Production of biofuels from pine needle via catalytic fast pyrolysis over HBeta

The thermal and catalytic pyrolysis of pine needles over HBeta catalysts with different SiO 2 /Al 2 O 3 ratios (25 and 300) were investigated by thermogravimetric analysis (TGA) and pyrolyzer-gas chromatography/mass spectrometry. TGA showed that the main decomposition of pine needles occurred betwee...

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Published in	The Korean journal of chemical engineering Vol. 37; no. 3; pp. 493 - 496
Main Authors	Kim, Young-Min, Lee, Hyung Won, Jang, Seong Ho, Jeong, Jaehun, Ryu, Sumin, Jung, Sang-Chul, Park, Young-Kwon
Format	Journal Article
Language	English
Published	New York Springer US 01.03.2020 Springer Nature B.V 한국화학공학회
Subjects	Aluminum oxide Benzene Biotechnology Catalysis Catalysts Catalytic converters Chemistry Chemistry and Materials Science Chromatography Decomposition Ethylbenzene Gas chromatography Hydrocarbons Industrial Chemistry/Chemical Engineering Mass spectrometry Materials Science Needles Pine Polycyclic aromatic hydrocarbons Pyrolysis Scientific imaging Silicon dioxide Spectroscopy Thermogravimetric analysis Toluene 화학공학 Pine Needle BTEX HBeta Catalytic Pyrolysis
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ISSN	0256-1115 1975-7220
DOI	10.1007/s11814-019-0467-8

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Abstract	The thermal and catalytic pyrolysis of pine needles over HBeta catalysts with different SiO 2 /Al 2 O 3 ratios (25 and 300) were investigated by thermogravimetric analysis (TGA) and pyrolyzer-gas chromatography/mass spectrometry. TGA showed that the main decomposition of pine needles occurred between 150 and 550 °C. The catalytic DTG curves revealed the same decomposition temperature region as the non-catalytic TG curve of pine needles. Pyrolyzergas chromatography/mass spectrometry suggested that the effective catalytic conversion of pyrolyzate intermediates and other hydrocarbons to aromatic hydrocarbons can be achieved using HBeta catalysts at 600 °C. HBeta(25) produced a larger amount of aromatic hydrocarbons than HBeta(300) because of its higher acid amounts. By increasing the reaction temperature from 500 to 700 °C, the formation of benzene, toluene, ethylbenzene, xylenes (BTEXs) and other polycyclic aromatic hydrocarbons was increased with a concomitant decrease in phenolics and other oxygenates. The formation efficiency of BTEXs was increased further by increasing the catalyst loading.
AbstractList	The thermal and catalytic pyrolysis of pine needles over HBeta catalysts with different SiO 2 /Al 2 O 3 ratios (25 and 300) were investigated by thermogravimetric analysis (TGA) and pyrolyzer-gas chromatography/mass spectrometry. TGA showed that the main decomposition of pine needles occurred between 150 and 550 °C. The catalytic DTG curves revealed the same decomposition temperature region as the non-catalytic TG curve of pine needles. Pyrolyzergas chromatography/mass spectrometry suggested that the effective catalytic conversion of pyrolyzate intermediates and other hydrocarbons to aromatic hydrocarbons can be achieved using HBeta catalysts at 600 °C. HBeta(25) produced a larger amount of aromatic hydrocarbons than HBeta(300) because of its higher acid amounts. By increasing the reaction temperature from 500 to 700 °C, the formation of benzene, toluene, ethylbenzene, xylenes (BTEXs) and other polycyclic aromatic hydrocarbons was increased with a concomitant decrease in phenolics and other oxygenates. The formation efficiency of BTEXs was increased further by increasing the catalyst loading. The thermal and catalytic pyrolysis of pine needles over HBeta catalysts with different SiO2/Al2O3 ratios (25 and 300) were investigated by thermogravimetric analysis (TGA) and pyrolyzer-gas chromatography/mass spectrometry. TGA showed that the main decomposition of pine needles occurred between 150 and 550 °C. The catalytic DTG curves revealed the same decomposition temperature region as the non-catalytic TG curve of pine needles. Pyrolyzergas chromatography/mass spectrometry suggested that the effective catalytic conversion of pyrolyzate intermediates and other hydrocarbons to aromatic hydrocarbons can be achieved using HBeta catalysts at 600 °C. HBeta(25) produced a larger amount of aromatic hydrocarbons than HBeta(300) because of its higher acid amounts. By increasing the reaction temperature from 500 to 700 °C, the formation of benzene, toluene, ethylbenzene, xylenes (BTEXs) and other polycyclic aromatic hydrocarbons was increased with a concomitant decrease in phenolics and other oxygenates. The formation efficiency of BTEXs was increased further by increasing the catalyst loading. The thermal and catalytic pyrolysis of pine needles over HBeta catalysts with different SiO2/Al2O3 ratios (25 and 300) were investigated by thermogravimetric analysis (TGA) and pyrolyzer-gas chromatography/mass spectrometry. TGA showed that the main decomposition of pine needles occurred between 150 and 550 oC. The catalytic DTG curves revealed the same decomposition temperature region as the non-catalytic TG curve of pine needles. Pyrolyzergas chromatography/mass spectrometry suggested that the effective catalytic conversion of pyrolyzate intermediates and other hydrocarbons to aromatic hydrocarbons can be achieved using HBeta catalysts at 600 oC. HBeta(25) produced a larger amount of aromatic hydrocarbons than HBeta(300) because of its higher acid amounts. By increasing the reaction temperature from 500 to 700 oC, the formation of benzene, toluene, ethylbenzene, xylenes (BTEXs) and other polycyclic aromatic hydrocarbons was increased with a concomitant decrease in phenolics and other oxygenates. The formation efficiency of BTEXs was increased further by increasing the catalyst loading. KCI Citation Count: 27
Author	Lee, Hyung Won Jang, Seong Ho Ryu, Sumin Jung, Sang-Chul Park, Young-Kwon Jeong, Jaehun Kim, Young-Min
Author_xml	– sequence: 1 givenname: Young-Min surname: Kim fullname: Kim, Young-Min organization: Department of Environmental Engineering, Daegu University – sequence: 2 givenname: Hyung Won surname: Lee fullname: Lee, Hyung Won organization: School of Environmental Engineering, University of Seoul – sequence: 3 givenname: Seong Ho surname: Jang fullname: Jang, Seong Ho organization: Department of BioEnvironmental Energy, Pusan National University – sequence: 4 givenname: Jaehun surname: Jeong fullname: Jeong, Jaehun organization: School of Environmental Engineering, University of Seoul – sequence: 5 givenname: Sumin surname: Ryu fullname: Ryu, Sumin organization: School of Environmental Engineering, University of Seoul – sequence: 6 givenname: Sang-Chul surname: Jung fullname: Jung, Sang-Chul organization: Department of Environmental Engineering, Sunchon National University – sequence: 7 givenname: Young-Kwon surname: Park fullname: Park, Young-Kwon email: catalica@uos.ac.kr organization: School of Environmental Engineering, University of Seoul
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Snippet	The thermal and catalytic pyrolysis of pine needles over HBeta catalysts with different SiO 2 /Al 2 O 3 ratios (25 and 300) were investigated by... The thermal and catalytic pyrolysis of pine needles over HBeta catalysts with different SiO2/Al2O3 ratios (25 and 300) were investigated by thermogravimetric...
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SubjectTerms	Aluminum oxide Benzene Biotechnology Catalysis Catalysts Catalytic converters Chemistry Chemistry and Materials Science Chromatography Decomposition Ethylbenzene Gas chromatography Hydrocarbons Industrial Chemistry/Chemical Engineering Mass spectrometry Materials Science Needles Pine Polycyclic aromatic hydrocarbons Pyrolysis Scientific imaging Silicon dioxide Spectroscopy Thermogravimetric analysis Toluene 화학공학
Title	Production of biofuels from pine needle via catalytic fast pyrolysis over HBeta
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