Structural characteristics and chemical bonding states with temperature in barium titanate nanopowders prepared by using the solvothermal method
We report the structural characteristics and the chemical bonding states of nano-sized BaTiO3 powders before and after having been heat treatment. We prepare BaTiO3 nanopowders by using the solvothermal method at different reaction temperatures. We anneal the prepared powders at 400 and 600 °C, resp...
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| Published in | Current applied physics Vol. 15; no. 11; pp. 1377 - 1383 |
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| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.11.2015
한국물리학회 |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1567-1739 1878-1675 1567-1739 |
| DOI | 10.1016/j.cap.2015.06.028 |
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| Abstract | We report the structural characteristics and the chemical bonding states of nano-sized BaTiO3 powders before and after having been heat treatment. We prepare BaTiO3 nanopowders by using the solvothermal method at different reaction temperatures. We anneal the prepared powders at 400 and 600 °C, respectively, for 1 h. We examine the structures of the prepared powders by using the Rietveld analysis, and the chemical bonding states of the ions by using a fitting program with an assumption that the measured spectra are Gaussian. Then, we study the morphology of the nanopowders, and measure the ferroelectric properties with frequency and reaction temperature. We show that the BaTiO3 nanopowders prepared by using the solvothermal method at lower reaction temperature exhibit the tetragonality and are useful for the electronic device applications.
•BaTiO3 nanopowders by using the solvothermal method at different reaction temperatures.•Studied the structures and the chemical bonding states before and after annealing.•Examined the ferroelectric properties of BaTiO3 nanopowders with a tetragonality.•BaTiO3 nanopowders prepared at lower reaction temperature exhibit the tetragonality. |
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| AbstractList | We report the structural characteristics and the chemical bonding states of nano-sized BaTiO3 powders before and after having been heat treatment.We prepare BaTiO3 nanopowders by using the solvothermal method at different reaction temperatures. We anneal the prepared powders at 400 and 600 ℃, respectively, for 1 h. We examine the structures of the prepared powders by using the Rietveld analysis, and the chemical bonding states of the ions by using a fitting program with an assumption that the measured spectra are Gaussian. Then, we study the morphology of the nanopowders, and measure the ferroelectric properties with frequency and reaction temperature. We show that the BaTiO3 nanopowders prepared by using the solvothermal method at lower reaction temperature exhibit the tetragonality and are useful for the electronic device applications. KCI Citation Count: 4 We report the structural characteristics and the chemical bonding states of nano-sized BaTiO3 powders before and after having been heat treatment. We prepare BaTiO3 nanopowders by using the solvothermal method at different reaction temperatures. We anneal the prepared powders at 400 and 600 °C, respectively, for 1 h. We examine the structures of the prepared powders by using the Rietveld analysis, and the chemical bonding states of the ions by using a fitting program with an assumption that the measured spectra are Gaussian. Then, we study the morphology of the nanopowders, and measure the ferroelectric properties with frequency and reaction temperature. We show that the BaTiO3 nanopowders prepared by using the solvothermal method at lower reaction temperature exhibit the tetragonality and are useful for the electronic device applications. •BaTiO3 nanopowders by using the solvothermal method at different reaction temperatures.•Studied the structures and the chemical bonding states before and after annealing.•Examined the ferroelectric properties of BaTiO3 nanopowders with a tetragonality.•BaTiO3 nanopowders prepared at lower reaction temperature exhibit the tetragonality. |
| Author | Hong, K.S. Bae, Jong-Seong Kim, Ill Won Kim, Ju Sung Ha, Myoung Gyu Bae, Yu Ri Ahn, Chang Won Kim, Jong Pil |
| Author_xml | – sequence: 1 givenname: K.S. surname: Hong fullname: Hong, K.S. organization: Pusan Center, Korea Basic Science Institute, Pusan, 618-230, Republic of Korea – sequence: 2 givenname: Myoung Gyu surname: Ha fullname: Ha, Myoung Gyu organization: Pusan Center, Korea Basic Science Institute, Pusan, 618-230, Republic of Korea – sequence: 3 givenname: Jong-Seong surname: Bae fullname: Bae, Jong-Seong organization: Pusan Center, Korea Basic Science Institute, Pusan, 618-230, Republic of Korea – sequence: 4 givenname: Ju Sung orcidid: 0000-0003-3937-3181 surname: Kim fullname: Kim, Ju Sung organization: R&D Center, KCMC Co., Yongin, Gyeonggi, 446-908, Republic of Korea – sequence: 5 givenname: Yu Ri surname: Bae fullname: Bae, Yu Ri organization: Korea Electrotechnology Research Institute, Changwon, 642-120, Republic of Korea – sequence: 6 givenname: Chang Won surname: Ahn fullname: Ahn, Chang Won organization: Department of Physics, Ulsan University, Ulsan, 680-749, Republic of Korea – sequence: 7 givenname: Ill Won surname: Kim fullname: Kim, Ill Won organization: Department of Physics, Ulsan University, Ulsan, 680-749, Republic of Korea – sequence: 8 givenname: Jong Pil surname: Kim fullname: Kim, Jong Pil email: jpkim@kbsi.re.kr organization: Pusan Center, Korea Basic Science Institute, Pusan, 618-230, Republic of Korea |
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| Keywords | Tetragonality BaTiO3 Solvothermal synthesis Chemical bonding state |
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| Snippet | We report the structural characteristics and the chemical bonding states of nano-sized BaTiO3 powders before and after having been heat treatment. We prepare... We report the structural characteristics and the chemical bonding states of nano-sized BaTiO3 powders before and after having been heat treatment.We prepare... |
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| SubjectTerms | BaTiO3 Chemical bonding state Solvothermal synthesis Tetragonality 물리학 |
| Title | Structural characteristics and chemical bonding states with temperature in barium titanate nanopowders prepared by using the solvothermal method |
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