Corrosion action and passivation mechanism of magnesium alloy in fluoride solution
Corrosion action and passive mechanism of magnesium alloy in the fluoride solution were studied by means of scanning electron microscopy（SEM）, energy dispersive X-ray spectroscopy（EDS）, and electrochemistry methods. The results show that an insoluble MgF2 fihn is generated on the surface of magnesiu...
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| Published in | Transactions of Nonferrous Metals Society of China Vol. 19; no. 1; pp. 50 - 54 |
|---|---|
| Main Author | |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
01.02.2009
Steel Sheet Cold Rolling Plant, Baosteel Branch, Baosteel Co., Ltd., Shanghai 200431, China%Steel Sheet Cold Rolling Plant, Baosteel Branch, Baosteel Co., Ltd., Shanghai 200431, China%School of Metallurgy and Materials, Northeastern University, Shenyang 110004, China School of Metallurgy and Materials, Northeastern University, Shenyang 110004, China |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1003-6326 |
| DOI | 10.1016/S1003-6326(08)60227-7 |
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| Abstract | Corrosion action and passive mechanism of magnesium alloy in the fluoride solution were studied by means of scanning electron microscopy（SEM）, energy dispersive X-ray spectroscopy（EDS）, and electrochemistry methods. The results show that an insoluble MgF2 fihn is generated on the surface of magnesium alloy activated in the hydrofluoric acid. And the mass of the deposited MgF2 film may reach a constant value, when the mass ratio of Mg/F on the magnesium alloy surface is fixed at 11.3：1. The activated magnesium alloy gains a ＇passivation state＇ in a mixture of sulfuric acid and hydrofluoric acid at a volume ratio of less than 1.2. At the same time the mass of magnesium alloy is maintained as a function of the time. When the ratio is above 1.4, the mass of magnesium alloy rapidly decreases. The passive film formed through adsorption of HF2- （or H2F3, H3F4-） ions by the deposited MgF2 film can protect the magnesium alloy from corrosion in fluoride solution, but not in non-fluoride solutions. The passive state is maintained for activated magnesium alloy in an acidic sulfuric nickel solution with added fluoride. If fluoride and carbonate are added to the acidic sulfuric nickel solution, a replacement reaction between magnesium alloy and solution takes place. |
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| AbstractList | TG1; Corrosion action and passive mechanism of magnesium alloy in the fluoride solution were studied by means of scanning electron microscopy(SEM), energy dispersive X-ray spectroscopy(EDS), and electrochemistry methods. The results show that an insoluble MgF2 film is generated on the surface of magnesium alloy activated in the hydrofluoric acid. And the mass of the deposited MgF2 film may reach a constant value, when the mass ratio of Mg/F on the magnesium alloy surface is fixed at 11.3-1. The activated magnesium alloy gains a 'passivation state' in a mixture of sulfuric acid and hydrofluoric acid at a volume ratio of less than 1.2. At the same time the mass of magnesium alloy is maintained as a function of the time. When the ratio is above 1.4, the mass of magnesium alloy rapidly decreases. The passive film formed through adsorption of HF2- (or H2F3-, H3F4-) ions by the deposited MgF2 film can protect the magnesium alloy from corrosion in fluoride solution, but not in non-fluoride solutions. The passive state is maintained for activated magnesium alloy in an acidic sulfuric nickel solution with added fluoride. If fluoride and carbonate are added to the acidic sulfuric nickel solution, a replacement reaction between magnesium alloy and solution takes place. Corrosion action and passive mechanism of magnesium alloy in the fluoride solution were studied by means of scanning electron microscopy(SEM), energy dispersive X-ray spectroscopy(EDS), and electrochemistry methods. The results show that an insoluble MgF2 film is generated on the surface of magnesium alloy activated in the hydrofluoric acid. And the mass of the deposited MgF2 film may reach a constant value, when the mass ratio of Mg/F on the magnesium alloy surface is fixed at 11.3:1. The activated magnesium alloy gains a 'passivation state' in a mixture of sulfuric acid and hydrofluoric acid at a volume ratio of less than 1.2. At the same time the mass of magnesium alloy is maintained as a function of the time. When the ratio is above 1.4, the mass of magnesium alloy rapidly decreases. The passive film formed through adsorption of HF2- (or H2F3-, H3F4-) ions by the deposited MgF2 film can protect the magnesium alloy from corrosion in fluoride solution, but not in non-fluoride solutions. The passive state is maintained for activated magnesium alloy in an acidic sulfuric nickel solution with added fluoride. If fluoride and carbonate are added to the acidic sulfuric nickel solution, a replacement reaction between magnesium alloy and solution takes place. Corrosion action and passive mechanism of magnesium alloy in the fluoride solution were studied by means of scanning electron microscopy（SEM）, energy dispersive X-ray spectroscopy（EDS）, and electrochemistry methods. The results show that an insoluble MgF2 fihn is generated on the surface of magnesium alloy activated in the hydrofluoric acid. And the mass of the deposited MgF2 film may reach a constant value, when the mass ratio of Mg/F on the magnesium alloy surface is fixed at 11.3：1. The activated magnesium alloy gains a ＇passivation state＇ in a mixture of sulfuric acid and hydrofluoric acid at a volume ratio of less than 1.2. At the same time the mass of magnesium alloy is maintained as a function of the time. When the ratio is above 1.4, the mass of magnesium alloy rapidly decreases. The passive film formed through adsorption of HF2- （or H2F3, H3F4-） ions by the deposited MgF2 film can protect the magnesium alloy from corrosion in fluoride solution, but not in non-fluoride solutions. The passive state is maintained for activated magnesium alloy in an acidic sulfuric nickel solution with added fluoride. If fluoride and carbonate are added to the acidic sulfuric nickel solution, a replacement reaction between magnesium alloy and solution takes place. Corrosion action and passive mechanism of magnesium alloy in the fluoride solution were studied by means of scanning electron microscopy(SEM), energy dispersive X-ray spectroscopy(EDS), and electrochemistry methods. The results show that an insoluble MgF 2 film is generated on the surface of magnesium alloy activated in the hydrofluoric acid. And the mass of the deposited MgF 2 film may reach a constant value, when the mass ratio of Mg/F on the magnesium alloy surface is fixed at 11.3:1. The activated magnesium alloy gains a ‘passivation state’ in a mixture of sulfuric acid and hydrofluoric acid at a volume ratio of less than 1.2. At the same time the mass of magnesium alloy is maintained as a function of the time. When the ratio is above 1.4, the mass of magnesium alloy rapidly decreases. The passive film formed through adsorption of HF 2 − (or H 2F 3 −, H 3F 4 −) ions by the deposited MgF 2 film can protect the magnesium alloy from corrosion in fluoride solution, but not in non-fluoride solutions. The passive state is maintained for activated magnesium alloy in an acidic sulfuric nickel solution with added fluoride. If fluoride and carbonate are added to the acidic sulfuric nickel solution, a replacement reaction between magnesium alloy and solution takes place. |
| Author | 李建中 黄久贵 田彦文 刘常升 |
| AuthorAffiliation | School of Metallurgy and Materials, Northeastern University, Shenyang I 10004, China Steel Sheet Cold Rolling Plant, Baosteel Branch, Baosteel Co., Ltd., Shanghai 200431, China |
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