Mechanical and microstructural characterization of powder metallurgy CoCrNi medium entropy alloy
The present study is focused on synthesis and mechanical properties characterization of equiatomic CoCrNi medium entropy alloy (MEA). Powder metallurgy processes of mechanical alloying (MA) with subsequent spark plasma sintering (SPS) for bulk alloy densification have been utilized. As opposed to th...
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| Published in | Materials science & engineering. A, Structural materials : properties, microstructure and processing Vol. 701; pp. 370 - 380 |
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| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Lausanne
Elsevier B.V
31.07.2017
Elsevier BV |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0921-5093 1873-4936 |
| DOI | 10.1016/j.msea.2017.06.086 |
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| Abstract | The present study is focused on synthesis and mechanical properties characterization of equiatomic CoCrNi medium entropy alloy (MEA). Powder metallurgy processes of mechanical alloying (MA) with subsequent spark plasma sintering (SPS) for bulk alloy densification have been utilized. As opposed to the single-phase alloys of identical composition fabricated via casting routes, the alloy after SPS compaction consisted of a major FCC solid solution phase (94.4%), minor fraction of secondary BCC phase (5.6%, precipitated at the FCC grains boundaries), and negligible amount of oxide inclusions. The alloy exhibited high ultimate tensile strength of 1024MPa and a elongation to fracture of 26%. Elastic modulus of the alloy reached 222GPa and the thermal expansion coefficient (CTE) was measured as 17.4 × 10−6K−1 The plastic deformation in the alloy is carried out by a combination of dislocation glide and mechanical nano-twinning at room temperature. |
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| AbstractList | The present study is focused on synthesis and mechanical properties characterization of equiatomic CoCrNi medium entropy alloy (MEA). Powder metallurgy processes of mechanical alloying (MA) with subsequent spark plasma sintering (SPS) for bulk alloy densification have been utilized. As opposed to the single-phase alloys of identical composition fabricated via casting routes, the alloy after SPS compaction consisted of a major FCC solid solution phase (94.4%), minor fraction of secondary BCC phase (5.6%, precipitated at the FCC grains boundaries), and negligible amount of oxide inclusions. The alloy exhibited high ultimate tensile strength of 1024 MPa and a elongation to fracture of 26%. Elastic modulus of the alloy reached 222 GPa and the thermal expansion coefficient (CTE) was measured as 17.4 ... 10-6 K-1 The plastic deformation in the alloy is carried out by a combination of dislocation glide and mechanical nano-twinning at room temperature. The present study is focused on synthesis and mechanical properties characterization of equiatomic CoCrNi medium entropy alloy (MEA). Powder metallurgy processes of mechanical alloying (MA) with subsequent spark plasma sintering (SPS) for bulk alloy densification have been utilized. As opposed to the single-phase alloys of identical composition fabricated via casting routes, the alloy after SPS compaction consisted of a major FCC solid solution phase (94.4%), minor fraction of secondary BCC phase (5.6%, precipitated at the FCC grains boundaries), and negligible amount of oxide inclusions. The alloy exhibited high ultimate tensile strength of 1024MPa and a elongation to fracture of 26%. Elastic modulus of the alloy reached 222GPa and the thermal expansion coefficient (CTE) was measured as 17.4 × 10−6K−1 The plastic deformation in the alloy is carried out by a combination of dislocation glide and mechanical nano-twinning at room temperature. |
| Author | Dlouhy, Ivo Kovacova, Zuzana Kitzmantel, Michael Neubauer, Erich Nejezchlebova, Jitka Kubena, Ivo Cizek, Jan Hornik, Vit Moravcik, Igor |
| Author_xml | – sequence: 1 givenname: Igor surname: Moravcik fullname: Moravcik, Igor email: moravcik@fme.vutbr.cz organization: NETME Centre, Institute of Materials Science and Engineering, Brno University of Technology, Technicka 2896/2, Brno, Czech Republic – sequence: 2 givenname: Jan surname: Cizek fullname: Cizek, Jan organization: Institute of Plasma Physics, Czech Academy of Sciences, Za Slovankou 1782/3, 182 00 Prague 8, Czech Republic – sequence: 3 givenname: Zuzana surname: Kovacova fullname: Kovacova, Zuzana organization: RHP-Technology GmbH, Forschungs, und Technologiezentrum, 2444 Seibersdorf, Austria – sequence: 4 givenname: Jitka surname: Nejezchlebova fullname: Nejezchlebova, Jitka organization: Faculty of Nuclear Sciences and Physical Engineering, Czech Technical University in Prague, Trojanova 13, 18200 Prague, Czech Republic – sequence: 5 givenname: Michael surname: Kitzmantel fullname: Kitzmantel, Michael organization: RHP-Technology GmbH, Forschungs, und Technologiezentrum, 2444 Seibersdorf, Austria – sequence: 6 givenname: Erich surname: Neubauer fullname: Neubauer, Erich organization: RHP-Technology GmbH, Forschungs, und Technologiezentrum, 2444 Seibersdorf, Austria – sequence: 7 givenname: Ivo surname: Kubena fullname: Kubena, Ivo organization: Institute of Physics of Materials CAS, Zizkova 22, 61662 Brno, Czech Republic – sequence: 8 givenname: Vit surname: Hornik fullname: Hornik, Vit organization: Institute of Physics of Materials CAS, Zizkova 22, 61662 Brno, Czech Republic – sequence: 9 givenname: Ivo surname: Dlouhy fullname: Dlouhy, Ivo organization: NETME Centre, Institute of Materials Science and Engineering, Brno University of Technology, Technicka 2896/2, Brno, Czech Republic |
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| SubjectTerms | Alloys Body centered cubic lattice Bulk density Casting alloys Densification Dislocations Elongation Entropy Face centered cubic lattice Mechanical alloying Mechanical characterization Mechanical properties Medium entropy alloys Metallurgical analysis Microstructure Modulus of elasticity Nonmetallic inclusions Plastic deformation Plasticity Powder metallurgy Spark plasma sintering Tensile test Thermal expansion Twinning Ultimate tensile strength |
| Title | Mechanical and microstructural characterization of powder metallurgy CoCrNi medium entropy alloy |
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