Effect of the naphthenic oil and precipitated silica on the crystallization of ultrahigh-molecular-weight polyethylene

Ultrahigh molecular weight polyethylene (UHMW-PE) belongs to the specialty polymer grade because of its unique properties. Among other applications, it is used for battery separator membranes elaboration for automotive applications. These PE separators are porous membranes composed of a blend of UHM...

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Published inPolymer (Guilford) Vol. 97; pp. 63 - 68
Main Authors Toquet, Fabien, Guy, Laurent, Schlegel, Brice, Cassagnau, Philippe, Fulchiron, René
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 05.08.2016
Elsevier
Subjects
Blends
Chemical Sciences
Crystallinity
Crystallization
Crystals
Material chemistry
Membranes
Naphthenic oil
Polyethylenes
Polymers
Separators
Silica
Silicon dioxide
Ultra high molecular weight polyethylene
Silica
Naphthenic oil
Ultra high molecular weight polyethylene
Online AccessGet full text
ISSN0032-3861
1873-2291
DOI10.1016/j.polymer.2016.05.021

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Abstract Ultrahigh molecular weight polyethylene (UHMW-PE) belongs to the specialty polymer grade because of its unique properties. Among other applications, it is used for battery separator membranes elaboration for automotive applications. These PE separators are porous membranes composed of a blend of UHMW-PE, naphthenic oil and precipitated silica. With the aim of understanding the membrane structuring mechanisms, we studied the influence of silica and oil concentrations on the UHMW-PE crystallization during the elaboration process. Results have shown that the high initial thickness of the UHMW-PE crystals is reduced after the process. Moreover, χc (crystallinity) and Tc (crystallization temperature) are both controlled by the volume fraction of oil. The initial high crystallinity of UHMW-PE (χc ≈ 65%) can be increased in the membrane with a high Oil/PE ratio. Furthermore, silica indirectly contributes to enhance the UHMW-PE crystallinity by acting as a reservoir, hence increasing the possible oil content in the blend. [Display omitted] •Crystallinity of UHMWPE in different blends with Oil and Silica is analyzed.•Melting behavior is successfully analyzed with the Flory-Huggins theory.•Crystallinity of nascent UHMWPE powder is recovered in the presence of oil.•Silica acts as an oil reservoir thus enhancing the UHMW-PE crystallinity.
AbstractList Ultrahigh molecular weight polyethylene (UHMW-PE) belongs to the specialty polymer grade because of its unique properties. Among other applications, it is used for battery separator membranes elaboration for automotive applications. These PE separators are porous membranes composed of a blend of UHMWPE, naphthenic oil and precipitated silica. With the aim of understanding the membrane structuring mechanisms, we studied the influence of silica and oil concentrations on the UHMW-PE crystallization during the elaboration process. Results have shown that the high initial thickness of the UHMW-PE crystals is reduced after the process. Moreover, chi(C) (crystallinity) and T-C (crystallization temperature) are both controlled by the volume fraction of oil. The initial high crystallinity of UHMW-PE (chi(C) approximate to 65%) can be increased in the membrane with a high Oil/PE ratio. Furthermore, silica indirectly contributes to enhance the UHMW-PE crystallinity by acting as a reservoir, hence increasing the possible oil content in the blend.
Ultrahigh molecular weight polyethylene (UHMW-PE) belongs to the specialty polymer grade because of its unique properties. Among other applications, it is used for battery separator membranes elaboration for automotive applications. These PE separators are porous membranes composed of a blend of UHMW-PE, naphthenic oil and precipitated silica. With the aim of understanding the membrane structuring mechanisms, we studied the influence of silica and oil concentrations on the UHMW-PE crystallization during the elaboration process. Results have shown that the high initial thickness of the UHMW-PE crystals is reduced after the process. Moreover, χc (crystallinity) and Tc (crystallization temperature) are both controlled by the volume fraction of oil. The initial high crystallinity of UHMW-PE (χc ≈ 65%) can be increased in the membrane with a high Oil/PE ratio. Furthermore, silica indirectly contributes to enhance the UHMW-PE crystallinity by acting as a reservoir, hence increasing the possible oil content in the blend. [Display omitted] •Crystallinity of UHMWPE in different blends with Oil and Silica is analyzed.•Melting behavior is successfully analyzed with the Flory-Huggins theory.•Crystallinity of nascent UHMWPE powder is recovered in the presence of oil.•Silica acts as an oil reservoir thus enhancing the UHMW-PE crystallinity.
Ultrahigh molecular weight polyethylene (UHMW-PE) belongs to the specialty polymer grade because of its unique properties. Among other applications, it is used for battery separator membranes elaboration for automotive applications. These PE separators are porous membranes composed of a blend of UHMW-PE, naphthenic oil and precipitated silica. With the aim of understanding the membrane structuring mechanisms, we studied the influence of silica and oil concentrations on the UHMW-PE crystallization during the elaboration process. Results have shown that the high initial thickness of the UHMW-PE crystals is reduced after the process. Moreover, chi c (crystallinity) and T c (crystallization temperature) are both controlled by the volume fraction of oil. The initial high crystallinity of UHMW-PE ( chi c approximately 65%) can be increased in the membrane with a high Oil/PE ratio. Furthermore, silica indirectly contributes to enhance the UHMW-PE crystallinity by acting as a reservoir, hence increasing the possible oil content in the blend.
Author Cassagnau, Philippe
Toquet, Fabien
Fulchiron, René
Guy, Laurent
Schlegel, Brice
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Keywords Silica
Naphthenic oil
Ultra high molecular weight polyethylene
Language English
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Snippet Ultrahigh molecular weight polyethylene (UHMW-PE) belongs to the specialty polymer grade because of its unique properties. Among other applications, it is used...
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SubjectTerms Blends
Chemical Sciences
Crystallinity
Crystallization
Crystals
Material chemistry
Membranes
Naphthenic oil
Polyethylenes
Polymers
Separators
Silica
Silicon dioxide
Ultra high molecular weight polyethylene
Title Effect of the naphthenic oil and precipitated silica on the crystallization of ultrahigh-molecular-weight polyethylene
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