Preparation and characterization of highly photocatalytic active hierarchical BiOX (X=Cl, Br, I) microflowers for rhodamine B degradation with kinetic modelling studies

The hierarchical BiOX (X=Cl, Br, I) microflowers were successfully synthesized via simple precipitation method at 160 °C for 24 h and characterized by XRD, SEM, TEM, UV-vis DRS and N 2 adsorption-desorption techniques. The as-prepared samples were pure phases and of microflowers composed of nanoshee...

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Published inJournal of Central South University Vol. 24; no. 4; pp. 754 - 765
Main Authors Gu, Ying-ying, Zhao, Li, Yang, Ming-yang, Xiong, Yi-qiu, Wu, Zhe, Zhou, Min-jia, Yan, Jun
Format Journal Article
LanguageEnglish
Published Changsha Central South University 01.04.2017
Springer Nature B.V
Subjects
Engineering
Kinetics
Light irradiation
Metallic Materials
Photodegradation
Rhodamine
microstructure
photocatalysis
semiconductors
BiOX
Online AccessGet full text
ISSN2095-2899
2227-5223
DOI10.1007/s11771-017-3477-x

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Abstract The hierarchical BiOX (X=Cl, Br, I) microflowers were successfully synthesized via simple precipitation method at 160 °C for 24 h and characterized by XRD, SEM, TEM, UV-vis DRS and N 2 adsorption-desorption techniques. The as-prepared samples were pure phases and of microflowers composed of nanosheets which intercrossed with each other. The specific surface areas were about 22.9, 17.3 and 16.2 m 2 /g for BiOCl, BiOBr and BiOI, respectively. The photocatalytic activities of BiOX powers were evaluated by RhB degradation under UV-vis light irradiation in the order of BiOCl > BiOBr > BiOI. Also, the kinetics of RhB degradation over BiOI was selectively investigated, demonstrating that the kinetics of RhB degradation follows apparent first-order kinetics and fits the Langmuir-Hinshelwood model.
AbstractList The hierarchical BiOX (X=Cl, Br, I) microflowers were successfully synthesized via simple precipitation method at 160 °C for 24 h and characterized by XRD, SEM, TEM, UV-vis DRS and N 2 adsorption-desorption techniques. The as-prepared samples were pure phases and of microflowers composed of nanosheets which intercrossed with each other. The specific surface areas were about 22.9, 17.3 and 16.2 m 2 /g for BiOCl, BiOBr and BiOI, respectively. The photocatalytic activities of BiOX powers were evaluated by RhB degradation under UV-vis light irradiation in the order of BiOCl > BiOBr > BiOI. Also, the kinetics of RhB degradation over BiOI was selectively investigated, demonstrating that the kinetics of RhB degradation follows apparent first-order kinetics and fits the Langmuir-Hinshelwood model.
The hierarchical BiOX (X=Cl, Br, I) microflowers were successfully synthesized via simple precipitation method at 160 °C for 24 h and characterized by XRD, SEM, TEM, UV-vis DRS and N2 adsorption-desorption techniques. The as-prepared samples were pure phases and of microflowers composed of nanosheets which intercrossed with each other. The specific surface areas were about 22.9, 17.3 and 16.2 m2/g for BiOCl, BiOBr and BiOI, respectively. The photocatalytic activities of BiOX powers were evaluated by RhB degradation under UV-vis light irradiation in the order of BiOCl > BiOBr > BiOI. Also, the kinetics of RhB degradation over BiOI was selectively investigated, demonstrating that the kinetics of RhB degradation follows apparent first-order kinetics and fits the Langmuir-Hinshelwood model.
Author Zhou, Min-jia
Wu, Zhe
Zhao, Li
Gu, Ying-ying
Xiong, Yi-qiu
Yang, Ming-yang
Yan, Jun
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  email: yanjun@csu.edu.cn
  organization: School of Chemistry and Chemical Engineering, Central South University
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semiconductors
BiOX
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Snippet The hierarchical BiOX (X=Cl, Br, I) microflowers were successfully synthesized via simple precipitation method at 160 °C for 24 h and characterized by XRD,...
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SubjectTerms Engineering
Kinetics
Light irradiation
Metallic Materials
Photodegradation
Rhodamine
Title Preparation and characterization of highly photocatalytic active hierarchical BiOX (X=Cl, Br, I) microflowers for rhodamine B degradation with kinetic modelling studies
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