083 |
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| Abstract | [Display omitted]
•Photochemical rapid preparation of NiS was realized for the first time.•One of the most robust NiS/g-C3N4 based composite photocatalysts.•A possible mechanism on the enhanced photocatalytic activity was proposed.
Precise deposition of cocatalysts on the outlet points of photo-generated electrons is helpful for highly efficient photocatalytic hydrogen evolution. Up to now, photochemical preparation of hydrogen production cocatalysts composed of earth-abundant elements is still great challenging and rarely reported. Herein, from the case of NiS/g-C3N4, a general photochemical synthesis route to typical transition metal sulfides as cocatalyst for hydrogen evolution was proposed. NiS were prepared by a facile and rapid photochemical method. The content of deposited NiS can be simply adjusted by the change of irradiation time. The optimized photocatalytic hydrogen evolution rate mounted up to 16 400μmolg−1h−1 with 0.76wt% NiS loading, which is about 2500 times higher than that of pure g-C3N4. The photocatalytic H2 evolution rate was stable after 40h. The turnover number (TON) reached 1230 000 in 52h with a turnover frequency (TOF) of 23 600 for NiS. Furthermore, the hydrogen evolution of the NiS/g-C3N4 composite photocatalyst reached 28.3mmolg−1 during 7h under natural sunlight. The presence of NiS cocatalyst can efficiently promote the separation of photogenerated electron-hole pairs of g-C3N4, which was supported by the steady-state photoluminescence spectroscopy and photoelectro- chemical analyses. |
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| AbstractList | [Display omitted]
•Photochemical rapid preparation of NiS was realized for the first time.•One of the most robust NiS/g-C3N4 based composite photocatalysts.•A possible mechanism on the enhanced photocatalytic activity was proposed.
Precise deposition of cocatalysts on the outlet points of photo-generated electrons is helpful for highly efficient photocatalytic hydrogen evolution. Up to now, photochemical preparation of hydrogen production cocatalysts composed of earth-abundant elements is still great challenging and rarely reported. Herein, from the case of NiS/g-C3N4, a general photochemical synthesis route to typical transition metal sulfides as cocatalyst for hydrogen evolution was proposed. NiS were prepared by a facile and rapid photochemical method. The content of deposited NiS can be simply adjusted by the change of irradiation time. The optimized photocatalytic hydrogen evolution rate mounted up to 16 400μmolg−1h−1 with 0.76wt% NiS loading, which is about 2500 times higher than that of pure g-C3N4. The photocatalytic H2 evolution rate was stable after 40h. The turnover number (TON) reached 1230 000 in 52h with a turnover frequency (TOF) of 23 600 for NiS. Furthermore, the hydrogen evolution of the NiS/g-C3N4 composite photocatalyst reached 28.3mmolg−1 during 7h under natural sunlight. The presence of NiS cocatalyst can efficiently promote the separation of photogenerated electron-hole pairs of g-C3N4, which was supported by the steady-state photoluminescence spectroscopy and photoelectro- chemical analyses. |
| Author | Wu, Xiuming Jiang, Pingping Zhang, Huizhen Dong, Yuming Zhao, Hui Zhao, Na Cui, Guanwei Wang, Guangli |
| Author_xml | – sequence: 1 givenname: Hui surname: Zhao fullname: Zhao, Hui organization: Key Laboratory of Synthetic and Biological Colloids (Ministry of Education of China), School of Chemical and Material Engineering, Jiangnan University, Wuxi 214122, PR China – sequence: 2 givenname: Huizhen surname: Zhang fullname: Zhang, Huizhen organization: Key Laboratory of Synthetic and Biological Colloids (Ministry of Education of China), School of Chemical and Material Engineering, Jiangnan University, Wuxi 214122, PR China – sequence: 3 givenname: Guanwei surname: Cui fullname: Cui, Guanwei organization: College of Chemistry, Chemical Engineering and Materials Science, Collaborative Innovation Center of Functionalized Probes for Chemical Imaging in Universities of Shandong, Shandong Normal University, Jinan 250014, PR China – sequence: 4 givenname: Yuming surname: Dong fullname: Dong, Yuming email: dongym@jiangnan.edu.cn organization: Key Laboratory of Synthetic and Biological Colloids (Ministry of Education of China), School of Chemical and Material Engineering, Jiangnan University, Wuxi 214122, PR China – sequence: 5 givenname: Guangli surname: Wang fullname: Wang, Guangli organization: Key Laboratory of Synthetic and Biological Colloids (Ministry of Education of China), School of Chemical and Material Engineering, Jiangnan University, Wuxi 214122, PR China – sequence: 6 givenname: Pingping surname: Jiang fullname: Jiang, Pingping organization: Key Laboratory of Synthetic and Biological Colloids (Ministry of Education of China), School of Chemical and Material Engineering, Jiangnan University, Wuxi 214122, PR China – sequence: 7 givenname: Xiuming surname: Wu fullname: Wu, Xiuming organization: Key Laboratory of Synthetic and Biological Colloids (Ministry of Education of China), School of Chemical and Material Engineering, Jiangnan University, Wuxi 214122, PR China – sequence: 8 givenname: Na surname: Zhao fullname: Zhao, Na organization: Key Laboratory of Synthetic and Biological Colloids (Ministry of Education of China), School of Chemical and Material Engineering, Jiangnan University, Wuxi 214122, PR China |
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| Keywords | Photocatalytic Water splitting Hydrogen evolution Photochemical method NiS/g-C3N4 |
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•Photochemical rapid preparation of NiS was realized for the first time.•One of the most robust NiS/g-C3N4 based composite photocatalysts.•A... |
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| SubjectTerms | Hydrogen evolution NiS/g-C3N4 Photocatalytic Photochemical method Water splitting |
| Title | A photochemical synthesis route to typical transition metal sulfides as highly efficient cocatalyst for hydrogen evolution: from the case of NiS/g-C3N4 |
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