Immobilization of MIL-88(Fe) anchored TiO2-chitosan(2D/2D) hybrid nanocomposite for the degradation of organophosphate pesticide: Characterization, mechanism and degradation intermediates
In this study, we have rationally designed and grafted a bio-assisted 2D/2D TiO2/MIL-88(Fe) (TCS@MOF) heterojunction by growing granular TiO2 on the surface of MIL-88(Fe) nanosheet, as hybrid photocatalyst. The hierarchical TCS@MOF composite was prepared via the one-pot solvothermal process and empl...
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| Published in | Journal of hazardous materials Vol. 406; p. 124728 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
15.03.2021
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| Subjects | |
| Online Access | Get full text |
| ISSN | 0304-3894 1873-3336 1873-3336 |
| DOI | 10.1016/j.jhazmat.2020.124728 |
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| Abstract | In this study, we have rationally designed and grafted a bio-assisted 2D/2D TiO2/MIL-88(Fe) (TCS@MOF) heterojunction by growing granular TiO2 on the surface of MIL-88(Fe) nanosheet, as hybrid photocatalyst. The hierarchical TCS@MOF composite was prepared via the one-pot solvothermal process and employed for monocrotophos (MCP) degradation under visible light region, since its persistent nature on soil and water causes major threat to the environment. The TCS@MOF promotes a number of packed high-speed nano-tunnels in the (p-n) heterojunctions, which significantly enhance the migration of photo-induced electrons (e−) and holes (h+), respectively and thus limits the charge recombination of e−s. The optimized photocatalyst achieves significant catalytic activity of ~98.79% for the degradation of MCP within 30 min of irradiation. The prominent oxidative radicals namely •OH, •O2− etc., were involved in the oxidation of organic pesticide. Besides, TCS@MOF exhibits outstanding stability even after five repetitive cycles for the oxidation of MCP with a negligible decrease in photo-activity. The proposed mechanism and oxidative pathways of MCP were rationally deduced in detail subject to experimental results. The mechanism renders insight into the oxidation and consequent bond rupture of pollutant as well as into the formation of products such as H2O, CO2, etc. This report unveils a novel architecture of proficiently optimized TCS@MOF material structure for the perceptive oxidation of organic contaminants.
[Display omitted]
●A rational TCS@MOF was fabricated through solvothermal method.●TCS@MOF was used to degrade MCP via visible light irradiation.●Investigation of various influencing parameters and batch studies were carried out.●TCS@MOF exhibited excellent photo-stability over five regeneration cycles.●A possible mechanism for MCP degradation by the photocatalyst was proposed. |
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| AbstractList | In this study, we have rationally designed and grafted a bio-assisted 2D/2D TiO2/MIL-88(Fe) (TCS@MOF) heterojunction by growing granular TiO2 on the surface of MIL-88(Fe) nanosheet, as hybrid photocatalyst. The hierarchical TCS@MOF composite was prepared via the one-pot solvothermal process and employed for monocrotophos (MCP) degradation under visible light region, since its persistent nature on soil and water causes major threat to the environment. The TCS@MOF promotes a number of packed high-speed nano-tunnels in the (p-n) heterojunctions, which significantly enhance the migration of photo-induced electrons (e-) and holes (h+), respectively and thus limits the charge recombination of e-s. The optimized photocatalyst achieves significant catalytic activity of ~98.79% for the degradation of MCP within 30 min of irradiation. The prominent oxidative radicals namely •OH, •O2- etc., were involved in the oxidation of organic pesticide. Besides, TCS@MOF exhibits outstanding stability even after five repetitive cycles for the oxidation of MCP with a negligible decrease in photo-activity. The proposed mechanism and oxidative pathways of MCP were rationally deduced in detail subject to experimental results. The mechanism renders insight into the oxidation and consequent bond rupture of pollutant as well as into the formation of products such as H2O, CO2, etc. This report unveils a novel architecture of proficiently optimized TCS@MOF material structure for the perceptive oxidation of organic contaminants.In this study, we have rationally designed and grafted a bio-assisted 2D/2D TiO2/MIL-88(Fe) (TCS@MOF) heterojunction by growing granular TiO2 on the surface of MIL-88(Fe) nanosheet, as hybrid photocatalyst. The hierarchical TCS@MOF composite was prepared via the one-pot solvothermal process and employed for monocrotophos (MCP) degradation under visible light region, since its persistent nature on soil and water causes major threat to the environment. The TCS@MOF promotes a number of packed high-speed nano-tunnels in the (p-n) heterojunctions, which significantly enhance the migration of photo-induced electrons (e-) and holes (h+), respectively and thus limits the charge recombination of e-s. The optimized photocatalyst achieves significant catalytic activity of ~98.79% for the degradation of MCP within 30 min of irradiation. The prominent oxidative radicals namely •OH, •O2- etc., were involved in the oxidation of organic pesticide. Besides, TCS@MOF exhibits outstanding stability even after five repetitive cycles for the oxidation of MCP with a negligible decrease in photo-activity. The proposed mechanism and oxidative pathways of MCP were rationally deduced in detail subject to experimental results. The mechanism renders insight into the oxidation and consequent bond rupture of pollutant as well as into the formation of products such as H2O, CO2, etc. This report unveils a novel architecture of proficiently optimized TCS@MOF material structure for the perceptive oxidation of organic contaminants. In this study, we have rationally designed and grafted a bio-assisted 2D/2D TiO₂/MIL-88(Fe) (TCS@MOF) heterojunction by growing granular TiO₂ on the surface of MIL-88(Fe) nanosheet, as hybrid photocatalyst. The hierarchical TCS@MOF composite was prepared via the one-pot solvothermal process and employed for monocrotophos (MCP) degradation under visible light region, since its persistent nature on soil and water causes major threat to the environment. The TCS@MOF promotes a number of packed high-speed nano-tunnels in the (p-n) heterojunctions, which significantly enhance the migration of photo-induced electrons (e⁻) and holes (h⁺), respectively and thus limits the charge recombination of e⁻s. The optimized photocatalyst achieves significant catalytic activity of ~98.79% for the degradation of MCP within 30 min of irradiation. The prominent oxidative radicals namely •OH, •O₂⁻ etc., were involved in the oxidation of organic pesticide. Besides, TCS@MOF exhibits outstanding stability even after five repetitive cycles for the oxidation of MCP with a negligible decrease in photo-activity. The proposed mechanism and oxidative pathways of MCP were rationally deduced in detail subject to experimental results. The mechanism renders insight into the oxidation and consequent bond rupture of pollutant as well as into the formation of products such as H₂O, CO₂, etc. This report unveils a novel architecture of proficiently optimized TCS@MOF material structure for the perceptive oxidation of organic contaminants. In this study, we have rationally designed and grafted a bio-assisted 2D/2D TiO2/MIL-88(Fe) (TCS@MOF) heterojunction by growing granular TiO2 on the surface of MIL-88(Fe) nanosheet, as hybrid photocatalyst. The hierarchical TCS@MOF composite was prepared via the one-pot solvothermal process and employed for monocrotophos (MCP) degradation under visible light region, since its persistent nature on soil and water causes major threat to the environment. The TCS@MOF promotes a number of packed high-speed nano-tunnels in the (p-n) heterojunctions, which significantly enhance the migration of photo-induced electrons (e−) and holes (h+), respectively and thus limits the charge recombination of e−s. The optimized photocatalyst achieves significant catalytic activity of ~98.79% for the degradation of MCP within 30 min of irradiation. The prominent oxidative radicals namely •OH, •O2− etc., were involved in the oxidation of organic pesticide. Besides, TCS@MOF exhibits outstanding stability even after five repetitive cycles for the oxidation of MCP with a negligible decrease in photo-activity. The proposed mechanism and oxidative pathways of MCP were rationally deduced in detail subject to experimental results. The mechanism renders insight into the oxidation and consequent bond rupture of pollutant as well as into the formation of products such as H2O, CO2, etc. This report unveils a novel architecture of proficiently optimized TCS@MOF material structure for the perceptive oxidation of organic contaminants. [Display omitted] ●A rational TCS@MOF was fabricated through solvothermal method.●TCS@MOF was used to degrade MCP via visible light irradiation.●Investigation of various influencing parameters and batch studies were carried out.●TCS@MOF exhibited excellent photo-stability over five regeneration cycles.●A possible mechanism for MCP degradation by the photocatalyst was proposed. |
| ArticleNumber | 124728 |
| Author | Sirajudheen, Palliyalil Vigneshwaran, Sivakumar Meenakshi, Sankaran Karthikeyan, Perumal Nikitha, Manuvelraja Ramkumar, Krishnapillai |
| Author_xml | – sequence: 1 givenname: Sivakumar orcidid: 0000-0002-4422-1150 surname: Vigneshwaran fullname: Vigneshwaran, Sivakumar email: vigneshwarangri@gmail.com organization: Department of Chemistry, The Gandhigram Rural Institute – Deemed to be University, Gandhigram 624302, Dindigul, Tamil Nadu, India – sequence: 2 givenname: Palliyalil orcidid: 0000-0002-8988-9613 surname: Sirajudheen fullname: Sirajudheen, Palliyalil email: sirajpalliyalil@gmail.com organization: Department of Chemistry, The Gandhigram Rural Institute – Deemed to be University, Gandhigram 624302, Dindigul, Tamil Nadu, India – sequence: 3 givenname: Perumal surname: Karthikeyan fullname: Karthikeyan, Perumal email: karthi2011chemistry@gmail.com organization: Department of Chemistry, The Gandhigram Rural Institute – Deemed to be University, Gandhigram 624302, Dindigul, Tamil Nadu, India – sequence: 4 givenname: Manuvelraja surname: Nikitha fullname: Nikitha, Manuvelraja email: nikitharose284@gmail.com organization: Department of Chemistry, The Gandhigram Rural Institute – Deemed to be University, Gandhigram 624302, Dindigul, Tamil Nadu, India – sequence: 5 givenname: Krishnapillai surname: Ramkumar fullname: Ramkumar, Krishnapillai email: ramkumarkrishnanls@gmail.com organization: Department of Chemistry, The Gandhigram Rural Institute – Deemed to be University, Gandhigram 624302, Dindigul, Tamil Nadu, India – sequence: 6 givenname: Sankaran orcidid: 0000-0003-3350-2325 surname: Meenakshi fullname: Meenakshi, Sankaran email: sankaranmeenakshi2014@gmail.com organization: Department of Chemistry, The Gandhigram Rural Institute – Deemed to be University, Gandhigram 624302, Dindigul, Tamil Nadu, India |
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| Keywords | TCS@MOF 2D/2D hybrid photocatalyst MCP Mineralization Degradation pathway |
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| Snippet | In this study, we have rationally designed and grafted a bio-assisted 2D/2D TiO2/MIL-88(Fe) (TCS@MOF) heterojunction by growing granular TiO2 on the surface of... In this study, we have rationally designed and grafted a bio-assisted 2D/2D TiO₂/MIL-88(Fe) (TCS@MOF) heterojunction by growing granular TiO₂ on the surface of... |
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| SubjectTerms | 2D/2D hybrid photocatalyst carbon dioxide catalytic activity Degradation pathway irradiation light MCP Mineralization monocrotophos nanocomposites nanosheets oxidation photocatalysts pollutants soil TCS@MOF |
| Title | Immobilization of MIL-88(Fe) anchored TiO2-chitosan(2D/2D) hybrid nanocomposite for the degradation of organophosphate pesticide: Characterization, mechanism and degradation intermediates |
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