RAFT Copolymerization of Glycidyl Methacrylate and N,N-Dimethylaminoethyl Methacrylate
In this work, copolymerization of two functional monomers, glycidyl methacrylate （GMA） and N,N-dimethylaminoethyl methacrylate （DMAEMA）, was firstly carried out via reversible addition-fragmentation chain transfer （RAFT） polymerization successfully. The copolymerization kinetics was investigated und...
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| Published in | Chinese journal of chemistry Vol. 30; no. 9; pp. 2138 - 2144 |
|---|---|
| Main Author | |
| Format | Journal Article |
| Language | English |
| Published |
Weinheim
WILEY-VCH Verlag
01.09.2012
WILEY‐VCH Verlag Wiley Subscription Services, Inc |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1001-604X 1614-7065 |
| DOI | 10.1002/cjoc.201200625 |
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| Abstract | In this work, copolymerization of two functional monomers, glycidyl methacrylate （GMA） and N,N-dimethylaminoethyl methacrylate （DMAEMA）, was firstly carried out via reversible addition-fragmentation chain transfer （RAFT） polymerization successfully. The copolymerization kinetics was investigated under the molar ratio of n[GMA＋DMAEMA]o/n[AIBN]o/n[CPDN]o=300/1/3 at 60℃. The copolymerization showed typical ＂living＂ features such as first-order polymerization kinetics, linear increase of molecular weight with monomer conversion and narrow molecular weight distribution. The reactivity ratios of GMA and DMAEMA were calculated by the extended Kelen-Tudos linearization methods. The epoxy group of the copolymer PGMA-co-PDMAEMA remained intact under the conditions of RAFT copolymerization and could easily be post-modified by ethylenedia- mine. Moreover, the modified copolymer could be used as a gene carrier. |
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| AbstractList | In this work, copolymerization of two functional monomers, glycidyl methacrylate (GMA) and
N
,
N
‐dimethylaminoethyl methacrylate (DMAEMA), was firstly carried out via reversible addition‐fragmentation chain transfer (RAFT) polymerization successfully. The copolymerization kinetics was investigated under the molar ratio of
n
[GMA+DMAEMA]
0
/
n
[AIBN]
0
/
n
[CPDN]
0
=300/1/3 at 60°C. The copolymerization showed typical "living" features such as first‐order polymerization kinetics, linear increase of molecular weight with monomer conversion and narrow molecular weight distribution. The reactivity ratios of GMA and DMAEMA were calculated by the extended Kelen‐Tüdös linearization methods. The epoxy group of the copolymer PGMA‐
co
‐PDMAEMA remained intact under the conditions of RAFT copolymerization and could easily be post‐modified by ethylenediamine. Moreover, the modified copolymer could be used as a gene carrier. In this work, copolymerization of two functional monomers, glycidyl methacrylate （GMA） and N,N-dimethylaminoethyl methacrylate （DMAEMA）, was firstly carried out via reversible addition-fragmentation chain transfer （RAFT） polymerization successfully. The copolymerization kinetics was investigated under the molar ratio of n[GMA＋DMAEMA]o/n[AIBN]o/n[CPDN]o=300/1/3 at 60℃. The copolymerization showed typical ＂living＂ features such as first-order polymerization kinetics, linear increase of molecular weight with monomer conversion and narrow molecular weight distribution. The reactivity ratios of GMA and DMAEMA were calculated by the extended Kelen-Tudos linearization methods. The epoxy group of the copolymer PGMA-co-PDMAEMA remained intact under the conditions of RAFT copolymerization and could easily be post-modified by ethylenedia- mine. Moreover, the modified copolymer could be used as a gene carrier. In this work, copolymerization of two functional monomers, glycidyl methacrylate (GMA) and N,N‐dimethylaminoethyl methacrylate (DMAEMA), was firstly carried out via reversible addition‐fragmentation chain transfer (RAFT) polymerization successfully. The copolymerization kinetics was investigated under the molar ratio of n[GMA+DMAEMA]0/n[AIBN]0/n[CPDN]0=300/1/3 at 60°C. The copolymerization showed typical "living" features such as first‐order polymerization kinetics, linear increase of molecular weight with monomer conversion and narrow molecular weight distribution. The reactivity ratios of GMA and DMAEMA were calculated by the extended Kelen‐Tüdös linearization methods. The epoxy group of the copolymer PGMA‐co‐PDMAEMA remained intact under the conditions of RAFT copolymerization and could easily be post‐modified by ethylenediamine. Moreover, the modified copolymer could be used as a gene carrier. Copolymerization of GMA and DMAEMA via RAFT method was firstly carried out. The epoxy group of the copolymers remained intact under the conditions of RAFT copolymerization and could be post‐modified by ethylenediamine and then used as gene carrier. In this work, copolymerization of two functional monomers, glycidyl methacrylate (GMA) and N,N-dimethylaminoethyl methacrylate (DMAEMA), was firstly carried out via reversible addition-fragmentation chain transfer (RAFT) polymerization successfully. The copolymerization kinetics was investigated under the molar ratio of n[GMA+DMAEMA]0/n[AIBN]0/n[CPDN]0=300/1/3 at 60°C. The copolymerization showed typical "living" features such as first-order polymerization kinetics, linear increase of molecular weight with monomer conversion and narrow molecular weight distribution. The reactivity ratios of GMA and DMAEMA were calculated by the extended Kelen-Tudös linearization methods. The epoxy group of the copolymer PGMA-co-PDMAEMA remained intact under the conditions of RAFT copolymerization and could easily be post-modified by ethylenediamine. Moreover, the modified copolymer could be used as a gene carrier. |
| Author | Pan, Xiangqiang Cheng, Zhenping Zhang, Lifen Cao, Jun Zhu, Xiulin |
| AuthorAffiliation | Jiangsu Key Laboratory of Advanced Functional Polymer Design and Application, Department of Polymer Science and Engineering, College of Chemistry,Chemical Engineering and Materials Science, Soochow University, Suzhou 215123, China |
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| CitedBy_id | crossref_primary_10_1002_pola_26956 crossref_primary_10_1002_macp_201200609 crossref_primary_10_1021_acsomega_4c03275 crossref_primary_10_4028_www_scientific_net_KEM_899_387 crossref_primary_10_1016_j_jhazmat_2020_123048 crossref_primary_10_1039_C4CC03699A crossref_primary_10_1080_10601325_2024_2345918 crossref_primary_10_1039_D1RA05555K crossref_primary_10_1007_s00289_023_05098_5 crossref_primary_10_1002_marc_201300513 crossref_primary_10_54097_a92k4n71 |
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| Notes | 31-1547/O6 Keywords reversible addition-fragmentation chain transfer, living radical polymerization, kinetics （polym.）, reac-tivity ratios, glycidyl methacrylate, N,N-dimethylaminoethyl methacrylate Cao, Jun Zhang, Lifen Pan, Xiangqiang Cheng, Zhenping Zhu, Xiulin（Jiangsu Key Laboratory of Advanced Functional Polymer Design and Application, Department of Polymer Science and Engineering, College of Chemistry, Chemical Engineering and Materials Science, Soochow University, Suzhou 215123, China） In this work, copolymerization of two functional monomers, glycidyl methacrylate （GMA） and N,N-dimethylaminoethyl methacrylate （DMAEMA）, was firstly carried out via reversible addition-fragmentation chain transfer （RAFT） polymerization successfully. The copolymerization kinetics was investigated under the molar ratio of n[GMA＋DMAEMA]o/n[AIBN]o/n[CPDN]o=300/1/3 at 60℃. The copolymerization showed typical ＂living＂ features such as first-order polymerization kinetics, linear increase of molecular weight with monomer conversion and narrow molecular weight distribution. The reactivity ratios of GMA and DMAEMA were calculated by the extended Kelen-Tudos linearization methods. The epoxy group of the copolymer PGMA-co-PDMAEMA remained intact under the conditions of RAFT copolymerization and could easily be post-modified by ethylenedia- mine. Moreover, the modified copolymer could be used as a gene carrier. ark:/67375/WNG-1PSN8SCC-N the Project Funded by the Priority Academic Program Development of Jiangsu Higher Education Institutions (PAPD) the Project of International Cooperation of the Ministry of Science and Technology of China - No. 2011DFA50530 ArticleID:CJOC201200625 the Specialized Research Fund for the Doctoral Program of Higher Education - No. 20103201110005 the Project Funded by Jiangsu Key Lab Carbon Based Functional Materials & Devices the National Natural Science Foundation of China - No. 20974071 and 21174096 istex:026D3A5039FD4EF95C8E4A58B4DD6ECB37FC0872 ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 14 |
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| Snippet | In this work, copolymerization of two functional monomers, glycidyl methacrylate （GMA） and N,N-dimethylaminoethyl methacrylate （DMAEMA）, was firstly... In this work, copolymerization of two functional monomers, glycidyl methacrylate (GMA) and N,N‐dimethylaminoethyl methacrylate (DMAEMA), was firstly carried... In this work, copolymerization of two functional monomers, glycidyl methacrylate (GMA) and N , N ‐dimethylaminoethyl methacrylate (DMAEMA), was firstly carried... In this work, copolymerization of two functional monomers, glycidyl methacrylate (GMA) and N,N-dimethylaminoethyl methacrylate (DMAEMA), was firstly carried... |
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| SubjectTerms | glycidyl methacrylate Kinetics kinetics (polym.) living radical polymerization N,N‐dimethylaminoethyl methacrylate N-dimethylaminoethyl methacrylate RAFT reactivity ratios reversible addition-fragmentation chain transfer 二甲基 共聚反应动力学 分子量分布 氨基 甲基丙烯酸甲酯 甲基丙烯酸缩水甘油酯 甲基丙烯酸酯 |
| Title | RAFT Copolymerization of Glycidyl Methacrylate and N,N-Dimethylaminoethyl Methacrylate |
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