Benevolent behavior of Kleinia grandiflora leaf extract as a green corrosion inhibitor for mild steel in sulfuric acid solution
The ethanolic extract of Kleinia grandiflora leaves was characterized and tested for its potential anticorrosion properties on mild steel in 1 M H2SO4 medium using mass-loss analysis, potentiodynamic polarization measurements, electrochemical impedance spectroscopy, Fourier-transform infrared spectr...
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| Published in | International journal of minerals, metallurgy and materials Vol. 21; no. 11; pp. 1083 - 1095 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Beijing
University of Science and Technology Beijing
01.11.2014
Springer Nature B.V |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1674-4799 1869-103X |
| DOI | 10.1007/s12613-014-1013-7 |
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| Abstract | The ethanolic extract of Kleinia grandiflora leaves was characterized and tested for its potential anticorrosion properties on mild steel in 1 M H2SO4 medium using mass-loss analysis, potentiodynamic polarization measurements, electrochemical impedance spectroscopy, Fourier-transform infrared spectroscopy, scanning electron microscopy, UV–visible spectroscopy, and X-ray diffraction analysis. The effect of temperature on the corrosion behavior of mild steel was studied in the range of 308 to 328 K. The inhibition efficiency was observed to increase with increasing concentration of the extract. Polarization curves revealed that the Kleinia grandiflora leaf extract is a mixed inhibitor. Impedance diagrams revealed that an increase of Kleinia grandiflora leaf extract concentration increased the charge transfer resistance and decreased the double-layer capacitance. The adsorption process obeys Langmuir＇s model, with a standard free energy of adsorption（ΔGads） of-18.62 k J/mol. The obtained results indicate that the Kleinia grandiflora leaf extract can serve as an effective inhibitor for the corrosion of mild steel in a sulfuric acid medium. |
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| AbstractList | The ethanolic extract of Kleinia grandiflora leaves was characterized and tested for its potential anticorrosion properties on mild steel in 1 M H2SO4 medium using mass-loss analysis, potentiodynamic polarization measurements, electrochemical impedance spectroscopy, Fourier-transform infrared spectroscopy, scanning electron microscopy, UV-visible spectroscopy, and X-ray diffraction analysis. The effect of temperature on the corrosion behavior of mild steel was studied in the range of 308 to 328 K. The inhibition efficiency was observed to increase with increasing concentration of the extract. Polarization curves revealed that the Kleinia grandiflora leaf extract is a mixed inhibitor. Impedance diagrams revealed that an increase of Kleinia grandiflora leaf extract concentration increased the charge transfer resistance and decreased the double-layer capacitance. The adsorption process obeys Langmuir’s model, with a standard free energy of adsorption (ΔGads) of −18.62 kJ/mol. The obtained results indicate that the Kleinia grandiflora leaf extract can serve as an effective inhibitor for the corrosion of mild steel in a sulfuric acid medium. The ethanolic extract of Kleinia grandiflora leaves was characterized and tested for its potential anticorrosion properties on mild steel in 1 M H2SO4 medium using mass-loss analysis, potentiodynamic polarization measurements, electrochemical impedance spectroscopy, Fourier-transform infrared spectroscopy, scanning electron microscopy, UV–visible spectroscopy, and X-ray diffraction analysis. The effect of temperature on the corrosion behavior of mild steel was studied in the range of 308 to 328 K. The inhibition efficiency was observed to increase with increasing concentration of the extract. Polarization curves revealed that the Kleinia grandiflora leaf extract is a mixed inhibitor. Impedance diagrams revealed that an increase of Kleinia grandiflora leaf extract concentration increased the charge transfer resistance and decreased the double-layer capacitance. The adsorption process obeys Langmuir＇s model, with a standard free energy of adsorption（ΔGads） of-18.62 k J/mol. The obtained results indicate that the Kleinia grandiflora leaf extract can serve as an effective inhibitor for the corrosion of mild steel in a sulfuric acid medium. The ethanolic extract of Kleinia grandiflora leaves was characterized and tested for its potential anticorrosion properties on mild steel in 1 M H 2 SO 4 medium using mass-loss analysis, potentiodynamic polarization measurements, electrochemical impedance spectroscopy, Fourier-transform infrared spectroscopy, scanning electron microscopy, UV-visible spectroscopy, and X-ray diffraction analysis. The effect of temperature on the corrosion behavior of mild steel was studied in the range of 308 to 328 K. The inhibition efficiency was observed to increase with increasing concentration of the extract. Polarization curves revealed that the Kleinia grandiflora leaf extract is a mixed inhibitor. Impedance diagrams revealed that an increase of Kleinia grandiflora leaf extract concentration increased the charge transfer resistance and decreased the double-layer capacitance. The adsorption process obeys Langmuir’s model, with a standard free energy of adsorption (Δ G ads ) of −18.62 kJ/mol. The obtained results indicate that the Kleinia grandiflora leaf extract can serve as an effective inhibitor for the corrosion of mild steel in a sulfuric acid medium. The ethanolic extract of Kleinia grandiflora leaves was characterized and tested for its potential anticorrosion properties on mild steel in 1 M H sub(2)SO sub(4) medium using mass-loss analysis, potentiodynamic polarization measurements, electrochemical impedance spectroscopy, Fourier-transform infrared spectroscopy, scanning electron microscopy, UV-visible spectroscopy, and X-ray diffraction analysis. The effect of temperature on the corrosion behavior of mild steel was studied in the range of 308 to 328 K. The inhibition efficiency was observed to increase with increasing concentration of the extract. Polarization curves revealed that the Kleinia grandiflora leaf extract is a mixed inhibitor. Impedance diagrams revealed that an increase of Kleinia grandiflora leaf extract concentration increased the charge transfer resistance and decreased the double-layer capacitance. The adsorption process obeys Langmuir's model, with a standard free energy of adsorption ( Delta G sub(ads)) of-18.62 kJ/mol. The obtained results indicate that the Kleinia grandiflora leaf extract can serve as an effective inhibitor for the corrosion of mild steel in a sulfuric acid medium. |
| Author | Muthukrishnan Pitchaipillai Karthik Raj Jeyaprabha Balasubramanian Prakash Periakaruppan |
| AuthorAffiliation | Department of Chemistry, Faculty of Engineering, Karpagam University, Coimbatore-641021, Tamil Nadu, India Department of Chemistry, Thiagarajar College, Madurai-625009, Tamil Nadu, India Deparanent of Civil Engineering, Fatima Michael College of Engineering ＆Technology, Madurai-625020, Tamil Nadu, India |
| Author_xml | – sequence: 1 givenname: Muthukrishnan surname: Pitchaipillai fullname: Pitchaipillai, Muthukrishnan organization: Department of Chemistry, Faculty of Engineering, Karpagam University – sequence: 2 givenname: Karthik surname: Raj fullname: Raj, Karthik organization: Department of Chemistry, Thiagarajar College – sequence: 3 givenname: Jeyaprabha surname: Balasubramanian fullname: Balasubramanian, Jeyaprabha organization: Department of Civil Engineering, Fatima Michael College of Engineering &Technology – sequence: 4 givenname: Prakash surname: Periakaruppan fullname: Periakaruppan, Prakash email: kmpprakash@gmail.com organization: Department of Chemistry, Thiagarajar College |
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| Copyright | University of Science and Technology Beijing and Springer-Verlag Berlin Heidelberg 2014 University of Science and Technology Beijing and Springer-Verlag Berlin Heidelberg 2014. |
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| Notes | steel corrosion mild steel sulfuric acid corrosion inhibitors The ethanolic extract of Kleinia grandiflora leaves was characterized and tested for its potential anticorrosion properties on mild steel in 1 M H2SO4 medium using mass-loss analysis, potentiodynamic polarization measurements, electrochemical impedance spectroscopy, Fourier-transform infrared spectroscopy, scanning electron microscopy, UV–visible spectroscopy, and X-ray diffraction analysis. The effect of temperature on the corrosion behavior of mild steel was studied in the range of 308 to 328 K. The inhibition efficiency was observed to increase with increasing concentration of the extract. Polarization curves revealed that the Kleinia grandiflora leaf extract is a mixed inhibitor. Impedance diagrams revealed that an increase of Kleinia grandiflora leaf extract concentration increased the charge transfer resistance and decreased the double-layer capacitance. The adsorption process obeys Langmuir＇s model, with a standard free energy of adsorption（ΔGads） of-18.62 k J/mol. The obtained results indicate that the Kleinia grandiflora leaf extract can serve as an effective inhibitor for the corrosion of mild steel in a sulfuric acid medium. 11-5787/T ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 14 content type line 23 |
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| Snippet | The ethanolic extract of Kleinia grandiflora leaves was characterized and tested for its potential anticorrosion properties on mild steel in 1 M H2SO4 medium... The ethanolic extract of Kleinia grandiflora leaves was characterized and tested for its potential anticorrosion properties on mild steel in 1 M H 2 SO 4... The ethanolic extract of Kleinia grandiflora leaves was characterized and tested for its potential anticorrosion properties on mild steel in 1 M H sub(2)SO... |
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| SubjectTerms | Adsorption Carbon steels Ceramics Characterization and Evaluation of Materials Charge transfer Chemistry and Materials Science Composites Corrosion Corrosion and Coatings Corrosion effects Corrosion inhibitors Corrosion prevention Electrochemical impedance spectroscopy Electrochemistry Extractive metallurgy Fourier transforms Free energy Glass Green chemistry Impedance Infrared analysis Infrared spectroscopy Inhibition Langmuir Low carbon steels Materials Science Metallic Materials Natural Materials Plant extracts Polarization Spectrum analysis Steel Sulfuric acid Surfaces and Interfaces Temperature effects Thin Films Tribology X-ray diffraction 低碳钢 傅立叶变换红外光谱仪 叶提取物 玉兰 硫酸溶液 绿色缓蚀剂 腐蚀行为 |
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| Title | Benevolent behavior of Kleinia grandiflora leaf extract as a green corrosion inhibitor for mild steel in sulfuric acid solution |
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