CO2-responsive aqueous foams stabilized by pseudogemini surfactants
[Display omitted] To obtain surfactants with superior surface activity and responsive behavior, “pseudogemini” surfactants (short for D-LCFA) are synthesized by mixing long chain fatty acids (LCFA) and polyetheramine D 230 at fixed molar ratio (2:1). Non-covalently bonded building blocks indicate th...
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| Published in | Journal of colloid and interface science Vol. 536; pp. 381 - 388 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Inc
15.02.2019
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| Subjects | |
| Online Access | Get full text |
| ISSN | 0021-9797 1095-7103 1095-7103 |
| DOI | 10.1016/j.jcis.2018.10.040 |
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| Abstract | [Display omitted]
To obtain surfactants with superior surface activity and responsive behavior, “pseudogemini” surfactants (short for D-LCFA) are synthesized by mixing long chain fatty acids (LCFA) and polyetheramine D 230 at fixed molar ratio (2:1). Non-covalently bonded building blocks indicate that CO2-responsive aqueous foams can be obtained by utilizing such pseudogemini surfactants.
1H NMR and FT-IR characterizations prove that the building blocks of these surfactants are associated by electrostatic interaction. The synthesis (Brønsted acid-base reaction) is simple and eco-friendly. “Pseudogemini” structure enables D-LCFA to reduce surface tension of aqueous solution effectively, thus facilitating foam generation. Rheograms, FF-TEM and Cryo-TEM results prove that different aggregates in D-LCFA aqueous solutions lead to different foam properties.
Bubbling of CO2 for about 30 s leads to the rupture of aqueous foams generated by D-LCFA, while removing CO2 by bubbling of N2 at 65 °C for 10 min enables re-generation of foams. The CO2-responsive foaming properties can be attributed to dissociation of D-LCFA upon bubbling of CO2 and re-association upon removal of CO2. The effective CO2-responsive foams can be applied to many areas, such as foam fracturing, foam enhanced oil recovery or recovering of radioactive materials. |
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| AbstractList | To obtain surfactants with superior surface activity and responsive behavior, "pseudogemini" surfactants (short for D-LCFA) are synthesized by mixing long chain fatty acids (LCFA) and polyetheramine D 230 at fixed molar ratio (2:1). Non-covalently bonded building blocks indicate that CO2-responsive aqueous foams can be obtained by utilizing such pseudogemini surfactants.HYPOTHESISTo obtain surfactants with superior surface activity and responsive behavior, "pseudogemini" surfactants (short for D-LCFA) are synthesized by mixing long chain fatty acids (LCFA) and polyetheramine D 230 at fixed molar ratio (2:1). Non-covalently bonded building blocks indicate that CO2-responsive aqueous foams can be obtained by utilizing such pseudogemini surfactants.1H NMR and FT-IR characterizations prove that the building blocks of these surfactants are associated by electrostatic interaction. The synthesis (Brønsted acid-base reaction) is simple and eco-friendly. "Pseudogemini" structure enables D-LCFA to reduce surface tension of aqueous solution effectively, thus facilitating foam generation. Rheograms, FF-TEM and Cryo-TEM results prove that different aggregates in D-LCFA aqueous solutions lead to different foam properties.EXPERIMENTS1H NMR and FT-IR characterizations prove that the building blocks of these surfactants are associated by electrostatic interaction. The synthesis (Brønsted acid-base reaction) is simple and eco-friendly. "Pseudogemini" structure enables D-LCFA to reduce surface tension of aqueous solution effectively, thus facilitating foam generation. Rheograms, FF-TEM and Cryo-TEM results prove that different aggregates in D-LCFA aqueous solutions lead to different foam properties.Bubbling of CO2 for about 30 s leads to the rupture of aqueous foams generated by D-LCFA, while removing CO2 by bubbling of N2 at 65 °C for 10 min enables re-generation of foams. The CO2-responsive foaming properties can be attributed to dissociation of D-LCFA upon bubbling of CO2 and re-association upon removal of CO2. The effective CO2-responsive foams can be applied to many areas, such as foam fracturing, foam enhanced oil recovery or recovering of radioactive materials.FINDINGSBubbling of CO2 for about 30 s leads to the rupture of aqueous foams generated by D-LCFA, while removing CO2 by bubbling of N2 at 65 °C for 10 min enables re-generation of foams. The CO2-responsive foaming properties can be attributed to dissociation of D-LCFA upon bubbling of CO2 and re-association upon removal of CO2. The effective CO2-responsive foams can be applied to many areas, such as foam fracturing, foam enhanced oil recovery or recovering of radioactive materials. [Display omitted] To obtain surfactants with superior surface activity and responsive behavior, “pseudogemini” surfactants (short for D-LCFA) are synthesized by mixing long chain fatty acids (LCFA) and polyetheramine D 230 at fixed molar ratio (2:1). Non-covalently bonded building blocks indicate that CO2-responsive aqueous foams can be obtained by utilizing such pseudogemini surfactants. 1H NMR and FT-IR characterizations prove that the building blocks of these surfactants are associated by electrostatic interaction. The synthesis (Brønsted acid-base reaction) is simple and eco-friendly. “Pseudogemini” structure enables D-LCFA to reduce surface tension of aqueous solution effectively, thus facilitating foam generation. Rheograms, FF-TEM and Cryo-TEM results prove that different aggregates in D-LCFA aqueous solutions lead to different foam properties. Bubbling of CO2 for about 30 s leads to the rupture of aqueous foams generated by D-LCFA, while removing CO2 by bubbling of N2 at 65 °C for 10 min enables re-generation of foams. The CO2-responsive foaming properties can be attributed to dissociation of D-LCFA upon bubbling of CO2 and re-association upon removal of CO2. The effective CO2-responsive foams can be applied to many areas, such as foam fracturing, foam enhanced oil recovery or recovering of radioactive materials. To obtain surfactants with superior surface activity and responsive behavior, “pseudogemini” surfactants (short for D-LCFA) are synthesized by mixing long chain fatty acids (LCFA) and polyetheramine D 230 at fixed molar ratio (2:1). Non-covalently bonded building blocks indicate that CO₂-responsive aqueous foams can be obtained by utilizing such pseudogemini surfactants.¹H NMR and FT-IR characterizations prove that the building blocks of these surfactants are associated by electrostatic interaction. The synthesis (Brønsted acid-base reaction) is simple and eco-friendly. “Pseudogemini” structure enables D-LCFA to reduce surface tension of aqueous solution effectively, thus facilitating foam generation. Rheograms, FF-TEM and Cryo-TEM results prove that different aggregates in D-LCFA aqueous solutions lead to different foam properties.Bubbling of CO₂ for about 30 s leads to the rupture of aqueous foams generated by D-LCFA, while removing CO₂ by bubbling of N₂ at 65 °C for 10 min enables re-generation of foams. The CO₂-responsive foaming properties can be attributed to dissociation of D-LCFA upon bubbling of CO₂ and re-association upon removal of CO₂. The effective CO₂-responsive foams can be applied to many areas, such as foam fracturing, foam enhanced oil recovery or recovering of radioactive materials. |
| Author | Sun, Dejun Wang, Zengzi Ren, Gaihuan Yang, Jiawen Xu, Zhenghe |
| Author_xml | – sequence: 1 givenname: Zengzi surname: Wang fullname: Wang, Zengzi organization: Key Laboratory of Colloid and Interface Chemistry, Shandong University, Ministry of Education, Jinan, Shandong 250100, PR China – sequence: 2 givenname: Gaihuan surname: Ren fullname: Ren, Gaihuan organization: Key Laboratory of Colloid and Interface Chemistry, Shandong University, Ministry of Education, Jinan, Shandong 250100, PR China – sequence: 3 givenname: Jiawen surname: Yang fullname: Yang, Jiawen organization: Key Laboratory of Colloid and Interface Chemistry, Shandong University, Ministry of Education, Jinan, Shandong 250100, PR China – sequence: 4 givenname: Zhenghe surname: Xu fullname: Xu, Zhenghe organization: Department of Materials Science and Engineering, Southern University of Science and Technology, Shenzhen, Guangdong 518055, PR China – sequence: 5 givenname: Dejun surname: Sun fullname: Sun, Dejun email: djsun@sdu.edu.cn organization: Key Laboratory of Colloid and Interface Chemistry, Shandong University, Ministry of Education, Jinan, Shandong 250100, PR China |
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To obtain surfactants with superior surface activity and responsive behavior, “pseudogemini” surfactants (short for D-LCFA) are synthesized... To obtain surfactants with superior surface activity and responsive behavior, "pseudogemini" surfactants (short for D-LCFA) are synthesized by mixing long... To obtain surfactants with superior surface activity and responsive behavior, “pseudogemini” surfactants (short for D-LCFA) are synthesized by mixing long... |
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| SubjectTerms | aqueous solutions carbon dioxide CO2 responsive foam dissociation electrostatic interactions foaming properties foams Fourier transform infrared spectroscopy Long chain fatty acids mixing nuclear magnetic resonance spectroscopy oils Polyetheramine Pseudogemini surfactants surface tension surfactants |
| Title | CO2-responsive aqueous foams stabilized by pseudogemini surfactants |
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